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Information card for entry 7702757
Preview
| Coordinates | 7702757.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C55 H95 K2 Li N6 O20 |
|---|---|
| Calculated formula | C55 H95 K2 Li N6 O20 |
| Title of publication | Formation of [M(15-crown-5)2]2[Li(NHPy)3] (M = K or Cs): the first structurally authenticated examples of a monomeric lithium species coordinated by three amide anions |
| Authors of publication | Liddle, Stephen T.; Clegg, William |
| Journal of publication | Journal of the Chemical Society, Dalton Transactions |
| Year of publication | 2001 |
| Journal issue | 24 |
| Pages of publication | 3549 |
| a | 13.5783 ± 0.001 Å |
| b | 15.1526 ± 0.0011 Å |
| c | 17.5303 ± 0.0013 Å |
| α | 76.265 ± 0.002° |
| β | 75.313 ± 0.002° |
| γ | 69.484 ± 0.002° |
| Cell volume | 3223.4 ± 0.4 Å3 |
| Cell temperature | 160 ± 2 K |
| Ambient diffraction temperature | 160 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1655 |
| Residual factor for significantly intense reflections | 0.0899 |
| Weighted residual factors for significantly intense reflections | 0.2467 |
| Weighted residual factors for all reflections included in the refinement | 0.2941 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.027 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 244004 (current) | 2019-11-28 | cif/ Adding structures of 7702757, 7702758 via cif-deposit CGI script. |
7702757.cif |
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Users of the data should acknowledge the original authors of the
structural data.