Crystallography Open Database

Information card for entry 7702863

Preview

Coordinates	7702863.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C41 H55 Cu Lu N10 O12
Calculated formula	C41 H53 Cu Lu N10 O12
Title of publication	Structural characterisation, EPR and magnetic properties of f‒f and f‒d lanthanide(iii) phenolic cryptates
Authors of publication	Avecilla, Fernando; Platas-Iglesias, Carlos; Rodríguez-Cortiñas, Raquel; Guillemot, Geoffroy; Bünzli, Jean-Claude G.; Brondino, Carlos D.; Geraldes, Carlos F. G. C.; Blas, Andrés de; Rodríguez-Blas, Teresa
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	2002
Journal issue	24
Pages of publication	4658
a	33.067 ± 0.009 Å
b	11.035 ± 0.003 Å
c	25.516 ± 0.007 Å
α	90°
β	104.098 ± 0.005°
γ	90°
Cell volume	9030 ± 4 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0515
Residual factor for significantly intense reflections	0.0351
Weighted residual factors for significantly intense reflections	0.0858
Weighted residual factors for all reflections included in the refinement	0.0915
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
244052 (current)	2019-11-28	cif/ Adding structures of 7702860, 7702861, 7702862, 7702863, 7702864 via cif-deposit CGI script.	7702863.cif