Crystallography Open Database

Information card for entry 7702916

Preview

Coordinates	7702916.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C140 H165 Dy6 N13 Na2 O71
Calculated formula	C138 H127 Dy6 N13 Na2 O56
Title of publication	Synthesis, structures and magnetic properties of a family of nitrate-bridged octanuclear [Na2Ln6] (Ln = Dy, Tb, Gd, Sm) complexes.
Authors of publication	She, Shixiong; Chen, Yanmei; Zaworotko, Michael J.; Liu, Wei; Cao, Yanyuan; Wu, Jian; Li, Yahong
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	29
Pages of publication	10433 - 10438
a	28.498 ± 0.0018 Å
b	19.397 ± 0.0011 Å
c	30.559 ± 0.0018 Å
α	90°
β	103.514 ± 0.0011°
γ	90°
Cell volume	16424.6 ± 1.7 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0414
Residual factor for significantly intense reflections	0.0312
Weighted residual factors for significantly intense reflections	0.0708
Weighted residual factors for all reflections included in the refinement	0.0739
Goodness-of-fit parameter for all reflections included in the refinement	1.015
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
244809 (current)	2019-11-29	cif/ Adding structures of 7702916, 7702917, 7702918, 7702919 via cif-deposit CGI script.	7702916.cif