Crystallography Open Database

Information card for entry 7703007

Preview

Coordinates	7703007.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H60 Ge2 Mo20 N24 Ni7 O90
Calculated formula	C12 H60 Ge2 Mo20 N24 Ni7 O90
Title of publication	Two Ni/Co-substituted sandwich-type germanomolybdates based on an unprecedented trivacant polyanion [α-GeMo<sub>10</sub>O<sub>36</sub>]<sup>8</sup>.
Authors of publication	Xu, Hui; Liu, Xing-Man; Su, Tan; Chen, Wei-Chao; Su, Zhong-Min
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	4
Pages of publication	977 - 982
a	13.933 ± 0.0019 Å
b	14.2147 ± 0.0019 Å
c	14.591 ± 0.002 Å
α	110.716 ± 0.002°
β	98.574 ± 0.002°
γ	112.773 ± 0.002°
Cell volume	2351.2 ± 0.6 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296.15 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0483
Residual factor for significantly intense reflections	0.0351
Weighted residual factors for significantly intense reflections	0.0824
Weighted residual factors for all reflections included in the refinement	0.0893
Goodness-of-fit parameter for all reflections included in the refinement	1.039
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
247707 (current)	2020-02-04	cif/ Updating files of 7703007, 7703008 Original log message: Adding full bibliography for 7703007--7703008.cif.	7703007.cif
245419	2019-12-20	cif/ Adding structures of 7703007, 7703008 via cif-deposit CGI script.	7703007.cif