Crystallography Open Database

Information card for entry 7703116

Preview

Coordinates	7703116.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H44 B2 O8 P2
Calculated formula	C28 H44 B2 O8 P2
Title of publication	Addition reactions and diazomethane capture by the intramolecular P-O-B FLP: tBu<sub>2</sub>POBcat.
Authors of publication	Zhu, Diya; Qu, Zheng-Wang; Stephan, Douglas W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	3
Pages of publication	901 - 910
a	16.8669 ± 0.0015 Å
b	10.5925 ± 0.0008 Å
c	17.1483 ± 0.0015 Å
α	90°
β	90°
γ	90°
Cell volume	3063.8 ± 0.4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150.15 K
Number of distinct elements	5
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0417
Residual factor for significantly intense reflections	0.0328
Weighted residual factors for significantly intense reflections	0.0858
Weighted residual factors for all reflections included in the refinement	0.0994
Goodness-of-fit parameter for all reflections included in the refinement	1.1044
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
247739 (current)	2020-02-04	cif/ Updating files of 7703107, 7703108, 7703109, 7703110, 7703111, 7703112, 7703113, 7703114, 7703115, 7703116 Original log message: Adding full bibliography for 7703107--7703116.cif.	7703116.cif
246382	2020-01-01	cif/ Adding structures of 7703107, 7703108, 7703109, 7703110, 7703111, 7703112, 7703113, 7703114, 7703115, 7703116 via cif-deposit CGI script.	7703116.cif