Crystallography Open Database

Information card for entry 7703256

Preview

Coordinates	7703256.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C109 H130 Cl26 Mo2 O8 P4 Ru4
Calculated formula	C106 H124 Cl20 Mo2 O8 P4 Ru4
Title of publication	A dimolybdenum paddlewheel as a building block for heteromultimetallic structures.
Authors of publication	Knöfel, Nicolai D; Schoo, Christoph; Seifert, Tim P.; Roesky, Peter W.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	5
Pages of publication	1513 - 1521
a	11.4314 ± 0.001 Å
b	17.3797 ± 0.0013 Å
c	17.3723 ± 0.0016 Å
α	91.633 ± 0.007°
β	100.343 ± 0.007°
γ	102.881 ± 0.006°
Cell volume	3301.4 ± 0.5 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1406
Residual factor for significantly intense reflections	0.0931
Weighted residual factors for significantly intense reflections	0.2392
Weighted residual factors for all reflections included in the refinement	0.2821
Goodness-of-fit parameter for all reflections included in the refinement	1.033
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
248934 (current)	2020-03-05	cif/ Updating files of 7703254, 7703255, 7703256, 7703257, 7703258, 7703259 Original log message: Adding full bibliography for 7703254--7703259.cif.	7703256.cif
246725	2020-01-11	cif/ Adding structures of 7703254, 7703255, 7703256, 7703257, 7703258, 7703259 via cif-deposit CGI script.	7703256.cif