Crystallography Open Database

Information card for entry 7703343

Preview

Coordinates	7703343.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43 H70 N4 O2 Si2 Y
Calculated formula	C43 H70 N4 O2 Si2 Y
Title of publication	Bis(alkyl) scandium and yttrium complexes coordinated by an amidopyridinate ligand: synthesis, characterization and catalytic performance in isoprene polymerization, hydroelementation and carbon dioxide hydrosilylation.
Authors of publication	Gurina, G. A.; Kissel, A. A.; Lyubov, D. M.; Luconi, L.; Rossin, A.; Tuci, G.; Cherkasov, A. V.; Lyssenko, K. A.; Shavyrin, A. S.; Ob'edkov, A. M.; Giambastiani, G.; Trifonov, A. A.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	3
Pages of publication	638 - 650
a	11.6694 ± 0.0006 Å
b	13.2058 ± 0.0007 Å
c	17.233 ± 0.0009 Å
α	112.225 ± 0.001°
β	104.719 ± 0.001°
γ	91.704 ± 0.001°
Cell volume	2354.1 ± 0.2 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0845
Residual factor for significantly intense reflections	0.0474
Weighted residual factors for significantly intense reflections	0.0981
Weighted residual factors for all reflections included in the refinement	0.1101
Goodness-of-fit parameter for all reflections included in the refinement	1.007
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
247075 (current)	2020-01-22	cif/ Adding structures of 7703341, 7703342, 7703343 via cif-deposit CGI script.	7703343.cif