Crystallography Open Database

Information card for entry 7703402

Preview

Coordinates	7703402.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H36 As4 Cl6 K N36 Na O154 Ru6 W42
Calculated formula	C24 H36 As4 Cl6 K N36 Na O154 Ru6 W42
Title of publication	Trinuclear ruthenium core-containing polyoxometalate-based hybrids: preparation, characterization and catalytic behavior.
Authors of publication	Li, Huafeng; He, Peipei; Wan, Rong; Zou, Yan; Zhao, Xue; Ma, Pengtao; Niu, Jingyang; Wang, Jingping
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	9
Pages of publication	2895 - 2904
a	20.0498 ± 0.0011 Å
b	24.3323 ± 0.0011 Å
c	25.4119 ± 0.0012 Å
α	89.231 ± 0.002°
β	72.661 ± 0.002°
γ	80.351 ± 0.002°
Cell volume	11657.8 ± 1 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 K
Number of distinct elements	10
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1335
Residual factor for significantly intense reflections	0.1042
Weighted residual factors for significantly intense reflections	0.2754
Weighted residual factors for all reflections included in the refinement	0.3173
Goodness-of-fit parameter for all reflections included in the refinement	1.134
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
248978 (current)	2020-03-05	cif/ Updating files of 7703402, 7703403 Original log message: Adding full bibliography for 7703402--7703403.cif.	7703402.cif
247370	2020-01-30	cif/ Adding structures of 7703402, 7703403 via cif-deposit CGI script.	7703402.cif