Crystallography Open Database

Information card for entry 7703418

Preview

Coordinates	7703418.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H36 B Co N6 O4
Calculated formula	C48 H36 B Co N6 O4
Title of publication	Oxidative C-N bond cleavage of (2-pyridylmethyl)amine-based tetradentate supporting ligands in ternary cobalt(ii)-carboxylate complexes.
Authors of publication	Chakraborty, Biswarup; Ghosh, Ivy; Jana, Rahul Dev; Paine, Tapan Kanti
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	11
Pages of publication	3463 - 3472
a	13.263 ± 0.002 Å
b	14.74 ± 0.003 Å
c	15.25 ± 0.005 Å
α	102.166 ± 0.006°
β	100.967 ± 0.006°
γ	113.879 ± 0.004°
Cell volume	2535.1 ± 1.1 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0722
Residual factor for significantly intense reflections	0.0536
Weighted residual factors for significantly intense reflections	0.0892
Weighted residual factors for all reflections included in the refinement	0.0912
Goodness-of-fit parameter for all reflections included in the refinement	1.963
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
250301 (current)	2020-04-05	cif/ Updating files of 7703417, 7703418, 7703419, 7703420, 7703421 Original log message: Adding full bibliography for 7703417--7703421.cif.	7703418.cif
247428	2020-02-01	cif/ Adding structures of 7703417, 7703418, 7703419, 7703420, 7703421 via cif-deposit CGI script.	7703418.cif