Crystallography Open Database

Information card for entry 7704238

Preview

Coordinates	7704238.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H36 I N4 P2 Sb
Calculated formula	C16 H36 I N4 P2 Sb
SMILES	C(C)(C)(C)N1P2N(C(C)(C)C)P3[N]2(C(C)(C)C)[Sb]1(N3C(C)(C)C)I
Title of publication	Covalent and ionic bonding in bi- and tricyclic Group 15 amides: equidistant P-I and As-I bonds and fluxional cations.
Authors of publication	Musongong, Joseph T.; Otang, Mathew E.; Mash, Brandon L.; Zeller, Matthias; Stahl, Lothar
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	19
Pages of publication	6341 - 6354
a	9.606 ± 0.0006 Å
b	18.7374 ± 0.0012 Å
c	26.7135 ± 0.0018 Å
α	90°
β	93.325 ± 0.003°
γ	90°
Cell volume	4800.1 ± 0.5 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0501
Residual factor for significantly intense reflections	0.0333
Weighted residual factors for significantly intense reflections	0.0732
Weighted residual factors for all reflections included in the refinement	0.0806
Goodness-of-fit parameter for all reflections included in the refinement	1.0235
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
252767 (current)	2020-06-05	cif/ Updating files of 7704230, 7704231, 7704232, 7704233, 7704234, 7704235, 7704236, 7704237, 7704238, 7704239 Original log message: Adding full bibliography for 7704230--7704239.cif.	7704238.cif
251299	2020-04-30	cif/ Adding structures of 7704230, 7704231, 7704232, 7704233, 7704234, 7704235, 7704236, 7704237, 7704238, 7704239 via cif-deposit CGI script.	7704238.cif