Crystallography Open Database

Information card for entry 7704508

Preview

Coordinates	7704508.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22.36 H35.49 Cl2.75 Mo N3 O4 P3
Calculated formula	C22.361 H34.682 Cl2.742 Mo N3 O4 P3
Title of publication	1,3,4-Azadiphospholides as building blocks for scorpionate and bidentate ligands in multinuclear complexes.
Authors of publication	Suter, Riccardo; Wagner, Mona; Querci, Lorenzo; Conti, Riccardo; Benkő, Zoltán; Grützmacher, Hansjörg
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	24
Pages of publication	8201 - 8208
a	59.1004 ± 0.0011 Å
b	34.6994 ± 0.0006 Å
c	12.38327 ± 0.00019 Å
α	90°
β	90°
γ	90°
Cell volume	25395 ± 0.8 Å³
Cell temperature	106.05 ± 0.13 K
Ambient diffraction temperature	106.05 ± 0.13 K
Number of distinct elements	7
Space group number	43
Hermann-Mauguin space group symbol	F d d 2
Hall space group symbol	F 2 -2d
Residual factor for all reflections	0.0503
Residual factor for significantly intense reflections	0.0471
Weighted residual factors for significantly intense reflections	0.1077
Weighted residual factors for all reflections included in the refinement	0.1093
Goodness-of-fit parameter for all reflections included in the refinement	1.096
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
253867 (current)	2020-07-06	cif/ Updating files of 7704506, 7704507, 7704508, 7704509, 7704510, 7704511, 7704512, 7704513, 7704514, 7704515, 7704516, 7704517 Original log message: Adding full bibliography for 7704506--7704517.cif.	7704508.cif
252421	2020-05-28	cif/ Adding structures of 7704506, 7704507, 7704508, 7704509, 7704510, 7704511, 7704512, 7704513, 7704514, 7704515, 7704516, 7704517 via cif-deposit CGI script.	7704508.cif