Crystallography Open Database

Information card for entry 7704714

Preview

Coordinates	7704714.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H52 Al Br F36 Ge2 N6 O4
Calculated formula	C52 H52 Al Br F36 Ge2 N6 O4
Title of publication	Cooperative N-H bond activation by amido-Ge(ii) cations.
Authors of publication	Zhou, Xueer; Vasko, Petra; Hicks, Jamie; Fuentes, M Ángeles; Heilmann, Andreas; Kolychev, Eugene L.; Aldridge, Simon
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	27
Pages of publication	9495 - 9504
a	11.0633 ± 0.0001 Å
b	18.7791 ± 0.0002 Å
c	18.8201 ± 0.0002 Å
α	61.968 ± 0.001°
β	80.519 ± 0.001°
γ	80.424 ± 0.001°
Cell volume	3386.38 ± 0.07 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0293
Residual factor for significantly intense reflections	0.0265
Weighted residual factors for significantly intense reflections	0.0662
Weighted residual factors for all reflections included in the refinement	0.0681
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
254978 (current)	2020-08-06	cif/ Updating files of 7704706, 7704707, 7704708, 7704709, 7704710, 7704711, 7704712, 7704713, 7704714 Original log message: Adding full bibliography for 7704706--7704714.cif.	7704714.cif
253467	2020-06-26	cif/ Adding structures of 7704706, 7704707, 7704708, 7704709, 7704710, 7704711, 7704712, 7704713, 7704714 via cif-deposit CGI script.	7704714.cif