Crystallography Open Database

Information card for entry 7705074

Preview

Coordinates	7705074.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C56.5 H42 Cl N12 O4 Zn2
Calculated formula	C56.5 H42 Cl N12 O4 Zn2
Title of publication	Zinc complexes supported by pyridine-<i>N</i>-oxide ligands: synthesis, structures and catalytic Michael addition reactions.
Authors of publication	Mo, Xiu-Fang; Xiong, Chang-Feng; Chen, Ze-Wen; Liu, Chao; He, Piao; Tong, Hai-Xia; Yi, Xiao-Yi
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	35
Pages of publication	12365 - 12371
a	31.092 ± 0.003 Å
b	17.2866 ± 0.0016 Å
c	9.3852 ± 0.0009 Å
α	90°
β	92.426 ± 0.006°
γ	90°
Cell volume	5039.8 ± 0.8 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.2148
Residual factor for significantly intense reflections	0.0703
Weighted residual factors for significantly intense reflections	0.1489
Weighted residual factors for all reflections included in the refinement	0.1806
Goodness-of-fit parameter for all reflections included in the refinement	0.893
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
257551 (current)	2020-10-06	cif/ Updating files of 7705072, 7705073, 7705074, 7705075 Original log message: Adding full bibliography for 7705072--7705075.cif.	7705074.cif
255200	2020-08-08	cif/ Adding structures of 7705072, 7705073, 7705074, 7705075 via cif-deposit CGI script.	7705074.cif