Crystallography Open Database

Information card for entry 7705681

Preview

Coordinates	7705681.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	[GaP(py){(NDipp)2C12H5}]2*2OEt2
Formula	C90 H110 Ga2 N6 O2 P2
Calculated formula	C90 H110 Ga2 N6 O2 P2
Title of publication	Synthesis and decarbonylation chemistry of gallium phosphaketenes.
Authors of publication	Wilson, Daniel W. N.; Myers, William K.; Goicoechea, Jose M.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	43
Pages of publication	15249 - 15255
a	12.23 ± 0.0003 Å
b	22.2691 ± 0.0004 Å
c	15.9009 ± 0.0004 Å
α	90°
β	111.732 ± 0.003°
γ	90°
Cell volume	4022.83 ± 0.18 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0676
Residual factor for significantly intense reflections	0.0413
Weighted residual factors for significantly intense reflections	0.0873
Weighted residual factors for all reflections included in the refinement	0.099
Goodness-of-fit parameter for all reflections included in the refinement	1.026
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
260742 (current)	2021-01-07	cif/ Updating files of 7705675, 7705676, 7705677, 7705678, 7705679, 7705680, 7705681, 7705682, 7705683 Original log message: Adding full bibliography for 7705675--7705683.cif.	7705681.cif
258354	2020-10-14	cif/ Adding structures of 7705675, 7705676, 7705677, 7705678, 7705679, 7705680, 7705681, 7705682, 7705683 via cif-deposit CGI script.	7705681.cif