Crystallography Open Database

Information card for entry 7705685

Preview

Coordinates	7705685.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C99.5 H90 N2 O2 Yb
Calculated formula	C99.5 H90 N2 O2 Yb
Title of publication	Low-coordinate Sm(II) and Yb(II) complexes derived from sterically-hindered 1,2-bis(imino)acenaphthene (Ar<sup>BIG</sup>-bian).
Authors of publication	Lukina, Daria A.; Skatova, Alexandra A.; Sokolov, Vladimir G.; Baranov, Evgenii V.; Demeshko, Serhiy; Ketkov, Sergey Yu; Fedushkin, Igor L.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	41
Pages of publication	14445 - 14451
a	12.9233 ± 0.0004 Å
b	14.4027 ± 0.0005 Å
c	22.7605 ± 0.0007 Å
α	87.887 ± 0.001°
β	74.114 ± 0.001°
γ	67.067 ± 0.001°
Cell volume	3740.9 ± 0.2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0301
Residual factor for significantly intense reflections	0.0255
Weighted residual factors for significantly intense reflections	0.0595
Weighted residual factors for all reflections included in the refinement	0.0608
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
258798 (current)	2020-11-06	cif/ Updating files of 7705684, 7705685, 7705686 Original log message: Adding full bibliography for 7705684--7705686.cif.	7705685.cif
258355	2020-10-14	cif/ Adding structures of 7705684, 7705685, 7705686 via cif-deposit CGI script.	7705685.cif