Crystallography Open Database

Information card for entry 7705688

Preview

Coordinates	7705688.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C72 H136 K2 N12 O4 P2
Calculated formula	C72 H136 K2 N12 O4 P2
Title of publication	Homoleptic cerium tris(dialkylamido)imidophosphorane guanidinate complexes.
Authors of publication	Aguirre Quintana, Luis M.; Jiang, Ningxin; Bacsa, John; La Pierre, Henry S.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	42
Pages of publication	14908 - 14913
a	16.8786 ± 0.0016 Å
b	20.72 ± 0.002 Å
c	22.088 ± 0.002 Å
α	90°
β	92.938 ± 0.004°
γ	90°
Cell volume	7714.6 ± 1.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1964
Residual factor for significantly intense reflections	0.1627
Weighted residual factors for significantly intense reflections	0.4009
Weighted residual factors for all reflections included in the refinement	0.4197
Goodness-of-fit parameter for all reflections included in the refinement	2.808
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
258807 (current)	2020-11-06	cif/ Updating files of 7705688, 7705689, 7705690 Original log message: Adding full bibliography for 7705688--7705690.cif.	7705688.cif
258411	2020-10-15	cif/ Adding structures of 7705688, 7705689, 7705690 via cif-deposit CGI script.	7705688.cif