Crystallography Open Database

Information card for entry 7705813

Preview

Coordinates	7705813.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C55.5 H88 Cu5 Dy4 N12 O33.5
Calculated formula	C50 H76 Cu5 Dy4 N10 O32
Title of publication	Further synthetic investigation of the general lanthanoid(iii) [Ln(iii)]/copper(ii)/pyridine-2,6-dimethanol/carboxylate reaction system: {CuLn} coordination clusters (Ln = Dy, Tb, Ho) and their yttrium(iii) analogue.
Authors of publication	Dermitzaki, Despina; Raptopoulou, Catherine P.; Psycharis, Vassilis; Escuer, Albert; Perlepes, Spyros P.; Mayans, Julia; Stamatatos, Theocharis C.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	1
Pages of publication	240 - 251
a	13.1964 ± 0.0004 Å
b	18.9068 ± 0.0006 Å
c	18.3821 ± 0.0006 Å
α	90°
β	98.374 ± 0.002°
γ	90°
Cell volume	4537.5 ± 0.2 Å³
Cell temperature	160 ± 2 K
Ambient diffraction temperature	160 ± 2 K
Number of distinct elements	6
Space group number	12
Hermann-Mauguin space group symbol	I 1 2/m 1
Hall space group symbol	-I 2y
Residual factor for all reflections	0.0418
Residual factor for significantly intense reflections	0.0352
Weighted residual factors for significantly intense reflections	0.0906
Weighted residual factors for all reflections included in the refinement	0.0953
Goodness-of-fit parameter for all reflections included in the refinement	1.058
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
261648 (current)	2021-02-05	cif/ Updating files of 7705813, 7705814, 7705815 Original log message: Adding full bibliography for 7705813--7705815.cif.	7705813.cif
259407	2020-12-01	cif/ Adding structures of 7705813, 7705814, 7705815 via cif-deposit CGI script.	7705813.cif