Crystallography Open Database

Information card for entry 7706358

Preview

Coordinates	7706358.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	4-Cl(Tip)
Formula	C27 H55 B Cl6 P4 Pt2
Calculated formula	C27 H55 B Cl6 P4 Pt2
Title of publication	Synthesis and characterisation of boranediyl- and diboranediyl-bridged diplatinum A-frame complexes.
Authors of publication	Brunecker, Carina; Arrowsmith, Merle; Müssig, Jonas H; Böhnke, Julian; Stoy, Andreas; Heß, Merlin; Hofmann, Alexander; Lenczyk, Carsten; Lichtenberg, Crispin; Ramler, Jacqueline; Rempel, Anna; Braunschweig, Holger
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	10
Pages of publication	3506 - 3515
a	15.217 ± 0.007 Å
b	9.891 ± 0.003 Å
c	26.831 ± 0.009 Å
α	90°
β	94.952 ± 0.014°
γ	90°
Cell volume	4023 ± 3 Å³
Cell temperature	102 ± 2 K
Ambient diffraction temperature	102 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0321
Residual factor for significantly intense reflections	0.0242
Weighted residual factors for significantly intense reflections	0.0423
Weighted residual factors for all reflections included in the refinement	0.0449
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
263751 (current)	2021-04-05	cif/ Updating files of 7706356, 7706357, 7706358, 7706359, 7706360, 7706361, 7706362, 7706363, 7706364, 7706365, 7706366, 7706367, 7706368 Original log message: Adding full bibliography for 7706356--7706368.cif.	7706358.cif
260872	2021-01-09	cif/ Adding structures of 7706356, 7706357, 7706358, 7706359, 7706360, 7706361, 7706362, 7706363, 7706364, 7706365, 7706366, 7706367, 7706368 via cif-deposit CGI script.	7706358.cif