Crystallography Open Database

Information card for entry 7706474

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Coordinates	7706474.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H70 Li2 O4
Calculated formula	C42 H70 Li2 O4
Title of publication	Synthesis, characterization, and alkoxide transfer reactivity of dimeric Tl<sub>2</sub>(OR)<sub>2</sub> complexes.
Authors of publication	Grass, Amanda; Kulathungage, Lakshani Wathsala; Wannipurage, Duleeka; Yousif, Maryam; Ward, Cassandra L.; Groysman, Stanislav
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	7
Pages of publication	2501 - 2509
a	11.9523 ± 0.0013 Å
b	21.215 ± 0.003 Å
c	15.9314 ± 0.0018 Å
α	90°
β	93.335 ± 0.005°
γ	90°
Cell volume	4032.9 ± 0.9 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0589
Residual factor for significantly intense reflections	0.0422
Weighted residual factors for significantly intense reflections	0.1027
Weighted residual factors for all reflections included in the refinement	0.1126
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
262658 (current)	2021-03-05	cif/ Updating files of 7706467, 7706468, 7706469, 7706470, 7706471, 7706472, 7706473, 7706474 Original log message: Adding full bibliography for 7706467--7706474.cif.	7706474.cif
261133	2021-01-22	cif/ Adding structures of 7706467, 7706468, 7706469, 7706470, 7706471, 7706472, 7706473, 7706474 via cif-deposit CGI script.	7706474.cif