Crystallography Open Database

Information card for entry 7706807

Preview

Coordinates	7706807.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C47 H65 N O Sn
Calculated formula	C47 H65 N O Sn
Title of publication	Low valent lead and tin hydrides in reactions with heteroallenes.
Authors of publication	Weiß, Sebastian; Widemann, Max; Eichele, Klaus; Schubert, Hartmut; Wesemann, Lars
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	14
Pages of publication	4952 - 4958
a	19.0046 ± 0.0014 Å
b	18.4257 ± 0.0012 Å
c	12.0392 ± 0.0008 Å
α	90°
β	99.42 ± 0.005°
γ	90°
Cell volume	4159 ± 0.5 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1157
Residual factor for significantly intense reflections	0.0669
Weighted residual factors for significantly intense reflections	0.1145
Weighted residual factors for all reflections included in the refinement	0.1287
Goodness-of-fit parameter for all reflections included in the refinement	1.258
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
266060 (current)	2021-06-05	cif/ Updating files of 7706807, 7706808, 7706809, 7706810, 7706811, 7706812 Original log message: Adding full bibliography for 7706807--7706812.cif.	7706807.cif
262956	2021-03-10	cif/ Adding structures of 7706807, 7706808, 7706809, 7706810, 7706811, 7706812 via cif-deposit CGI script.	7706807.cif