Crystallography Open Database

Information card for entry 7706899

Preview

Coordinates	7706899.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C122 H188 Cl8 Mn8 N72 O46
Calculated formula	C108 H132 Cl8 Mn8 N72 O32
Title of publication	Preparation of a magnetic metal-organic square and metal-organic cubes using 4,5-bis(2-imidazolinyl)imidazolate: slow magnetization relaxation behavior in mixed-valent octamanganese(ii/iii) clusters.
Authors of publication	Kamebuchi, Hajime; Murakami, Hiroki; Shiga, Ryosuke; Tadokoro, Makoto
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	16
Pages of publication	5452 - 5464
a	17.046 ± 0.003 Å
b	17.684 ± 0.003 Å
c	18.154 ± 0.003 Å
α	68.925 ± 0.002°
β	70.325 ± 0.002°
γ	70.352 ± 0.002°
Cell volume	4661.8 ± 1.4 Å³
Cell temperature	243 ± 2 K
Ambient diffraction temperature	243 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1231
Residual factor for significantly intense reflections	0.0918
Weighted residual factors for significantly intense reflections	0.2982
Weighted residual factors for all reflections included in the refinement	0.3293
Goodness-of-fit parameter for all reflections included in the refinement	1.181
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
266022 (current)	2021-06-05	cif/ Updating files of 7706898, 7706899, 7706900 Original log message: Adding full bibliography for 7706898--7706900.cif.	7706899.cif
263194	2021-03-20	cif/ Adding structures of 7706898, 7706899, 7706900 via cif-deposit CGI script.	7706899.cif