Crystallography Open Database

Information card for entry 7706902

Preview

Coordinates	7706902.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	(N,N'-Ethylene-bis(salicylideneiminato))-nitromethyl-cobalt(iii) nitromethane solvate
Formula	C18 H19 Co N4 O6
Calculated formula	C18 H19 Co N4 O6
Title of publication	Preparation of organocobalt(iii) complexes via O<sub>2</sub> activation.
Authors of publication	Møller, Mads Sondrup; Kongsted, Jacob; McKenzie, Christine J.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	14
Pages of publication	4819 - 4829
a	10.0428 ± 0.0001 Å
b	13.7874 ± 0.0001 Å
c	13.33 ± 0.0001 Å
α	90°
β	97.79 ± 0.001°
γ	90°
Cell volume	1828.69 ± 0.03 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.034
Residual factor for significantly intense reflections	0.033
Weighted residual factors for significantly intense reflections	0.0934
Weighted residual factors for all reflections included in the refinement	0.0943
Goodness-of-fit parameter for all reflections included in the refinement	1.051
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
266066 (current)	2021-06-05	cif/ Updating files of 7706901, 7706902, 7706903, 7706904, 7706905, 7706906, 7706907, 7706908, 7706909 Original log message: Adding full bibliography for 7706901--7706909.cif.	7706902.cif
263195	2021-03-20	cif/ Adding structures of 7706901, 7706902, 7706903, 7706904, 7706905, 7706906, 7706907, 7706908, 7706909 via cif-deposit CGI script.	7706902.cif