Crystallography Open Database

Information card for entry 7707222

Preview

Coordinates	7707222.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	tris(Ethane-1,2-diamine)berylliumazide
Formula	C6 H24 Be N12
Calculated formula	C6 H24 Be N12
Title of publication	Ethylenediamine complexes of the beryllium halides and pseudo-halides.
Authors of publication	Buchner, Magnus R.; Müller, Matthias
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	21
Pages of publication	7246 - 7255
a	10.503 ± 0.0004 Å
b	9.3016 ± 0.0003 Å
c	14.8498 ± 0.0006 Å
α	90°
β	105.734 ± 0.003°
γ	90°
Cell volume	1396.39 ± 0.09 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0355
Residual factor for significantly intense reflections	0.0308
Weighted residual factors for significantly intense reflections	0.0853
Weighted residual factors for all reflections included in the refinement	0.0883
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
266105 (current)	2021-06-05	cif/ Updating files of 7707219, 7707220, 7707221, 7707222, 7707223, 7707224, 7707225 Original log message: Adding full bibliography for 7707219--7707225.cif.	7707222.cif
264610	2021-04-28	cif/ Adding structures of 7707219, 7707220, 7707221, 7707222, 7707223, 7707224, 7707225 via cif-deposit CGI script.	7707222.cif