Crystallography Open Database

Information card for entry 7707350

Preview

Coordinates	7707350.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C62 H65 Br4 Co2 N11 O4
Calculated formula	C62 H65 Br4 Co2 N11 O4
Title of publication	Coordination chemistry of [2 + 2] Schiff-base macrocycles derived from the dianilines [(2-NH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>)<sub>2</sub>X] (X = CH<sub>2</sub>CH<sub>2</sub>, O): structural studies and ROP capability towards cyclic esters.
Authors of publication	Wang, Kuiyuan; Prior, Timothy J.; Hughes, David L.; Arbaoui, Abdessamad; Redshaw, Carl
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	23
Pages of publication	8057 - 8069
a	15.7781 ± 0.0001 Å
b	25.0018 ± 0.0002 Å
c	16.2838 ± 0.0001 Å
α	90°
β	91.911 ± 0.001°
γ	90°
Cell volume	6420.08 ± 0.08 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	9
Hermann-Mauguin space group symbol	I 1 a 1
Hall space group symbol	I -2ya
Residual factor for all reflections	0.0381
Residual factor for significantly intense reflections	0.0315
Weighted residual factors for significantly intense reflections	0.0618
Weighted residual factors for all reflections included in the refinement	0.0637
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
267192 (current)	2021-07-05	cif/ Updating files of 7707347, 7707348, 7707349, 7707350, 7707351, 7707352, 7707353, 7707354, 7707355, 7707356, 7707357, 7707358, 7707359 Original log message: Adding full bibliography for 7707347--7707359.cif.	7707350.cif
265025	2021-05-07	cif/ Adding structures of 7707347, 7707348, 7707349, 7707350, 7707351, 7707352, 7707353, 7707354, 7707355, 7707356, 7707357, 7707358, 7707359 via cif-deposit CGI script.	7707350.cif