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Information card for entry 7707415
Preview
| Coordinates | 7707415.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C53 H83 N O P2 U |
|---|---|
| Calculated formula | C53 H83 N O P2 U |
| Title of publication | Reactivity studies involving a Lewis base supported terminal uranium phosphinidene metallocene [η<sup>5</sup>-1,3-(Me<sub>3</sub>C)<sub>2</sub>C<sub>5</sub>H<sub>3</sub>]<sub>2</sub>U([double bond, length as m-dash]P-2,4,6-<sup>i</sup>Pr<sub>3</sub>C<sub>6</sub>H<sub>2</sub>)(OPMe<sub>3</sub>). |
| Authors of publication | Wang, Deqiang; Wang, Shichun; Li, Tongyu; Heng, Yi; Hou, Guohua; Zi, Guofu; Walter, Marc D. |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2021 |
| Journal volume | 50 |
| Journal issue | 24 |
| Pages of publication | 8349 - 8363 |
| a | 15.5525 ± 0.0002 Å |
| b | 16.8123 ± 0.0002 Å |
| c | 21.0005 ± 0.0002 Å |
| α | 90° |
| β | 106.735 ± 0.001° |
| γ | 90° |
| Cell volume | 5258.51 ± 0.11 Å3 |
| Cell temperature | 100 ± 0.1 K |
| Ambient diffraction temperature | 100 ± 0.1 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0319 |
| Residual factor for significantly intense reflections | 0.0303 |
| Weighted residual factors for significantly intense reflections | 0.0789 |
| Weighted residual factors for all reflections included in the refinement | 0.0803 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.062 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 267146 (current) | 2021-07-05 | cif/ Updating files of 7707402, 7707403, 7707404, 7707405, 7707406, 7707407, 7707408, 7707409, 7707410, 7707411, 7707412, 7707413, 7707414, 7707415, 7707416 Original log message: Adding full bibliography for 7707402--7707416.cif. |
7707415.cif |
| 265324 | 2021-05-19 | cif/ Adding structures of 7707402, 7707403, 7707404, 7707405, 7707406, 7707407, 7707408, 7707409, 7707410, 7707411, 7707412, 7707413, 7707414, 7707415, 7707416 via cif-deposit CGI script. |
7707415.cif |
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Users of the data should acknowledge the original authors of the
structural data.