#------------------------------------------------------------------------------ #$Date: 2021-06-11 05:01:55 +0300 (Fri, 11 Jun 2021) $ #$Revision: 266382 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/76/7707649.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7707649 loop_ _publ_author_name 'Zhao, Xin-Hua' 'Shao, Dong' 'Chen, Jia-Tao' 'Liu, Min' 'Li, Tao' 'Yang, Jiong' 'Zhang, Yuan-Zhu' _publ_section_title ; Spin and Valence Isomerism in Cyanide-Bridged {FeIII2MII} (M = Fe, Co) Clusters ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT01298C _journal_year 2021 _chemical_formula_moiety 'C63 H73 B2 Fe3 N23, C H4 O, 3(H2 O)' _chemical_formula_sum 'C64 H83 B2 Fe3 N23 O4' _chemical_formula_weight 1427.70 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2020-04-08 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-05-13 deposited with the CCDC. 2021-06-07 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 113.207(5) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 23.462(4) _cell_length_b 22.513(4) _cell_length_c 16.255(3) _cell_measurement_reflns_used 9950 _cell_measurement_temperature 290(2) _cell_measurement_theta_max 26.337 _cell_measurement_theta_min 2.597 _cell_volume 7891(2) _computing_cell_refinement 'SAINT V8.38A (?, 2016)' _computing_data_collection 'Bruker APEX3' _computing_data_reduction 'SAINT V8.38A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'XT (Sheldrick, 2015)' _diffrn_ambient_temperature 290.0 _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0514 _diffrn_reflns_av_unetI/netI 0.0626 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_h_min -29 _diffrn_reflns_limit_k_max 28 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 28350 _diffrn_reflns_point_group_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.371 _diffrn_reflns_theta_min 2.583 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.601 _exptl_absorpt_correction_T_max 0.7454 _exptl_absorpt_correction_T_min 0.6092 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0955 before and 0.0576 after correction. The Ratio of minimum to maximum transmission is 0.8173. The \l/2 correction factor is Not present.' _exptl_crystal_colour 'dark red' _exptl_crystal_colour_modifier dark _exptl_crystal_colour_primary red _exptl_crystal_density_diffrn 1.202 _exptl_crystal_description block _exptl_crystal_F_000 2992 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.532 _refine_diff_density_min -0.608 _refine_diff_density_rms 0.083 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.032 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 454 _refine_ls_number_reflns 8036 _refine_ls_number_restraints 39 _refine_ls_restrained_S_all 1.036 _refine_ls_R_factor_all 0.1238 _refine_ls_R_factor_gt 0.0681 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1431P)^2^+7.5563P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1986 _refine_ls_wR_factor_ref 0.2491 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4643 _reflns_number_total 8036 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt01298c3.cif _cod_data_source_block Fe2Fe-290K _cod_database_code 7707649 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.931 _shelx_estimated_absorpt_t_min 0.889 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All B(H) groups, All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups, All O(H,H) groups 2. Shared sites {C12A, N12} 3. Restrained distances O1-C32 1.45 with sigma of 0.01 O2_$1-H3A_$1 1.6 with sigma of 0.01 4. Rigid bond restraints O1, C32 with sigma for 1-2 distances of 0.02 and sigma for 1-3 distances of 0.02 5. Uiso/Uaniso restraints and constraints O1 \\sim C32: within 2A with sigma of 0.02 and sigma for terminal atoms of 0.04 Uanis(O3) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C32) \\sim Ueq, Uanis(O1) \\sim Ueq, Uanis(O4) \\sim Ueq, Uanis(O2) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C12A) = Uanis(N12) Uanis(O2) = Uanis(O2A) 6. Others Sof(O2A)=Sof(H2AA)=Sof(H2AB)=0.5*(1-FVAR(2)) Sof(O2)=Sof(H2A)=Sof(H2B)=0.5*FVAR(2) Fixed Sof: N12(0.5) H13A(0.5) H13(0.5) C12A(0.5) H12A(0.5) O1(0.5) H1B(0.5) C32(0.5) H32A(0.5) H32B(0.5) H32C(0.5) O3(0.5) H3A(0.5) H3B(0.5) O4(0.5) H4A(0.5) H4B(0.5) 7.a Riding coordinates: O1(H1B), C32(H32A,H32B,H32C), O2(H2A,H2B), O3(H3A,H3B), O4(H4A,H4B), O2A(H2AA, H2AB) 7.b Ternary CH refined with riding coordinates: B1(H1A) 7.c Secondary CH2 refined with riding coordinates: C6(H6A,H6B), C7(H7A,H7B), C8(H8A,H8B) 7.d Aromatic/amide H refined with riding coordinates: C10(H10), C11(H11), C12(H12), C13(H13A), C13(H13), C1(H1), C2(H2), C3(H3), C4(H4), C12A(H12A), C18(H18), C23(H23), C28(H28) 7.e Fitted hexagon refined as free rotating group: N12(C9,C10,C11,C12,C13) 7.f Idealised Me refined as rotating group: C20(H20A,H20B,H20C), C21(H21A,H21B,H21C), C25(H25A,H25B,H25C), C26(H26A,H26B, H26C), C30(H30A,H30B,H30C), C31(H31A,H31B,H31C) ; _shelx_res_file ; a.res created by SHELXL-2014/7 TITL a_a.res in C2/c REM Old TITL a in C2/c REM SHELXT solution in C2/c REM R1 0.213, Rweak 0.002, Alpha 0.059, Orientation as input REM Formula found by SHELXT: C66 N16 O6 Fe3 CELL 0.71073 23.4617 22.5134 16.2548 90 113.207 90 ZERR 4 0.004 0.0035 0.0029 0 0.005 0 LATT 7 SYMM -X,+Y,0.5-Z SFAC C H B Fe N O UNIT 256 332 8 12 92 16 EQIV $1 1-X,-Y,1-Z DFIX 1.45 0.01 O1 C32 DFIX 1.6 0.01 O2_$1 H3a_$1 DELU 0.02 0.02 O1 C32 SIMU 0.02 0.04 2 O1 C32 ISOR 0.01 0.02 O3 ISOR 0.01 0.02 C32 O1 O4 O2 EADP C12A N12 EADP O2 O2A EXYZ C12A N12 L.S. 20 PLAN 20 SIZE 0.12 0.15 0.2 TEMP 16.85 BOND $H list 4 fmap 2 acta REM REM REM WGHT 0.143100 7.556300 FVAR 0.23869 0.48447 FE1 4 0.500000 0.173723 0.250000 10.50000 0.03193 0.03743 = 0.04700 0.00000 0.00236 0.00000 FE2 4 0.581950 0.327778 0.498677 11.00000 0.03637 0.04653 = 0.05873 -0.00807 0.01011 0.00161 N1 5 0.586957 0.167103 0.234979 11.00000 0.04685 0.04601 = 0.04681 -0.00096 0.00952 0.00149 N2 5 0.548217 0.099195 0.339841 11.00000 0.03871 0.05243 = 0.06033 0.00769 0.00644 -0.00050 N3 5 0.535792 0.236510 0.349250 11.00000 0.03746 0.04813 = 0.06188 -0.01008 0.00276 0.00085 N4 5 0.658623 0.222467 0.601933 11.00000 0.07362 0.07485 = 0.09821 0.01698 0.03139 0.01750 N5 5 0.466461 0.283629 0.524503 11.00000 0.07000 0.11491 = 0.12224 -0.02408 0.05054 -0.02674 N6 5 0.653504 0.357290 0.472660 11.00000 0.03592 0.04654 = 0.05279 -0.00480 0.00736 0.00253 N7 5 0.669391 0.416052 0.490367 11.00000 0.03867 0.04485 = 0.05838 -0.00719 0.01040 0.00281 N8 5 0.535632 0.397437 0.430893 11.00000 0.04007 0.05036 = 0.06327 -0.01195 0.00928 0.00415 N9 5 0.563086 0.451801 0.455051 11.00000 0.04108 0.04582 = 0.06322 -0.00556 0.01405 0.00659 N10 5 0.609936 0.374550 0.612834 11.00000 0.04964 0.05817 = 0.05935 -0.00661 0.01619 -0.00049 N11 5 0.634035 0.430319 0.612613 11.00000 0.04414 0.05060 = 0.06319 -0.01205 0.01035 0.00099 PART 4 AFIX 66 N12 5 0.568125 -0.007463 0.476709 10.50000 0.09799 0.09739 = 0.11309 0.04385 0.04408 0.01583 PART 0 C9 1 0.567324 0.053392 0.490643 11.00000 0.05512 0.08566 = 0.09100 0.02962 0.02770 -0.00219 C10 1 0.602069 0.077242 0.574410 11.00000 0.09057 0.10875 = 0.09572 0.04461 -0.01065 -0.01424 AFIX 43 H10 2 0.601533 0.117959 0.583732 11.00000 -1.20000 AFIX 65 C11 1 0.637617 0.040237 0.644245 11.00000 0.10245 0.15911 = 0.11530 0.05480 -0.01243 -0.01260 AFIX 43 H11 2 0.660864 0.056195 0.700291 11.00000 -1.20000 AFIX 65 C12 1 0.638419 -0.020618 0.630313 11.00000 0.08250 0.14833 = 0.14438 0.08606 0.03866 0.00594 AFIX 43 H12 2 0.662202 -0.045377 0.677037 11.00000 -1.20000 AFIX 65 C13 1 0.603673 -0.044469 0.546546 11.00000 0.10468 0.11897 = 0.16782 0.07419 0.06474 0.02776 PART 4 AFIX 43 H13A 2 0.604210 -0.085186 0.537225 10.50000 -1.20000 AFIX 43 PART 0 PART 3 H13 2 0.604210 -0.085186 0.537225 10.50000 -1.20000 AFIX 0 PART 0 C1 1 0.601456 0.192307 0.172761 11.00000 0.05756 0.05143 = 0.05996 0.00090 0.01613 0.00361 AFIX 43 H1 2 0.569956 0.210297 0.124738 11.00000 -1.20000 AFIX 0 C2 1 0.660716 0.193524 0.174815 11.00000 0.07024 0.07627 = 0.07395 -0.00039 0.03452 -0.00077 AFIX 43 H2 2 0.668872 0.212189 0.129573 11.00000 -1.20000 AFIX 0 C3 1 0.707468 0.166647 0.244943 11.00000 0.05198 0.07581 = 0.07739 -0.00330 0.02483 0.00594 AFIX 43 H3 2 0.748068 0.167176 0.248747 11.00000 -1.20000 AFIX 0 C4 1 0.692724 0.138705 0.309948 11.00000 0.04398 0.06185 = 0.06502 -0.00855 0.00946 0.01150 AFIX 43 H4 2 0.723297 0.119314 0.357456 11.00000 -1.20000 AFIX 0 C5 1 0.632402 0.139860 0.303677 11.00000 0.03992 0.04726 = 0.05325 -0.00268 0.00472 0.00317 C6 1 0.614875 0.113681 0.373929 11.00000 0.03796 0.06060 = 0.05712 0.00574 0.00235 0.00511 AFIX 23 H6A 2 0.638863 0.077827 0.396648 11.00000 -1.20000 H6B 2 0.624903 0.141508 0.423207 11.00000 -1.20000 AFIX 0 C7 1 0.533844 0.046497 0.281693 11.00000 0.05855 0.04106 = 0.07867 0.00266 0.00349 0.00306 AFIX 23 H7A 2 0.542916 0.010870 0.318179 11.00000 -1.20000 H7B 2 0.559669 0.046319 0.247519 11.00000 -1.20000 AFIX 0 C8 1 0.528489 0.092807 0.415465 11.00000 0.05182 0.07359 = 0.07174 0.02283 0.01049 0.00166 AFIX 23 H8A 2 0.486358 0.077712 0.392041 11.00000 -1.20000 H8B 2 0.527659 0.132016 0.439705 11.00000 -1.20000 AFIX 0 PART 3 C12A 1 0.568125 -0.007463 0.476709 10.50000 0.09799 0.09739 = 0.11309 0.04385 0.04408 0.01583 AFIX 43 H12A 2 0.544878 -0.023421 0.420663 10.50000 -1.20000 AFIX 0 PART 0 C14 1 0.553922 0.273247 0.401891 11.00000 0.03124 0.05026 = 0.06179 0.00102 0.01000 0.00479 C15 1 0.630022 0.261063 0.564138 11.00000 0.04607 0.05611 = 0.06901 -0.00372 0.01571 0.00263 C16 1 0.510607 0.299719 0.517593 11.00000 0.06102 0.06377 = 0.07144 -0.01428 0.02275 0.00046 C17 1 0.691844 0.334689 0.436771 11.00000 0.03573 0.05559 = 0.04815 -0.00507 0.00668 0.00369 C18 1 0.731697 0.378711 0.433548 11.00000 0.04060 0.06941 = 0.05674 0.00096 0.01532 0.00230 AFIX 43 H18 2 0.763110 0.374664 0.412616 11.00000 -1.20000 AFIX 0 C19 1 0.716621 0.429559 0.466806 11.00000 0.04006 0.05246 = 0.04923 0.00333 0.00888 0.00311 C20 1 0.688097 0.272355 0.404621 11.00000 0.04286 0.06030 = 0.06985 -0.01737 0.01341 0.00609 AFIX 137 H20A 2 0.682580 0.246062 0.447398 11.00000 -1.50000 H20B 2 0.725714 0.262334 0.397641 11.00000 -1.50000 H20C 2 0.653581 0.268453 0.348081 11.00000 -1.50000 AFIX 0 C21 1 0.745053 0.489134 0.480509 11.00000 0.06104 0.06109 = 0.07409 0.00533 0.02557 -0.00412 AFIX 137 H21A 2 0.714328 0.517884 0.447503 11.00000 -1.50000 H21B 2 0.778176 0.489414 0.459889 11.00000 -1.50000 H21C 2 0.761154 0.498872 0.543051 11.00000 -1.50000 AFIX 0 C22 1 0.481586 0.406628 0.360542 11.00000 0.03616 0.06491 = 0.06218 -0.00706 0.00451 0.01213 C23 1 0.474803 0.465934 0.341584 11.00000 0.04641 0.07081 = 0.07036 0.00079 0.00999 0.02001 AFIX 43 H23 2 0.441339 0.483975 0.296505 11.00000 -1.20000 AFIX 0 C24 1 0.526591 0.494097 0.401450 11.00000 0.05111 0.05791 = 0.07037 0.00491 0.02529 0.01695 C25 1 0.436924 0.357866 0.312809 11.00000 0.04091 0.08575 = 0.09873 -0.02574 -0.01078 0.01048 AFIX 137 H25A 2 0.458099 0.328165 0.293124 11.00000 -1.50000 H25B 2 0.403457 0.374096 0.261968 11.00000 -1.50000 H25C 2 0.420724 0.340228 0.352884 11.00000 -1.50000 AFIX 0 C26 1 0.542721 0.558212 0.411299 11.00000 0.07751 0.05956 = 0.09820 0.01485 0.03109 0.01505 AFIX 137 H26A 2 0.550871 0.570648 0.471382 11.00000 -1.50000 H26B 2 0.508754 0.580792 0.370082 11.00000 -1.50000 H26C 2 0.578967 0.564649 0.398800 11.00000 -1.50000 AFIX 0 C27 1 0.617592 0.363333 0.697495 11.00000 0.06030 0.07375 = 0.06568 -0.00101 0.02032 0.01199 C28 1 0.647264 0.411330 0.751294 11.00000 0.06106 0.08433 = 0.05894 -0.01439 0.01600 0.00903 AFIX 43 H28 2 0.658190 0.414940 0.812629 11.00000 -1.20000 AFIX 0 C29 1 0.657101 0.451936 0.696222 11.00000 0.04603 0.07425 = 0.06069 -0.02614 0.00942 0.00331 C30 1 0.596176 0.308369 0.729136 11.00000 0.11837 0.08935 = 0.08361 0.00506 0.03913 -0.00063 AFIX 137 H30A 2 0.551856 0.305398 0.700137 11.00000 -1.50000 H30B 2 0.608170 0.310453 0.792760 11.00000 -1.50000 H30C 2 0.614802 0.274094 0.714752 11.00000 -1.50000 AFIX 0 C31 1 0.687110 0.512246 0.716500 11.00000 0.06922 0.08151 = 0.08505 -0.03493 0.00987 -0.01234 AFIX 137 H31A 2 0.656590 0.542240 0.688052 11.00000 -1.50000 H31B 2 0.719412 0.514381 0.694338 11.00000 -1.50000 H31C 2 0.704470 0.518587 0.780044 11.00000 -1.50000 AFIX 0 B1 3 0.629975 0.455268 0.524747 11.00000 0.04183 0.04686 = 0.06706 -0.01055 0.01514 0.00420 AFIX 13 1.1900 H1A 2 0.648089 0.505189 0.533722 11.00000 -1.20000 AFIX 0 O1 6 0.707086 0.158310 0.772312 10.50000 0.25483 0.20476 = 0.16656 0.04738 0.07404 -0.00428 AFIX 3 H1B 2 0.690936 0.175690 0.724332 10.50000 -1.50000 AFIX 0 C32 1 0.772391 0.162094 0.802142 10.50000 0.23678 0.17772 = 0.23678 0.00157 0.06137 -0.00531 AFIX 3 H32A 2 0.788881 0.181744 0.859202 10.50000 -1.50000 H32B 2 0.782811 0.184424 0.759702 10.50000 -1.50000 H32C 2 0.789791 0.122954 0.808022 10.50000 -1.50000 AFIX 0 PART 1 O2 6 0.332132 0.328329 0.502365 20.50000 0.14887 0.21387 = 0.17280 -0.01532 0.06223 -0.06011 AFIX 3 H2A 2 0.350582 0.335139 0.558105 20.50000 -1.50000 H2B 2 0.352302 0.299799 0.492455 20.50000 -1.50000 AFIX 0 PART 0 O3 6 0.250045 0.327914 0.533431 10.50000 0.39040 0.41167 = 0.35940 0.01770 0.15285 -0.02348 AFIX 3 H3A 2 0.278205 0.303734 0.528891 10.50000 -1.50000 H3B 2 0.228525 0.344284 0.480201 10.50000 -1.50000 AFIX 0 O4 6 0.423747 0.174749 0.596185 10.50000 0.40245 0.29734 = 0.35681 -0.03556 0.15440 -0.10349 AFIX 3 H4A 2 0.417257 0.212589 0.580785 10.50000 -1.50000 H4B 2 0.463417 0.166379 0.613285 10.50000 -1.50000 AFIX 0 PART 2 O2A 6 0.346598 0.268081 0.528084 -20.50000 0.14887 0.21387 = 0.17280 -0.01532 0.06223 -0.06011 AFIX 3 H2AA 2 0.342278 0.261681 0.576844 -20.50000 -1.50000 H2AB 2 0.383028 0.255991 0.537954 -20.50000 -1.50000 AFIX 0 HKLF 4 REM a_a.res in C2/c REM R1 = 0.0681 for 4643 Fo > 4sig(Fo) and 0.1238 for all 8036 data REM 454 parameters refined using 39 restraints END WGHT 0.1431 7.5558 REM Highest difference peak 0.532, deepest hole -0.608, 1-sigma level 0.083 Q1 1 0.5000 0.4831 0.2500 10.50000 0.05 0.53 Q2 1 0.7284 0.1976 0.8003 11.00000 0.05 0.52 Q3 1 0.5810 0.0218 0.5018 11.00000 0.05 0.48 Q4 1 0.4890 0.1533 0.6219 11.00000 0.05 0.48 Q5 1 0.3722 0.2116 0.5588 11.00000 0.05 0.44 Q6 1 0.2939 0.3596 0.5227 11.00000 0.05 0.43 Q7 1 0.3646 0.0937 0.6442 11.00000 0.05 0.42 Q8 1 0.5000 0.1109 0.7500 10.50000 0.05 0.42 Q9 1 0.7493 0.1176 0.8620 11.00000 0.05 0.41 Q10 1 0.8150 0.1635 0.9246 11.00000 0.05 0.37 Q11 1 0.7518 0.1711 0.8047 11.00000 0.05 0.37 Q12 1 0.6599 0.1728 0.7457 11.00000 0.05 0.37 Q13 1 0.2989 0.3247 0.4992 11.00000 0.05 0.36 Q14 1 0.4741 0.1721 0.6544 11.00000 0.05 0.35 Q15 1 0.6619 0.4799 0.7412 11.00000 0.05 0.35 Q16 1 0.4815 0.1139 0.6682 11.00000 0.05 0.35 Q17 1 0.2335 0.3590 0.5395 11.00000 0.05 0.31 Q18 1 0.1504 0.3415 0.3810 11.00000 0.05 0.31 Q19 1 0.4105 0.1191 0.6815 11.00000 0.05 0.30 Q20 1 0.5181 0.1341 0.7184 11.00000 0.05 0.30 ; _shelx_res_checksum 73073 _shelx_hkl_file ; 4 0 0 1775.72 75.49 4 0 0 1931.81 75.29 -4 0 0 1883.91 75.19 -4 0 0 1817.42 75.59 -6 0 0 62.29 6.20 6 0 0 88.79 6.70 6 0 0 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4 4 123.49 12.20 8 -4 4 67.89 8.60 8 -4 4 54.39 6.40 -8 -4 -4 59.49 8.70 -8 4 -4 48.50 7.30 8 4 4 47.80 9.30 -8 4 -4 62.99 7.10 -8 4 -4 56.09 7.30 -10 -4 -4 102.69 8.50 10 -4 4 115.49 11.20 -10 -4 -4 95.99 11.30 10 -4 4 107.29 8.70 -10 4 -4 102.29 9.40 10 4 4 98.49 13.30 -10 4 -4 112.09 11.00 -10 4 -4 96.19 9.90 10 4 4 109.99 9.70 12 -4 4 103.29 11.60 -12 -4 -4 91.89 9.50 12 -4 4 114.49 9.30 -12 -4 -4 110.49 12.60 12 4 4 123.59 15.50 -12 4 -4 100.79 9.80 -12 4 -4 111.99 11.10 12 4 4 110.49 11.10 -12 4 -4 100.19 11.80 14 -4 4 373.66 22.60 -14 -4 -4 298.87 18.70 -14 4 -4 342.37 21.50 14 4 4 312.87 20.00 14 4 4 337.97 24.40 -14 4 -4 319.67 22.80 16 -4 4 83.19 13.00 -16 -4 -4 76.59 9.20 -16 4 -4 82.79 10.20 -16 4 -4 88.49 13.00 16 4 4 64.19 13.40 -16 4 -4 62.29 11.10 -18 -4 -4 37.10 4.90 18 -4 4 24.20 9.00 -18 -4 -4 31.50 7.20 -18 4 -4 37.80 8.00 18 4 4 32.30 11.40 20 -4 4 7.70 8.10 -20 4 -4 6.20 5.50 20 4 4 12.00 9.70 22 -4 4 7.90 9.30 22 4 4 -7.60 9.00 -22 4 -4 -2.80 4.80 -27 5 4 3.00 8.00 27 5 -4 1.90 10.50 25 -5 -4 26.90 12.40 -25 5 4 9.30 8.70 25 5 -4 21.00 11.40 -23 -5 4 -5.20 5.80 -23 5 4 -1.80 7.40 23 5 -4 15.10 12.30 -21 -5 4 5.70 5.90 21 -5 -4 -7.30 7.80 21 5 -4 -9.60 9.10 -21 5 4 -7.20 6.70 19 -5 -4 197.38 20.90 -19 -5 4 216.58 14.80 -19 5 4 202.78 17.80 -19 5 4 198.68 19.40 19 5 -4 248.68 22.30 -17 -5 4 547.35 28.60 17 -5 -4 503.35 31.30 -17 -5 4 520.15 26.00 -17 -5 4 558.54 42.30 17 5 -4 534.75 31.00 15 -5 -4 2.10 6.50 -15 -5 4 11.40 6.60 -15 -5 4 12.10 4.90 15 5 -4 6.60 7.70 -15 5 4 10.10 6.50 -15 5 4 6.50 7.00 -13 -5 4 -1.80 3.80 13 -5 -4 -2.00 5.50 -13 -5 4 -1.20 5.10 -13 5 4 -5.50 4.90 -13 5 4 2.80 4.90 13 5 -4 4.30 6.60 -11 -5 4 2.70 4.40 -11 -5 4 6.20 4.00 11 -5 -4 11.90 5.80 -11 5 4 6.90 5.60 11 5 -4 2.90 5.70 -9 -5 4 3.40 4.30 -9 -5 4 -0.40 3.10 9 -5 -4 -2.40 4.20 9 5 -4 -1.40 3.20 9 5 -4 -6.90 4.30 -9 5 4 0.00 4.40 -7 -5 4 368.76 21.10 -7 -5 4 432.36 20.60 7 -5 -4 487.85 22.70 7 5 -4 443.16 21.40 -7 5 4 445.86 22.10 7 5 -4 461.45 20.50 5 -5 -4 1354.86 57.29 -5 -5 4 1376.46 56.79 5 5 -4 1337.07 56.49 -5 5 4 1362.36 57.09 -3 -5 4 72.39 7.00 3 5 -4 83.79 6.50 -3 5 4 71.29 6.20 -1 -5 4 784.92 33.90 1 5 -4 759.52 33.60 1 -5 4 8.60 3.20 1 5 4 4.70 4.00 -1 5 -4 3.00 2.80 3 -5 4 547.75 25.20 3 -5 4 595.74 26.40 3 5 4 531.65 27.80 -3 5 -4 608.34 26.60 5 -5 4 730.93 33.70 5 -5 4 725.63 33.50 -5 -5 -4 777.92 35.90 -5 5 -4 767.12 34.10 5 5 4 784.12 36.70 7 -5 4 2.40 4.00 -7 -5 -4 4.20 4.50 7 -5 4 0.50 3.00 -7 5 -4 2.30 3.70 7 5 4 2.70 5.80 -9 -5 -4 13.90 5.70 9 -5 4 8.40 4.10 9 -5 4 16.80 5.80 -9 5 -4 9.70 4.80 9 5 4 12.60 7.00 -9 5 -4 11.00 4.50 -9 5 -4 7.70 4.70 -11 -5 -4 42.90 5.50 11 -5 4 46.70 6.60 11 -5 4 43.20 8.10 -11 -5 -4 38.90 8.50 11 5 4 20.20 8.80 -11 5 -4 40.60 7.50 -11 5 -4 36.40 7.40 11 5 4 51.09 7.20 -11 5 -4 43.00 6.90 13 -5 4 64.09 10.40 -13 -5 -4 55.09 6.80 -13 5 -4 40.10 8.90 -13 5 -4 60.49 9.20 13 5 4 61.19 12.30 13 5 4 55.39 7.90 -13 5 -4 66.49 9.00 15 -5 4 20.60 8.10 -15 -5 -4 7.30 5.40 -15 5 -4 20.50 7.10 15 5 4 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34.90 12.40 24 8 -4 35.10 18.90 -22 -8 4 24.70 7.20 -22 8 4 39.10 10.20 22 8 -4 33.40 12.50 -20 -8 4 22.00 6.60 -20 8 4 12.00 7.80 -20 8 4 20.20 9.10 20 8 -4 32.40 11.40 -18 -8 4 48.00 7.30 -18 8 4 38.00 10.00 18 8 -4 60.79 12.00 -18 8 4 42.00 9.20 -16 -8 4 17.50 5.50 -16 8 4 9.30 6.70 16 8 -4 0.10 7.50 16 8 -4 20.20 9.00 -16 8 4 2.10 6.70 -14 -8 4 138.69 15.10 -14 -8 4 200.58 12.80 -14 8 4 177.08 14.80 -14 8 4 159.58 14.60 -14 8 4 225.98 17.10 14 8 -4 175.68 16.00 14 8 -4 207.18 16.80 -12 -8 4 414.76 21.30 -12 -8 4 391.26 24.20 -12 8 4 414.26 23.10 12 8 -4 490.75 27.40 -12 8 4 429.26 24.90 -10 -8 4 1338.77 57.49 -10 -8 4 1402.86 60.59 -10 8 4 1262.47 59.69 -10 8 4 1418.96 59.09 10 8 -4 1335.57 56.89 10 8 -4 1344.97 58.79 -8 -8 4 17.10 4.50 -8 -8 4 17.00 5.30 -8 8 4 16.10 5.50 -8 8 4 15.80 4.60 8 8 -4 14.40 4.50 -6 -8 4 180.38 11.90 -6 -8 4 193.88 11.80 -6 8 4 189.18 12.80 -6 8 4 188.18 11.90 6 8 -4 181.48 11.50 -4 -8 4 49.90 6.00 -4 -8 4 32.20 4.70 -4 8 4 34.80 4.90 -2 -8 4 599.34 26.30 -2 -8 4 619.44 28.10 -2 8 4 597.64 26.90 2 8 -4 586.84 27.90 0 -8 4 3987.50 165.48 0 8 4 4060.99 166.18 0 8 -4 4124.09 165.58 0 8 4 4130.09 163.68 2 -8 4 2542.05 105.29 2 8 4 2523.75 106.69 -2 8 -4 2547.95 105.49 2 8 4 2575.94 102.59 4 -8 4 0.20 2.70 4 -8 4 2.40 3.50 4 8 4 7.40 5.80 -4 8 -4 6.10 4.00 6 -8 4 184.58 13.00 6 -8 4 192.88 11.20 -6 -8 -4 190.68 14.50 -6 8 -4 201.28 13.60 6 8 4 204.18 16.00 -8 -8 -4 3.10 6.60 8 -8 4 13.40 4.30 8 -8 4 8.60 3.90 8 8 4 8.30 6.60 -10 -8 -4 236.98 18.00 10 -8 4 219.28 14.70 10 -8 4 253.67 14.50 10 8 4 243.98 19.70 -10 8 -4 219.38 16.10 12 -8 4 216.58 14.70 12 -8 4 221.28 14.70 12 8 4 219.38 19.50 -12 8 -4 222.48 17.30 -12 8 -4 219.58 16.10 -12 8 -4 213.28 14.50 14 -8 4 57.09 8.60 14 8 4 41.50 11.20 -14 8 -4 41.70 7.60 14 8 4 42.80 8.40 -14 8 -4 40.80 8.40 16 -8 4 2.10 5.60 16 8 4 2.40 5.60 16 8 4 -11.10 7.60 -16 8 -4 -3.20 5.40 18 -8 4 -0.30 6.60 -18 8 -4 8.00 6.70 -18 8 -4 -2.30 5.40 18 8 4 -1.60 9.30 18 8 4 4.60 6.60 20 -8 4 -2.60 7.20 20 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144.79 15.10 9 -11 4 169.98 13.30 9 11 4 182.58 17.90 -9 11 -4 159.38 14.70 11 11 4 67.79 12.50 -11 11 -4 74.69 10.80 13 11 4 4.30 6.40 13 11 4 5.30 9.20 -13 11 -4 1.80 6.40 -15 11 -4 59.19 10.70 15 11 4 49.90 14.00 15 11 4 70.29 10.80 17 11 4 15.80 11.70 -17 11 -4 19.20 8.20 17 11 4 20.60 8.40 19 11 4 70.89 10.80 19 11 4 51.69 14.10 -21 11 -4 21.60 8.40 21 11 4 25.00 11.90 21 11 4 22.50 8.60 26 12 -4 19.00 12.70 -26 12 4 30.10 10.20 -24 -12 4 90.39 10.50 24 12 -4 116.79 18.50 -24 12 4 78.39 13.10 -22 -12 4 30.70 7.80 22 12 -4 43.60 15.60 -22 12 4 26.20 9.70 -20 -12 4 38.00 9.90 20 12 -4 29.30 12.40 -20 12 4 42.30 10.50 -20 12 4 30.50 10.30 -18 -12 4 1.30 5.50 -18 12 4 13.80 7.70 18 12 -4 6.20 9.60 18 12 -4 -3.50 9.30 -18 12 4 7.40 8.30 -16 -12 4 35.10 7.10 16 12 -4 30.40 10.10 -16 12 4 30.50 8.30 16 12 -4 39.60 10.40 -16 12 4 37.60 9.20 -14 -12 4 218.98 18.30 -14 -12 4 208.88 14.70 -14 12 4 213.08 17.90 14 12 -4 224.98 19.10 14 12 -4 208.98 18.60 -14 12 4 205.88 16.00 -12 -12 4 456.65 27.60 -12 -12 4 462.95 23.60 -12 12 4 442.26 25.80 12 12 -4 439.36 26.10 -12 12 4 451.95 27.10 12 12 -4 443.46 23.00 12 12 -4 458.85 26.20 -10 -12 4 427.36 25.50 -10 -12 4 449.06 23.30 -10 12 4 456.35 25.20 10 12 -4 476.15 26.70 10 12 -4 442.56 22.90 -8 -12 4 2.40 5.20 -8 -12 4 -3.20 3.80 -8 12 4 0.60 5.10 8 12 -4 -3.30 4.40 -8 12 4 -4.30 4.50 -6 -12 4 490.75 25.00 -6 -12 4 461.25 24.80 6 12 -4 515.15 25.10 -6 12 4 492.45 25.30 -6 12 4 503.55 26.40 -4 -12 4 16.20 5.10 -4 12 4 21.60 5.10 4 12 -4 25.40 6.20 -2 -12 4 9.10 3.50 -2 -12 4 6.60 4.40 -2 12 4 2.60 4.00 2 12 -4 2.80 4.70 -2 12 4 8.20 5.00 0 -12 4 1647.64 71.59 0 12 4 1737.73 72.59 0 12 4 1613.34 69.59 2 -12 4 1.90 4.00 2 12 4 2.60 3.50 2 12 4 3.60 5.50 -2 12 -4 4.40 4.60 4 -12 4 215.38 17.40 -4 12 -4 246.58 16.40 4 12 4 222.38 12.00 6 -12 4 86.39 10.20 6 12 4 91.69 13.40 -6 12 -4 98.69 11.60 -8 -12 -4 19.10 7.60 8 -12 4 43.60 7.70 8 12 4 46.80 11.30 -8 12 -4 36.60 8.20 -10 12 -4 345.57 22.10 10 12 4 322.87 25.00 -12 12 -4 1045.10 51.59 12 12 4 1129.79 56.69 14 12 4 116.99 14.00 -14 12 -4 122.59 14.80 14 12 4 95.79 15.50 16 12 4 25.30 12.90 -16 12 -4 24.40 8.80 18 12 4 -3.60 10.00 18 12 4 5.50 7.30 20 12 4 13.70 7.50 -20 12 -4 -1.30 6.30 20 12 4 5.00 9.90 -25 13 4 7.50 9.70 25 13 -4 0.30 12.00 -23 -13 4 5.00 7.30 -23 13 4 2.10 8.50 23 13 -4 1.50 12.00 -21 -13 4 29.30 10.40 -21 13 4 29.00 9.30 -21 13 4 17.80 9.00 21 13 -4 22.20 13.10 -19 -13 4 -2.10 6.10 19 13 -4 -9.80 10.00 -19 13 4 -8.90 7.10 19 13 -4 -8.60 9.50 -19 13 4 -7.10 11.50 -17 -13 4 7.80 5.70 17 13 -4 5.00 8.10 17 13 -4 2.50 9.90 -17 13 4 4.40 6.50 -17 13 4 5.90 8.20 -15 -13 4 103.39 11.10 -15 13 4 95.29 13.00 15 13 -4 98.39 13.40 -15 13 4 98.09 11.90 15 13 -4 119.29 15.00 -13 -13 4 -4.90 4.80 -13 -13 4 -6.40 6.10 13 13 -4 -2.80 7.50 -13 13 4 -6.10 6.50 13 13 -4 -10.60 5.90 13 13 -4 4.30 7.80 -11 -13 4 -3.30 4.60 -11 -13 4 -8.10 5.20 11 13 -4 -6.70 5.40 -11 13 4 2.60 5.70 11 13 -4 -1.30 6.50 -11 13 4 -4.60 6.10 -9 -13 4 -2.70 5.20 -9 -13 4 0.50 4.50 -9 13 4 -2.50 5.60 9 13 -4 -3.30 5.40 -7 -13 4 7.50 4.70 -7 -13 4 -5.00 4.70 -7 13 4 -4.90 5.10 7 13 -4 12.30 5.60 -7 13 4 -3.90 4.70 -5 -13 4 240.38 15.10 -5 -13 4 212.38 14.50 -5 13 4 247.78 15.40 5 13 -4 228.68 15.30 -3 -13 4 -1.20 4.10 -3 -13 4 0.50 3.70 -3 13 4 -4.20 4.30 -3 13 4 0.50 4.40 -1 -13 4 194.58 10.30 -1 -13 4 175.28 13.40 -1 13 4 177.28 12.10 -1 13 4 180.28 13.90 1 13 -4 182.78 13.90 1 -13 4 25.10 6.50 1 13 4 21.40 6.90 1 13 4 24.60 4.80 -1 13 -4 31.90 7.00 3 -13 4 2.00 4.10 3 13 4 -3.80 3.30 3 13 4 -1.80 8.50 -3 13 -4 8.20 5.10 5 -13 4 15.70 5.40 -5 13 -4 14.50 6.40 5 13 4 16.90 3.80 5 13 4 3.90 7.10 7 -13 4 28.60 7.10 -7 13 -4 29.20 7.60 7 13 4 30.00 9.50 -9 13 -4 109.69 13.10 9 13 4 155.78 17.80 9 13 4 115.39 11.30 11 13 4 8.80 9.70 -11 13 -4 19.70 7.20 -13 13 -4 8.60 6.70 13 13 4 5.00 9.60 -15 13 -4 101.29 13.80 15 13 4 71.99 19.00 15 13 4 108.69 17.60 -17 13 -4 1.00 9.90 17 13 4 10.50 7.90 17 13 4 18.30 11.80 19 13 4 5.20 11.10 -19 13 -4 1.50 7.40 21 13 4 18.50 12.30 21 13 4 2.90 7.40 -21 13 -4 0.00 6.70 -24 -14 4 69.29 10.80 -24 14 4 69.49 13.50 24 14 -4 62.39 16.50 -22 -14 4 53.39 8.90 -22 14 4 43.30 11.40 22 14 -4 38.20 14.50 -20 -14 4 -0.50 8.90 -20 14 4 4.90 8.40 20 14 -4 -7.00 10.10 -20 14 4 3.10 8.10 -18 -14 4 39.00 9.90 18 14 -4 62.59 13.20 -18 14 4 23.60 9.00 -18 14 4 39.20 9.80 18 14 -4 20.90 11.70 -16 -14 4 -3.00 5.50 16 14 -4 6.30 9.40 -16 14 4 7.80 7.60 -16 14 4 -6.10 6.30 16 14 -4 -2.10 8.90 -14 -14 4 177.28 13.80 14 14 -4 182.88 19.30 -14 14 4 170.78 17.30 14 14 -4 193.78 18.60 14 14 -4 157.68 14.50 -14 14 4 188.38 14.70 -12 -14 4 253.37 20.20 -12 -14 4 249.88 16.90 12 14 -4 300.87 20.80 12 14 -4 278.27 21.20 -12 14 4 285.77 20.00 -10 -14 4 376.76 24.00 -10 -14 4 402.26 22.10 -10 14 4 399.16 23.90 -10 14 4 368.76 25.10 10 14 -4 445.16 24.20 -8 -14 4 0.30 4.50 -8 -14 4 -6.30 4.60 -8 14 4 -3.90 5.20 8 14 -4 5.20 9.80 -6 -14 4 70.39 9.00 -6 -14 4 72.99 8.70 -6 14 4 65.99 9.30 6 14 -4 66.39 9.00 -4 -14 4 2.70 4.10 -4 -14 4 -1.90 4.40 -4 14 4 -5.30 4.80 4 14 -4 0.60 5.40 -4 14 4 1.00 4.60 -2 -14 4 405.26 23.10 -2 -14 4 384.96 19.50 -2 14 4 410.56 21.70 -2 14 4 389.86 22.30 2 14 -4 446.06 23.20 0 -14 4 330.57 19.80 0 14 4 348.07 18.30 0 14 -4 362.66 20.90 0 14 4 318.87 20.50 2 -14 4 369.26 22.20 2 14 4 432.46 24.90 2 14 4 410.06 20.10 -2 14 -4 395.46 23.30 4 -14 4 37.40 7.30 4 14 4 38.30 5.40 -4 14 -4 47.80 8.10 4 14 4 38.60 10.00 6 14 4 78.09 7.00 6 14 4 82.09 12.70 -6 14 -4 83.59 11.40 -8 14 -4 4.20 6.30 8 14 4 -12.60 5.40 8 14 4 -2.20 8.20 10 14 4 164.18 18.60 -10 14 -4 156.58 15.50 -12 14 -4 459.65 28.00 12 14 4 449.86 32.20 -14 14 -4 291.37 21.70 14 14 4 286.37 31.70 14 14 4 250.77 20.20 16 14 4 19.70 9.20 -16 14 -4 30.70 9.40 16 14 4 35.40 12.60 -18 14 -4 11.80 8.60 18 14 4 0.90 9.60 20 14 4 16.00 11.60 -20 14 -4 19.20 8.30 -23 -15 4 -5.60 6.50 -23 15 4 5.60 9.20 23 15 -4 -3.30 12.30 -21 -15 4 20.00 7.10 -21 15 4 28.50 9.70 -21 15 4 6.00 8.30 21 15 -4 15.70 13.30 -19 -15 4 130.39 15.80 -19 15 4 98.49 14.10 19 15 -4 127.19 18.10 -19 15 4 77.29 12.70 -17 -15 4 62.69 14.00 17 15 -4 44.70 13.20 -17 15 4 44.50 10.90 17 15 -4 44.90 12.10 -17 15 4 47.40 9.40 -15 -15 4 3.80 5.90 15 15 -4 3.10 9.20 15 15 -4 3.30 6.70 -15 15 4 -1.30 6.40 15 15 -4 1.40 8.50 -15 15 4 8.30 7.20 -13 -15 4 20.60 6.70 13 15 -4 26.20 8.00 -13 15 4 16.20 7.80 13 15 -4 21.00 9.00 13 15 -4 30.30 9.30 -11 -15 4 29.30 8.40 -11 -15 4 25.60 7.00 11 15 -4 25.60 9.00 -11 15 4 17.60 7.40 11 15 -4 24.50 7.60 -9 -15 4 134.19 13.00 -9 -15 4 138.79 12.30 -9 15 4 105.39 12.90 -9 15 4 147.59 16.30 9 15 -4 141.69 12.80 -7 -15 4 577.44 30.90 -7 -15 4 618.14 30.90 -7 15 4 717.63 37.10 7 15 -4 623.04 31.00 -7 15 4 558.84 31.60 -5 -15 4 1249.47 54.99 5 15 -4 1235.18 55.69 -5 15 4 1209.58 55.89 -5 15 4 1286.87 55.09 -3 -15 4 194.58 12.10 -3 -15 4 176.18 14.10 -3 15 4 172.08 15.40 3 15 -4 158.88 14.50 -3 15 4 187.48 14.10 -1 -15 4 63.39 5.80 -1 -15 4 60.79 8.50 -1 15 4 54.39 7.90 1 15 -4 77.89 10.60 -1 15 4 57.19 9.10 1 -15 4 13.90 5.70 1 15 4 23.60 5.30 -1 15 -4 17.20 6.70 1 15 4 28.80 7.90 3 -15 4 10.00 6.00 3 15 4 12.00 8.30 3 15 4 7.00 4.80 -3 15 -4 10.60 6.70 -5 15 -4 447.76 25.80 5 15 4 420.46 20.60 5 15 4 413.56 27.10 7 15 4 5.90 8.70 -7 15 -4 5.50 6.50 -9 15 -4 117.49 13.90 9 15 4 102.89 11.90 9 15 4 101.29 14.80 -11 15 -4 10.80 7.10 11 15 4 20.00 7.20 11 15 4 0.40 10.00 13 15 4 10.10 8.50 13 15 4 20.50 11.40 -13 15 -4 15.00 7.90 15 15 4 0.10 9.20 -15 15 -4 12.20 8.10 15 15 4 18.30 11.10 17 15 4 89.09 17.20 17 15 4 72.59 11.80 -17 15 -4 79.69 13.30 19 15 4 154.58 17.80 19 15 4 108.79 18.80 -19 15 -4 148.49 18.00 -22 -16 4 -10.80 5.90 -22 16 4 3.20 9.80 -22 16 4 12.00 7.70 22 16 -4 10.40 13.20 -20 -16 4 -5.10 5.50 20 16 -4 4.50 21.30 -20 16 4 -3.90 8.40 -18 -16 4 0.80 5.90 -18 16 4 2.40 8.10 -18 16 4 21.20 9.50 18 16 -4 8.40 11.30 18 16 -4 4.60 10.70 -16 -16 4 67.89 10.10 16 16 -4 78.99 14.20 -16 16 4 48.90 9.00 16 16 -4 52.79 13.10 -16 16 4 54.49 11.40 -14 -16 4 9.60 7.20 14 16 -4 1.10 8.50 14 16 -4 5.20 9.00 -14 16 4 1.70 6.50 14 16 -4 10.30 7.30 -14 16 4 13.60 8.20 -12 -16 4 94.29 13.80 -12 -16 4 123.29 17.80 12 16 -4 84.49 10.60 12 16 -4 105.89 13.90 -12 16 4 93.19 12.60 -10 -16 4 -8.30 6.00 10 16 -4 -6.20 6.50 -10 16 4 -10.80 5.80 -8 -16 4 -7.50 5.60 -8 -16 4 -10.30 5.60 8 16 -4 0.70 6.90 -8 16 4 7.40 7.10 -8 16 4 -0.30 6.30 -6 -16 4 10.70 5.90 -6 -16 4 21.70 6.80 -6 16 4 21.60 7.40 -6 16 4 11.20 6.00 6 16 -4 3.60 7.00 -4 -16 4 144.99 13.30 -4 -16 4 114.29 11.20 -4 16 4 128.99 12.30 4 16 -4 140.39 13.50 -4 16 4 159.78 13.70 -2 -16 4 20.30 6.60 -2 -16 4 27.50 5.00 -2 16 4 18.70 7.20 2 16 -4 23.20 6.90 0 -16 4 15.90 6.10 0 16 -4 16.20 7.20 0 16 4 13.60 7.40 0 16 4 20.10 5.90 -2 16 -4 57.19 9.80 2 16 4 38.60 6.80 2 16 4 37.10 9.90 4 16 4 57.09 7.10 4 16 4 53.59 11.70 -4 16 -4 67.79 10.60 -6 16 -4 -8.10 6.00 6 16 4 0.40 8.10 6 16 4 -4.60 4.10 -8 16 -4 48.00 9.70 8 16 4 51.69 12.70 10 16 4 7.50 10.10 10 16 4 -6.20 6.00 -10 16 -4 -2.40 6.40 12 16 4 -6.40 7.10 12 16 4 -7.90 8.90 -12 16 -4 -4.40 6.80 -14 16 -4 14.90 8.30 14 16 4 11.60 9.90 14 16 4 -12.60 9.10 16 16 4 -5.40 7.50 -16 16 -4 6.60 7.80 16 16 4 1.20 11.00 18 16 4 17.60 12.40 -18 16 -4 8.90 7.90 -23 17 4 -15.80 8.20 23 17 -4 -16.80 11.60 -21 -17 4 17.80 7.10 -21 17 4 16.10 9.80 21 17 -4 14.10 13.00 -21 17 4 9.20 10.70 -19 -17 4 132.89 13.20 -19 17 4 97.89 15.20 -19 17 4 123.59 14.20 -17 -17 4 49.30 8.40 17 17 -4 47.30 13.40 17 17 -4 39.70 12.80 -17 17 4 34.10 8.40 -17 17 4 49.30 11.60 -15 -17 4 5.10 6.00 15 17 -4 -5.10 10.40 15 17 -4 19.00 10.30 15 17 -4 -17.50 7.00 -15 17 4 15.30 9.20 -15 17 4 -0.90 6.70 -13 -17 4 1.90 5.80 13 17 -4 4.80 7.10 13 17 -4 4.80 8.60 -13 17 4 -4.30 7.70 -11 -17 4 4.70 7.40 -11 -17 4 7.50 5.80 -11 17 4 -6.70 7.40 11 17 -4 0.50 6.90 -9 -17 4 1.80 5.70 -9 -17 4 -0.70 6.40 9 17 -4 7.50 7.70 -9 17 4 5.00 7.20 -7 -17 4 665.33 34.80 -7 -17 4 686.03 34.70 -7 17 4 738.13 38.20 -7 17 4 684.23 33.20 -7 17 4 738.03 36.50 7 17 -4 672.13 34.80 -5 -17 4 706.53 34.80 -5 -17 4 727.83 36.20 -5 17 4 755.82 35.60 -5 17 4 713.13 36.50 5 17 -4 748.93 36.50 -3 -17 4 -2.70 4.90 -3 17 4 -6.50 5.40 -3 17 4 -6.50 5.60 3 17 -4 -15.90 5.80 -1 17 4 9.90 6.90 1 17 -4 -4.40 6.30 -1 17 4 1.40 6.00 1 17 4 46.60 9.80 1 17 4 32.40 7.10 -1 17 -4 35.60 8.70 3 17 4 47.00 7.30 -3 17 -4 37.40 9.30 3 17 4 45.60 11.40 5 17 4 59.59 11.40 5 17 4 48.00 6.70 -5 17 -4 49.10 10.10 -7 17 -4 174.38 17.60 7 17 4 193.08 19.60 9 17 4 -0.60 6.20 9 17 4 7.50 9.30 -9 17 -4 4.50 7.30 -11 17 -4 9.30 7.70 11 17 4 -1.60 10.50 -13 17 -4 9.90 8.40 13 17 4 -8.60 10.00 13 17 4 -15.90 7.10 -15 17 -4 16.70 9.00 15 17 4 0.80 9.20 15 17 4 24.70 12.20 -17 17 -4 94.19 14.20 17 17 4 84.99 17.30 22 18 -4 5.40 12.30 -22 18 4 17.50 10.10 -20 -18 4 9.30 6.40 -20 18 4 19.70 9.90 -20 18 4 5.00 6.80 20 18 -4 5.90 12.30 -18 -18 4 73.29 9.80 -18 18 4 58.29 9.80 -18 18 4 70.19 12.80 -16 -18 4 -7.30 5.70 16 18 -4 -7.70 7.80 -16 18 4 4.50 6.70 16 18 -4 8.70 10.50 -16 18 4 -4.20 8.00 16 18 -4 4.10 10.80 -14 -18 4 274.27 18.70 14 18 -4 283.27 24.20 14 18 -4 275.07 18.60 -14 18 4 286.47 23.20 14 18 -4 302.87 23.20 -14 18 4 265.57 17.80 -12 -18 4 169.68 14.30 -12 18 4 159.38 18.00 12 18 -4 148.29 14.70 -10 -18 4 173.18 14.60 -10 -18 4 167.68 15.10 10 18 -4 139.49 14.80 -10 18 4 123.69 15.00 -8 -18 4 -1.50 6.20 -8 -18 4 5.10 5.40 -8 18 4 2.60 5.20 -8 18 4 0.90 6.70 8 18 -4 5.90 7.30 -6 -18 4 451.15 25.80 -6 -18 4 450.95 25.20 -6 18 4 462.25 24.70 -6 18 4 475.05 27.20 6 18 -4 463.05 26.60 -4 -18 4 -1.00 4.40 -4 18 4 0.10 5.90 4 18 -4 5.30 7.00 -4 18 4 5.70 6.50 -2 -18 4 142.09 9.50 -2 18 4 144.19 13.90 -2 18 4 141.19 14.10 2 18 -4 129.69 14.90 0 18 4 218.68 17.90 0 18 -4 208.48 18.10 0 18 4 224.18 16.30 2 18 4 250.07 20.50 2 18 4 255.87 16.70 -2 18 -4 262.37 20.10 4 18 4 4.90 5.50 -4 18 -4 1.60 7.00 4 18 4 11.90 8.70 -6 18 -4 23.00 8.70 6 18 4 28.50 6.20 6 18 4 44.00 11.10 8 18 4 -5.30 8.80 -8 18 -4 0.30 7.60 8 18 4 0.90 5.00 10 18 4 100.19 17.00 10 18 4 83.89 11.90 12 18 4 131.19 20.50 12 18 4 65.29 11.20 -12 18 -4 109.49 14.80 14 18 4 21.90 12.40 -14 18 -4 5.60 8.60 14 18 4 9.90 9.60 16 18 4 10.80 9.10 -16 18 -4 11.30 8.70 16 18 4 -7.70 10.10 21 19 -4 1.90 12.70 -21 19 4 10.90 9.50 -19 -19 4 11.50 8.50 -19 19 4 22.70 7.20 19 19 -4 37.90 14.10 -19 19 4 12.40 9.90 -17 -19 4 59.69 9.70 17 19 -4 44.00 17.70 -17 19 4 30.90 7.50 -17 19 4 63.79 13.50 -15 -19 4 24.60 7.50 -15 19 4 7.80 7.00 -15 19 4 30.50 10.20 15 19 -4 13.90 9.10 15 19 -4 10.40 11.30 -13 -19 4 -6.50 5.90 -13 19 4 4.40 11.40 13 19 -4 2.10 7.60 -11 -19 4 5.10 7.00 -11 -19 4 -3.80 7.00 11 19 -4 -5.60 7.10 -11 19 4 -6.10 7.80 -9 -19 4 15.40 7.80 9 19 -4 12.00 8.20 -9 19 4 8.30 7.50 -9 19 4 10.00 5.50 -7 -19 4 11.10 6.30 7 19 -4 16.60 8.00 -7 19 4 14.80 6.30 -7 19 4 10.50 7.80 -5 -19 4 7.00 5.50 -5 19 4 9.60 6.30 5 19 -4 2.60 7.40 -5 19 4 -2.50 6.50 -3 -19 4 4.70 6.20 3 19 -4 7.60 7.60 -3 19 4 9.20 7.40 -3 19 4 7.00 6.80 -1 19 4 6.70 9.00 1 19 -4 0.70 7.60 -1 19 4 9.80 6.60 1 19 4 1.60 6.00 -1 19 -4 4.80 7.70 1 19 4 13.10 8.70 -3 19 -4 18.10 8.30 3 19 4 10.50 8.00 3 19 4 19.30 6.50 5 19 4 18.00 6.40 5 19 4 20.70 10.60 -5 19 -4 14.40 7.90 -7 19 -4 59.99 10.60 7 19 4 51.79 7.30 7 19 4 67.39 14.00 -9 19 -4 25.70 9.90 9 19 4 34.20 9.00 9 19 4 51.99 13.90 11 19 4 -15.50 7.20 -11 19 -4 6.60 8.60 13 19 4 3.60 10.30 13 19 4 -13.10 7.20 -13 19 -4 -5.70 7.40 15 19 4 27.70 13.00 -15 19 -4 1.30 8.20 -20 20 4 7.20 9.20 20 20 -4 -0.90 12.80 -18 20 4 29.90 11.20 18 20 -4 32.30 13.20 -18 20 4 12.90 6.60 16 20 -4 7.40 8.90 -16 20 4 -1.30 8.80 -16 20 4 -3.10 6.00 16 20 -4 -1.30 11.70 14 20 -4 57.09 12.50 14 20 -4 75.69 11.50 -14 20 4 77.69 13.30 -14 20 4 83.49 10.60 12 20 -4 160.48 15.50 -10 -20 4 81.19 12.50 -10 20 4 90.39 9.90 -10 20 4 71.19 12.60 10 20 -4 67.89 10.80 -8 -20 4 2.00 6.40 -8 20 4 -0.70 5.10 8 20 -4 6.10 7.70 -8 20 4 6.20 7.40 -6 -20 4 53.19 8.40 -6 20 4 43.30 9.70 6 20 -4 56.09 10.60 -6 20 4 51.59 8.30 -4 -20 4 75.89 9.60 -4 20 4 94.79 12.40 -4 20 4 108.79 12.30 4 20 -4 98.99 12.40 -2 20 4 202.98 16.80 2 20 -4 194.58 18.20 0 20 4 83.79 12.70 0 20 4 69.39 10.00 0 20 -4 71.59 11.70 2 20 4 93.09 13.40 2 20 4 87.29 10.70 -2 20 -4 96.09 12.70 4 20 4 8.30 9.00 4 20 4 1.40 6.20 -4 20 -4 5.80 7.60 -6 20 -4 -4.20 9.60 6 20 4 -10.40 5.90 6 20 4 -1.30 9.60 8 20 4 20.20 12.40 8 20 4 10.10 6.30 -8 20 -4 7.90 8.90 10 20 4 144.49 16.30 10 20 4 160.68 25.90 -10 20 -4 103.69 15.30 12 20 4 122.79 18.80 -12 20 -4 101.99 14.70 12 20 4 77.19 11.70 -14 20 -4 22.70 10.60 14 20 4 5.70 7.70 14 20 4 12.70 11.90 -19 21 4 37.10 11.50 19 21 -4 39.40 13.70 -17 21 4 32.40 11.30 17 21 -4 36.80 13.50 -17 21 4 18.60 6.50 15 21 -4 24.40 12.60 -15 21 4 8.10 7.30 15 21 -4 3.60 8.80 -15 21 4 20.90 10.50 -13 21 4 -12.40 7.40 -13 21 4 -2.10 4.30 -13 21 4 -4.40 5.70 13 21 -4 -8.40 7.80 -11 21 4 1.00 4.80 -11 21 4 4.90 9.30 11 21 -4 -2.00 7.50 -9 -21 4 0.80 6.00 9 21 -4 9.00 8.50 -9 21 4 -0.70 5.10 -9 21 4 10.00 8.20 -7 -21 4 31.30 7.50 7 21 -4 46.20 10.00 -7 21 4 37.60 9.50 -7 21 4 28.20 7.00 -5 -21 4 5.50 5.70 -5 21 4 21.90 7.20 -5 21 4 8.00 7.50 5 21 -4 8.80 8.10 -3 21 4 38.80 9.20 -3 21 4 27.60 9.20 3 21 -4 24.10 8.90 -1 21 4 -5.30 6.50 -1 21 4 -4.30 6.50 1 21 -4 -5.10 7.60 1 21 4 -1.10 6.50 1 21 4 -3.10 7.10 -1 21 -4 -11.80 7.50 3 21 4 17.80 9.50 -3 21 -4 9.10 8.10 3 21 4 5.60 7.20 5 21 4 52.79 9.30 -5 21 -4 58.99 13.50 5 21 4 82.99 14.50 -7 21 -4 217.28 21.30 7 21 4 204.38 22.90 9 21 4 50.69 13.20 -9 21 -4 23.90 10.80 11 21 4 4.60 7.50 -11 21 -4 0.20 8.70 11 21 4 -10.20 10.50 13 21 4 2.40 7.90 -13 21 -4 12.70 9.20 13 21 4 4.30 11.20 18 22 -4 -7.20 11.10 -18 22 4 6.40 9.40 16 22 -4 -11.10 8.80 16 22 -4 9.10 12.40 -16 22 4 29.50 11.20 14 22 -4 11.20 10.90 -14 22 4 19.10 10.30 14 22 -4 -2.10 8.20 12 22 -4 14.60 8.80 -12 22 4 15.10 5.00 -12 22 4 26.20 11.00 -10 22 4 -3.90 4.40 -10 22 4 0.50 8.50 10 22 -4 9.10 8.60 -8 -22 4 5.50 6.50 8 22 -4 24.20 9.00 -8 22 4 4.40 5.70 -8 22 4 1.60 8.40 -6 -22 4 -9.00 4.90 -6 22 4 6.70 5.80 -6 22 4 8.00 7.80 6 22 -4 2.50 8.30 -4 22 4 71.09 10.90 4 22 -4 63.59 11.50 -4 22 4 64.49 11.00 2 22 -4 0.10 8.70 -2 22 4 5.80 7.50 -2 22 4 1.90 6.80 0 22 4 41.40 9.90 0 22 -4 38.40 10.70 0 22 4 26.10 8.70 2 22 4 9.20 8.80 2 22 4 -8.80 7.00 -2 22 -4 8.60 13.90 4 22 4 -2.30 9.20 4 22 4 -5.50 6.80 -4 22 -4 -4.20 8.60 -6 22 -4 -3.30 8.50 6 22 4 1.40 7.00 6 22 4 -13.60 9.50 -8 22 -4 35.30 11.40 8 22 4 33.40 7.50 8 22 4 31.20 12.50 10 22 4 -10.80 9.80 10 22 4 -1.80 8.10 -10 22 -4 -4.10 8.40 12 22 4 -2.10 8.00 12 22 4 11.20 12.30 -12 22 -4 -2.10 8.40 15 23 -4 -5.70 8.70 15 23 -4 -0.80 11.10 -15 23 4 28.10 11.30 -13 23 4 -9.00 8.80 13 23 -4 1.10 8.00 -11 23 4 -2.30 4.40 11 23 -4 -11.20 7.60 -11 23 4 -4.60 8.60 -9 -23 4 51.89 10.30 -9 23 4 51.79 11.80 -9 23 4 80.69 9.40 9 23 -4 64.49 12.20 -7 -23 4 42.20 9.10 -7 23 4 60.89 9.10 -7 23 4 51.39 11.50 7 23 -4 70.39 11.90 -5 23 4 66.89 9.90 5 23 -4 59.19 12.00 -5 23 4 60.19 11.30 -3 23 4 98.99 13.40 -3 23 4 136.39 15.10 3 23 -4 70.99 12.70 -1 23 4 28.00 9.50 1 23 -4 9.50 9.90 -1 23 4 4.60 8.40 1 23 4 -4.10 7.90 1 23 4 4.20 9.20 -1 23 -4 -1.90 8.90 -3 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1 5 -9 28.20 6.40 1 -5 9 12.40 5.60 -1 5 -9 6.40 6.20 1 5 9 7.10 4.70 3 -5 9 166.78 13.20 3 -5 9 162.28 14.40 3 5 9 145.09 17.20 3 5 9 122.19 10.90 -3 5 -9 184.08 17.30 5 -5 9 28.30 8.60 5 -5 9 23.80 6.30 -5 5 -9 27.40 6.60 5 5 9 21.80 10.10 5 5 9 15.50 4.10 7 -5 9 483.55 29.00 7 -5 9 481.35 25.90 -7 5 -9 507.35 26.30 7 5 9 492.65 32.40 9 -5 9 278.67 21.70 9 -5 9 245.68 16.70 9 5 9 279.87 25.40 -9 5 -9 296.87 18.40 -9 5 -9 250.77 18.00 11 -5 9 117.69 11.30 11 -5 9 150.78 16.20 -11 5 -9 131.29 12.90 -11 5 -9 116.49 12.90 11 5 9 134.49 19.80 13 -5 9 33.40 10.40 13 -5 9 7.10 5.00 -13 5 -9 23.30 6.90 -13 5 -9 24.90 7.40 15 -5 9 -3.60 7.50 15 5 9 6.90 10.20 -15 5 -9 3.10 6.10 17 -5 9 -1.70 7.30 -17 5 -9 2.50 5.90 17 5 9 -4.80 10.20 28 -6 -9 6.00 11.50 -28 6 9 -5.10 8.60 28 6 -9 6.20 13.10 26 -6 -9 -2.80 10.20 26 6 -9 -6.50 11.50 24 -6 -9 11.20 10.20 24 6 -9 -5.50 12.50 22 -6 -9 2.10 10.40 22 6 -9 -2.40 13.00 20 -6 -9 68.39 14.10 20 6 -9 45.80 13.20 18 -6 -9 83.79 14.20 18 6 -9 69.29 13.00 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72.09 11.90 10 6 9 59.19 14.70 -10 6 -9 61.09 9.20 -10 6 -9 71.59 9.80 12 -6 9 -3.10 7.10 12 6 9 -7.40 9.50 -12 6 -9 -7.10 4.90 -12 6 -9 -2.70 5.00 14 -6 9 2.20 7.30 14 6 9 12.50 10.50 -14 6 -9 18.60 6.80 16 -6 9 42.70 11.40 -16 6 -9 40.30 8.90 16 6 9 53.99 14.90 18 -6 9 -5.00 7.50 -18 6 -9 5.90 6.80 18 6 9 3.30 11.60 27 -7 -9 57.79 15.50 -27 7 9 19.50 10.20 27 7 -9 68.09 16.80 25 -7 -9 -6.20 9.80 25 7 -9 14.40 14.50 23 -7 -9 16.90 11.80 23 7 -9 19.70 14.20 21 -7 -9 30.00 11.80 21 7 -9 26.40 13.60 19 -7 -9 -5.60 8.60 19 7 -9 -7.90 9.90 17 -7 -9 34.20 10.50 17 7 -9 34.50 11.90 -15 -7 9 578.74 30.10 -15 -7 9 539.85 33.70 15 -7 -9 561.14 33.30 15 7 -9 570.94 32.90 -15 7 9 596.64 32.10 -13 -7 9 645.74 32.40 -13 -7 9 580.44 29.60 13 -7 -9 483.65 31.40 13 7 -9 581.14 31.50 -13 7 9 553.14 36.20 -11 -7 9 -6.50 5.10 11 -7 -9 -7.00 5.90 -11 7 9 -9.10 5.70 11 7 -9 -5.40 5.80 11 7 -9 -9.40 6.30 9 -7 -9 -5.00 5.30 9 7 -9 -5.30 5.30 -9 7 9 -0.10 5.00 7 -7 -9 3.60 5.10 -7 -7 9 13.20 6.60 -7 7 9 4.70 4.60 7 7 -9 10.60 6.00 5 -7 -9 1254.47 50.99 -5 -7 9 1125.19 52.39 5 7 -9 1130.89 51.79 -3 -7 9 1344.67 58.69 3 7 -9 1321.47 58.19 -3 7 9 1314.47 56.09 -1 -7 9 426.06 23.10 1 7 -9 449.26 23.00 -1 7 9 380.36 20.00 1 -7 9 18.50 9.20 1 7 9 27.10 8.20 -1 7 -9 4.10 5.40 3 -7 9 99.19 12.00 3 -7 9 94.09 11.00 3 7 9 111.49 14.80 3 7 9 90.89 8.00 -3 7 -9 114.49 11.90 5 -7 9 32.60 8.30 5 -7 9 30.60 6.70 5 7 9 25.10 10.00 -5 7 -9 26.00 7.00 7 -7 9 12.80 5.10 7 -7 9 12.30 7.50 7 7 9 20.10 11.10 -7 7 -9 22.70 6.90 9 -7 9 46.40 10.00 9 -7 9 17.80 5.20 -9 7 -9 35.70 7.90 9 7 9 30.30 11.90 11 -7 9 104.39 13.60 -11 7 -9 119.09 13.30 11 7 9 96.59 17.40 13 -7 9 33.90 9.80 13 7 9 30.50 12.90 -13 7 -9 14.40 7.30 15 -7 9 20.00 8.70 15 7 9 9.90 12.00 -15 7 -9 22.60 8.00 17 -7 9 2.50 7.70 17 7 9 10.40 12.10 -17 7 -9 -5.00 5.90 28 -8 -9 5.80 11.40 28 8 -9 11.80 12.00 -28 8 9 -8.50 9.40 26 -8 -9 28.30 12.90 -26 8 9 34.00 10.80 26 8 -9 39.30 14.70 24 -8 -9 39.60 13.50 24 8 -9 18.10 14.00 22 8 -9 121.09 22.20 20 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9 22.60 11.80 -8 8 -9 35.00 8.10 10 -8 9 80.59 11.90 10 8 9 76.79 16.00 -10 8 -9 73.09 10.80 12 -8 9 10.30 7.80 12 8 9 13.50 11.90 -12 8 -9 17.60 7.60 14 -8 9 185.08 18.00 14 8 9 213.78 25.00 -14 8 -9 202.48 17.60 16 -8 9 126.59 16.30 16 8 9 132.89 20.20 -16 8 -9 104.39 13.40 27 -9 -9 -4.60 10.90 27 9 -9 8.80 13.20 -27 9 9 -11.90 8.70 25 -9 -9 6.40 11.20 25 9 -9 8.90 12.80 -25 9 9 7.90 9.60 23 -9 -9 26.50 12.80 23 9 -9 28.60 14.50 21 -9 -9 16.10 11.70 21 9 -9 34.20 18.80 19 -9 -9 -10.50 8.80 19 9 -9 -4.00 10.40 17 -9 -9 100.69 15.50 17 9 -9 108.69 15.70 15 -9 -9 235.28 22.20 15 9 -9 239.18 21.80 -15 9 9 262.27 23.70 -13 -9 9 -6.10 7.50 13 -9 -9 -5.10 7.70 -13 -9 9 -12.10 5.70 -13 9 9 0.90 7.20 13 9 -9 -4.50 8.20 13 9 -9 3.30 7.30 -11 -9 9 -6.10 5.80 -11 -9 9 5.90 7.10 11 9 -9 -4.10 6.50 -11 9 9 14.80 7.00 11 9 -9 5.80 6.60 -9 -9 9 -4.60 5.70 -9 9 9 12.90 6.10 9 9 -9 6.00 6.20 -7 -9 9 60.39 8.60 -7 9 9 66.09 8.10 7 9 -9 70.99 9.40 -5 -9 9 3.50 5.20 5 9 -9 3.40 5.70 -3 -9 9 17.80 5.70 3 9 -9 24.00 6.80 -1 -9 9 93.29 10.60 1 9 -9 100.59 11.60 -1 9 9 76.59 8.20 1 -9 9 54.59 8.30 -1 9 -9 69.39 9.30 1 9 9 58.99 7.40 1 9 9 54.09 10.70 3 -9 9 7.20 5.50 3 -9 9 22.50 6.90 -3 9 -9 16.30 6.80 3 9 9 43.00 11.60 3 9 9 10.70 4.40 5 -9 9 128.89 12.70 5 -9 9 107.69 12.90 -5 9 -9 126.19 13.40 5 9 9 129.09 17.10 7 -9 9 5.00 6.30 7 9 9 13.50 10.00 -7 9 -9 7.70 6.20 9 -9 9 66.49 10.20 -9 9 -9 75.89 11.00 9 9 9 84.39 16.20 11 -9 9 77.59 11.70 -11 9 -9 59.99 10.60 13 -9 9 2.80 7.60 -13 9 -9 1.10 6.70 13 9 9 3.00 11.10 15 -9 9 23.30 8.50 -15 9 -9 9.60 7.20 15 9 9 11.20 12.10 17 -9 9 17.60 8.20 17 9 9 14.60 11.60 26 10 -9 16.20 14.70 -26 10 9 8.70 10.30 24 10 -9 26.00 13.30 -24 10 9 10.00 9.20 22 -10 -9 185.48 25.30 22 10 -9 220.58 26.80 20 -10 -9 296.07 27.70 20 10 -9 308.87 27.10 18 -10 -9 -8.00 8.80 18 10 -9 -0.70 10.30 16 -10 -9 1.20 8.70 16 10 -9 -20.60 9.10 -14 -10 9 21.60 9.40 14 -10 -9 8.30 8.70 14 10 -9 33.10 10.20 14 10 -9 14.80 8.40 -14 10 9 19.20 9.20 -12 -10 9 288.27 19.80 -12 -10 9 279.07 21.30 12 10 -9 317.47 19.80 12 10 -9 338.67 22.90 -10 -10 9 700.83 36.10 -10 -10 9 708.63 35.50 -10 10 9 750.72 35.70 10 10 -9 678.03 34.30 -8 -10 9 810.62 39.40 8 10 -9 828.62 39.00 -8 10 9 800.52 38.30 -6 -10 9 188.48 14.30 6 10 -9 166.28 13.90 -6 10 9 155.78 13.30 -4 -10 9 123.69 11.70 4 10 -9 107.59 12.00 -2 -10 9 200.48 15.60 2 10 -9 219.68 16.40 0 -10 9 21.90 6.60 0 10 9 38.30 5.90 0 10 9 13.40 8.10 0 10 -9 24.10 7.50 2 -10 9 432.86 25.20 2 10 9 424.56 20.70 2 10 9 444.66 28.40 -2 10 -9 446.36 25.40 4 -10 9 134.99 12.30 -4 10 -9 105.99 13.50 4 10 9 145.09 18.50 6 -10 9 7.10 5.80 6 10 9 2.30 8.60 -6 10 -9 -9.80 5.40 8 -10 9 4.00 6.40 -8 10 -9 -1.80 5.90 8 10 9 14.20 10.30 10 -10 9 3.80 7.20 -10 10 -9 2.60 6.40 10 10 9 -7.60 12.10 12 -10 9 9.90 7.10 -12 10 -9 12.80 7.80 12 10 9 -0.20 10.10 14 -10 9 233.88 18.90 -14 10 -9 235.78 19.80 14 10 9 266.17 28.50 16 -10 9 122.59 15.10 -16 10 -9 100.49 14.50 16 10 9 126.49 21.20 25 11 -9 9.20 14.30 -25 11 9 7.70 10.80 23 11 -9 11.60 13.00 -23 11 9 4.50 9.80 21 11 -9 48.60 14.60 -21 11 9 36.00 10.40 19 11 -9 1.10 10.90 17 11 -9 11.50 10.50 15 11 -9 31.10 9.20 15 11 -9 25.70 10.60 -13 -11 9 3.40 8.40 13 11 -9 13.30 9.30 -13 11 9 12.40 8.30 13 11 -9 2.90 7.50 -11 -11 9 111.19 22.60 -11 11 9 87.49 11.40 11 11 -9 79.99 10.50 -9 -11 9 -2.30 6.20 -9 -11 9 -4.80 6.80 -9 11 9 -2.20 6.50 9 11 -9 -2.30 6.70 -7 -11 9 -10.30 5.30 -7 11 9 -12.20 5.50 7 11 -9 -2.80 6.20 -5 -11 9 116.09 12.00 -5 11 9 109.29 11.70 5 11 -9 131.29 12.90 -3 -11 9 109.49 11.90 3 11 -9 112.69 13.40 -1 -11 9 227.18 23.00 -1 11 9 258.77 19.70 1 11 -9 228.28 18.00 1 11 9 197.08 18.70 -1 11 -9 152.08 15.10 1 11 9 174.88 10.90 1 11 9 144.29 10.60 3 -11 9 0.80 5.20 -3 11 -9 -7.70 5.50 3 11 9 0.00 2.80 3 11 9 -2.30 8.40 3 11 9 0.30 3.70 5 -11 9 -2.00 5.20 5 11 9 -4.60 8.60 -5 11 -9 1.80 6.50 7 -11 9 11.50 6.70 7 11 9 3.10 10.10 -7 11 -9 -9.80 5.70 9 -11 9 35.30 8.70 9 11 9 39.80 13.50 -9 11 -9 43.80 9.50 11 -11 9 123.89 14.60 11 11 9 127.79 21.10 -11 11 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7.30 13.00 10 -12 9 0.00 5.80 -10 12 -9 6.00 7.20 10 12 9 21.70 13.70 12 -12 9 10.40 5.70 -12 12 -9 -4.00 7.30 12 12 9 25.80 12.90 14 -12 9 62.99 10.00 -14 12 -9 44.20 10.40 14 12 9 52.49 16.00 16 -12 9 19.50 7.70 16 12 9 19.40 11.90 -16 12 -9 20.70 8.50 25 13 -9 27.10 14.80 -25 13 9 4.30 10.10 23 13 -9 -4.00 13.20 -23 13 9 6.20 9.90 21 13 -9 -6.40 11.80 -21 13 9 -5.80 8.80 -19 13 9 -2.50 7.70 19 13 -9 0.60 12.80 -17 13 9 74.39 12.70 17 13 -9 99.99 15.30 15 13 -9 468.55 29.10 15 13 -9 653.43 34.60 -15 13 9 538.95 31.90 -13 -13 9 134.99 16.20 -13 13 9 104.59 16.80 13 13 -9 151.28 18.40 -13 13 9 167.38 16.40 13 13 -9 114.09 14.50 -11 -13 9 6.30 7.90 -11 13 9 -12.10 7.00 -11 13 9 0.10 7.00 11 13 -9 -3.30 7.50 -9 -13 9 -12.00 6.60 -9 13 9 -11.90 5.50 -9 13 9 -13.10 6.10 9 13 -9 -8.40 6.70 -7 -13 9 6.50 7.30 -7 13 9 10.70 6.50 -7 13 9 0.80 6.40 7 13 -9 11.60 7.60 -5 -13 9 243.28 17.30 -5 13 9 247.18 17.40 -5 13 9 301.37 17.40 5 13 -9 274.77 19.30 -3 13 9 269.77 17.30 3 13 -9 283.97 20.30 -1 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7.90 -1 5 17 53.99 15.80 1 -5 17 33.90 16.00 -1 5 -17 10.70 15.80 1 5 17 12.90 15.90 1 5 17 -0.50 11.40 3 -5 17 1.30 11.90 -3 5 -17 -4.00 9.10 3 5 17 9.60 14.50 3 5 17 -2.60 9.20 22 -6 -17 13.50 13.80 22 6 -17 -1.30 15.10 20 -6 -17 -5.90 11.50 20 6 -17 -7.10 13.00 18 -6 -17 19.30 12.50 18 6 -17 24.20 14.70 16 -6 -17 -2.50 9.80 16 6 -17 2.00 15.20 14 -6 -17 -4.20 9.50 14 6 -17 17.90 12.40 12 -6 -17 4.00 9.30 12 6 -17 -6.70 11.90 10 6 -17 5.50 9.90 10 6 -17 5.70 11.20 8 6 -17 5.00 10.20 8 6 -17 8.50 9.50 6 6 -17 3.30 9.50 6 6 -17 6.40 10.20 4 6 -17 6.20 9.10 2 6 -17 3.30 8.80 -2 6 17 -9.10 10.80 0 -6 17 0.80 13.30 0 6 17 5.50 10.60 0 6 -17 14.30 9.50 0 6 17 16.00 13.60 2 -6 17 19.60 13.90 2 6 17 1.60 13.60 -2 6 -17 17.00 9.30 2 6 17 6.50 8.70 21 -7 -17 6.50 11.30 21 7 -17 -6.60 13.10 19 -7 -17 -4.00 11.30 19 7 -17 -11.30 12.90 17 -7 -17 50.19 13.50 17 7 -17 32.20 14.90 15 -7 -17 79.89 14.60 15 7 -17 89.49 24.90 13 -7 -17 20.30 9.90 13 7 -17 3.70 12.10 11 -7 -17 -6.90 7.80 11 7 -17 -5.80 11.60 11 7 -17 -9.60 9.50 9 7 -17 9.40 11.10 9 7 -17 16.70 10.60 7 7 -17 9.90 9.90 7 7 -17 1.50 9.70 5 7 -17 20.00 10.50 3 7 -17 6.50 9.50 1 7 -17 -15.40 8.00 -1 7 17 0.40 12.80 1 -7 17 -3.10 14.40 1 7 17 7.60 13.00 -1 7 -17 5.70 9.10 3 -7 17 18.00 13.50 3 7 17 -12.00 11.70 -3 7 -17 2.90 8.60 22 -8 -17 12.00 12.60 22 8 -17 3.20 13.80 20 -8 -17 16.80 11.70 20 8 -17 10.70 13.90 18 -8 -17 -4.40 10.40 18 8 -17 27.80 15.10 16 -8 -17 7.30 10.50 16 8 -17 11.00 13.60 14 -8 -17 -0.10 9.10 14 8 -17 -11.00 12.90 12 -8 -17 2.40 8.40 12 8 -17 -10.50 9.70 12 8 -17 -14.50 11.20 10 8 -17 38.50 11.90 10 8 -17 46.70 13.60 8 8 -17 63.09 13.30 8 8 -17 78.09 13.20 6 8 -17 2.70 9.60 4 8 -17 -15.00 8.70 2 8 -17 -10.60 8.80 -2 8 17 -10.90 10.90 0 -8 17 -5.10 11.40 0 8 17 -25.30 8.40 0 8 -17 0.50 8.90 0 8 17 -1.40 13.70 2 -8 17 14.30 15.70 -2 8 -17 4.80 9.10 2 8 17 -2.30 13.20 21 -9 -17 11.60 12.00 21 9 -17 3.00 14.60 19 9 -17 -6.60 13.10 17 -9 -17 13.70 11.10 17 9 -17 24.50 14.30 15 -9 -17 -6.30 9.10 15 9 -17 -8.40 13.00 13 -9 -17 6.60 9.40 13 9 -17 -22.30 11.70 13 9 -17 -4.40 9.50 11 9 -17 -12.90 13.00 11 9 -17 9.50 10.90 9 9 -17 31.70 11.50 9 9 -17 22.80 11.90 7 9 -17 15.90 10.10 5 9 -17 -11.30 8.80 3 9 -17 1.40 9.70 -3 9 17 3.80 11.40 1 9 -17 7.50 9.60 -1 9 17 -21.40 8.40 -1 9 17 5.30 12.70 1 -9 17 -32.40 11.20 -1 9 -17 -6.60 9.30 1 9 17 -12.40 12.50 20 -10 -17 35.40 13.20 20 10 -17 32.50 16.00 18 -10 -17 4.70 11.30 18 10 -17 24.00 14.00 16 -10 -17 25.50 12.20 16 10 -17 22.30 14.00 14 10 -17 2.20 13.40 14 10 -17 4.80 10.80 12 10 -17 -6.50 9.60 12 10 -17 -12.30 11.70 10 10 -17 75.59 13.80 8 10 -17 49.40 12.90 8 10 -17 36.40 11.50 6 10 -17 -19.60 8.80 4 10 -17 -1.90 9.10 -2 10 17 0.40 12.10 2 10 -17 23.30 10.50 0 -10 17 8.20 11.90 0 10 17 9.00 13.60 0 10 -17 -5.90 9.50 0 10 17 -27.30 13.50 19 11 -17 -8.50 14.10 17 11 -17 12.90 14.00 15 11 -17 16.70 13.20 13 11 -17 -2.80 13.20 13 11 -17 -4.60 9.90 11 11 -17 -2.40 12.80 11 11 -17 7.30 10.20 9 11 -17 13.30 10.80 9 11 -17 -3.00 11.00 7 11 -17 -5.90 9.50 5 11 -17 -11.50 8.90 3 11 -17 19.70 10.40 -3 11 17 -2.70 11.60 -1 -11 17 -5.20 10.70 -1 11 17 -6.30 10.40 -1 11 17 3.40 13.40 1 11 -17 8.90 10.70 18 12 -17 -6.50 14.00 16 12 -17 0.10 12.90 14 12 -17 5.80 12.90 14 12 -17 -5.90 10.80 12 12 -17 4.80 10.70 12 12 -17 -2.20 12.80 10 12 -17 13.80 11.20 10 12 -17 38.00 13.20 8 12 -17 17.70 11.00 6 12 -17 -10.10 9.10 4 12 -17 2.70 10.70 -4 12 17 2.20 11.10 -2 12 17 7.80 14.20 2 12 -17 -0.90 10.30 17 13 -17 27.30 15.40 15 13 -17 9.90 13.00 15 13 -17 10.10 10.70 13 13 -17 0.80 11.00 13 13 -17 -10.70 12.10 11 13 -17 -13.20 11.80 11 13 -17 -2.00 10.90 9 13 -17 -6.60 9.30 7 13 -17 -6.30 10.10 5 13 -17 -7.20 9.80 -5 13 17 0.80 12.70 3 13 -17 45.40 13.00 -3 13 17 32.30 14.80 14 14 -17 -2.70 13.50 14 14 -17 -8.40 11.20 12 14 -17 -6.10 11.70 12 14 -17 -3.50 11.20 10 14 -17 -10.50 9.80 8 14 -17 -11.50 9.50 6 14 -17 8.80 10.60 -6 14 17 9.60 12.80 -4 14 17 -2.00 12.60 4 14 -17 -17.60 10.40 13 15 -17 -23.80 10.30 13 15 -17 -20.90 11.80 11 15 -17 -1.30 10.70 11 15 -17 -15.90 11.20 9 15 -17 10.90 11.10 7 15 -17 3.90 10.50 22 0 -18 6.70 14.50 20 0 -18 -19.30 13.50 16 0 -18 21.80 13.20 14 0 -18 11.80 11.80 12 0 -18 -2.30 10.80 10 0 -18 4.00 10.10 8 0 -18 59.69 11.60 0 0 18 5.40 13.60 2 0 18 11.50 14.40 21 -1 -18 5.90 14.40 21 1 -18 -8.30 13.60 19 -1 -18 -3.60 13.80 19 1 -18 -5.70 13.50 17 -1 -18 -3.70 12.20 17 1 -18 3.80 13.50 15 -1 -18 -5.50 11.20 15 1 -18 2.60 11.90 13 -1 -18 -4.90 11.10 13 1 -18 -5.00 11.10 11 -1 -18 49.70 12.40 11 1 -18 0.90 10.50 9 -1 -18 8.90 10.10 9 1 -18 5.00 9.70 7 1 -18 17.20 9.70 -1 -1 18 -13.00 11.40 -1 1 18 -8.30 11.90 1 -1 18 -5.30 14.10 1 1 18 9.70 16.00 22 -2 -18 5.40 13.60 22 2 -18 8.80 14.60 20 -2 -18 -4.50 13.00 20 2 -18 0.70 13.90 18 -2 -18 -9.50 12.00 18 2 -18 -3.50 13.20 16 -2 -18 0.70 11.90 16 2 -18 11.40 13.10 14 -2 -18 -13.80 11.10 14 2 -18 -12.50 11.00 12 -2 -18 8.30 11.20 12 2 -18 4.80 11.10 10 -2 -18 7.40 9.80 10 2 -18 1.60 10.50 8 2 -18 18.20 10.40 6 2 -18 21.70 9.20 0 -2 18 19.60 14.20 0 2 18 37.60 15.60 2 -2 18 7.10 12.80 2 2 18 19.60 15.40 21 -3 -18 9.10 13.80 21 3 -18 14.00 15.70 19 -3 -18 11.60 12.80 19 3 -18 1.60 14.40 17 -3 -18 0.30 11.90 17 3 -18 -7.10 13.30 15 -3 -18 3.50 11.60 15 3 -18 -0.50 12.40 13 -3 -18 31.80 12.20 13 3 -18 22.20 12.50 11 -3 -18 54.99 12.10 11 3 -18 24.20 11.70 9 3 -18 15.10 10.50 7 3 -18 4.90 9.50 5 3 -18 -7.20 9.00 -1 -3 18 -4.60 11.60 -1 3 18 -0.40 13.30 1 3 -18 29.40 12.80 1 -3 18 22.70 15.90 1 3 18 17.20 16.70 -1 3 -18 34.70 12.70 22 -4 -18 9.30 13.20 22 4 -18 -15.40 14.30 20 -4 -18 3.80 12.20 20 4 -18 -5.40 14.40 18 -4 -18 18.10 12.30 18 4 -18 -14.70 13.00 16 -4 -18 -16.20 10.40 14 -4 -18 11.20 11.30 14 4 -18 10.40 12.80 12 -4 -18 4.70 10.30 12 4 -18 3.70 11.80 10 4 -18 19.00 11.40 8 4 -18 20.90 11.20 6 4 -18 30.60 10.50 4 4 -18 4.00 9.50 4 4 -18 -0.30 9.20 2 4 -18 11.50 10.00 -2 4 18 -8.80 12.60 0 -4 18 18.50 13.60 0 4 18 -3.10 13.60 0 4 -18 5.20 8.90 21 -5 -18 11.90 12.80 21 5 -18 -5.30 14.10 19 5 -18 -9.80 13.60 17 -5 -18 6.70 11.70 17 5 -18 16.80 13.80 15 -5 -18 20.50 12.10 13 -5 -18 30.20 11.10 13 5 -18 16.20 12.20 11 -5 -18 26.50 10.60 11 5 -18 3.60 11.40 9 5 -18 10.70 11.50 7 5 -18 -0.90 10.10 7 5 -18 8.80 10.20 5 5 -18 15.90 10.20 5 5 -18 -3.10 9.30 3 5 -18 -1.00 9.10 3 5 -18 10.70 10.40 -1 -5 18 -4.50 12.30 -1 5 18 5.60 13.80 1 5 -18 14.80 9.30 1 5 -18 9.90 9.70 1 -5 18 -6.80 13.40 1 5 18 15.80 15.50 -1 5 -18 4.70 9.20 20 -6 -18 19.90 12.40 20 6 -18 5.50 14.70 18 -6 -18 54.99 14.10 18 6 -18 40.50 15.10 16 -6 -18 29.30 12.60 16 6 -18 35.20 14.90 14 -6 -18 14.90 10.30 12 -6 -18 9.30 9.70 12 6 -18 10.90 11.90 10 6 -18 6.20 11.30 8 6 -18 18.40 11.90 8 6 -18 19.70 10.80 6 6 -18 60.29 12.80 6 6 -18 53.59 12.30 4 6 -18 -0.50 9.60 4 6 -18 -0.30 10.00 2 6 -18 -12.20 9.00 -2 6 18 -6.00 12.00 0 -6 18 -1.00 12.20 0 6 18 3.10 15.00 0 6 -18 -17.00 8.30 19 7 -18 13.60 14.30 17 -7 -18 37.50 12.60 17 7 -18 42.70 14.50 15 -7 -18 -5.80 9.50 15 7 -18 4.30 13.50 13 -7 -18 0.70 9.10 11 7 -18 2.10 11.40 9 7 -18 14.60 11.30 9 7 -18 13.80 10.80 7 7 -18 7.30 11.60 7 7 -18 5.50 10.00 5 7 -18 -5.60 9.80 5 7 -18 -13.40 9.70 -3 7 18 -5.00 10.30 3 7 -18 -17.30 8.70 -1 -7 18 -9.70 11.20 -1 7 18 -17.60 11.00 1 7 -18 -11.00 9.30 20 -8 -18 7.20 11.20 20 8 -18 2.60 15.20 18 -8 -18 34.50 12.90 18 8 -18 19.10 14.60 16 -8 -18 19.40 10.60 16 8 -18 13.50 13.40 14 -8 -18 11.10 10.30 14 8 -18 -9.60 13.40 12 -8 -18 13.70 9.60 12 8 -18 -15.90 14.10 10 8 -18 20.60 11.10 10 8 -18 -4.30 11.40 8 8 -18 39.20 12.50 8 8 -18 50.29 13.80 6 8 -18 17.80 10.60 6 8 -18 19.20 11.50 4 8 -18 5.70 10.10 2 8 -18 -0.10 9.40 -2 8 18 2.20 13.10 19 -9 -18 18.80 13.60 19 9 -18 1.50 14.80 17 9 -18 9.20 13.80 15 -9 -18 4.10 10.70 15 9 -18 4.50 13.20 13 9 -18 4.30 12.90 11 9 -18 14.90 11.30 11 9 -18 18.80 13.10 9 9 -18 25.70 11.80 9 9 -18 27.80 18.50 7 9 -18 -6.10 10.00 7 9 -18 -7.60 10.10 5 9 -18 -4.40 9.90 -3 9 18 -3.80 11.90 3 9 -18 3.90 10.30 18 -10 -18 -4.20 10.60 18 10 -18 4.70 14.20 16 10 -18 9.50 14.40 14 10 -18 15.20 13.30 12 10 -18 -6.40 10.30 12 10 -18 -0.80 12.90 10 10 -18 2.50 10.60 10 10 -18 -2.10 12.10 8 10 -18 -13.30 9.50 8 10 -18 2.60 11.30 6 10 -18 -20.00 9.70 -4 10 18 -18.10 11.50 4 10 -18 -17.10 9.50 15 11 -18 27.30 15.20 13 11 -18 23.10 12.00 13 11 -18 35.20 14.30 11 11 -18 32.90 13.00 11 11 -18 17.60 14.60 9 11 -18 -1.80 10.90 9 11 -18 6.70 10.80 7 11 -18 -25.50 9.50 5 11 -18 -21.60 9.90 14 12 -18 -3.70 11.80 14 12 -18 0.90 13.40 12 12 -18 13.50 11.90 12 12 -18 -1.30 13.60 10 12 -18 11.40 13.60 10 12 -18 -9.40 10.80 8 12 -18 15.60 11.50 6 12 -18 13.40 11.70 11 13 -18 0.70 12.90 11 13 -18 -8.70 10.60 20 0 -19 6.00 13.40 18 0 -19 -21.50 12.50 16 0 -19 1.30 12.70 14 0 -19 -13.60 11.70 12 0 -19 -8.10 10.70 10 0 -19 8.20 10.70 8 0 -19 3.60 10.20 -2 0 19 -10.40 11.90 19 -1 -19 15.70 13.40 19 1 -19 -5.10 13.00 17 -1 -19 -11.50 15.20 17 1 -19 -0.10 13.50 15 -1 -19 -10.10 12.00 15 1 -19 -5.20 12.10 13 -1 -19 -2.90 11.30 13 1 -19 12.70 11.90 11 -1 -19 23.40 11.50 11 1 -19 8.50 10.60 9 -1 -19 56.09 12.30 9 1 -19 60.29 12.30 7 1 -19 3.70 9.90 20 -2 -19 -4.40 12.90 20 2 -19 19.90 15.80 18 -2 -19 -17.60 12.20 18 2 -19 -1.40 13.50 16 -2 -19 25.20 12.70 14 -2 -19 -7.70 11.30 14 2 -19 1.30 12.30 12 -2 -19 1.30 10.80 12 2 -19 -6.00 10.60 10 2 -19 13.30 10.90 8 2 -19 -5.40 9.90 6 2 -19 17.30 10.10 -2 2 19 -0.50 12.00 19 -3 -19 5.50 12.30 19 3 -19 -6.10 13.90 17 -3 -19 11.20 12.20 17 3 -19 -3.20 12.90 15 -3 -19 1.00 12.20 15 3 -19 -2.30 17.20 13 -3 -19 -4.00 10.90 13 3 -19 -3.00 12.10 11 -3 -19 -16.30 9.80 11 3 -19 -22.70 10.40 9 3 -19 -11.40 9.90 7 3 -19 -0.80 9.60 5 3 -19 -7.50 9.30 18 4 -19 -0.40 13.50 16 -4 -19 61.19 14.40 16 4 -19 48.60 14.60 14 -4 -19 8.30 11.20 14 4 -19 16.90 14.70 12 -4 -19 4.50 10.30 12 4 -19 -18.60 11.40 10 4 -19 -9.30 10.40 8 4 -19 5.80 10.30 6 4 -19 24.80 11.00 4 4 -19 26.30 11.00 19 -5 -19 15.70 11.90 19 5 -19 -4.40 14.00 17 -5 -19 12.30 11.90 17 5 -19 4.80 13.30 15 -5 -19 26.30 11.60 15 5 -19 -2.40 11.90 13 -5 -19 5.60 9.80 13 5 -19 -9.00 12.60 11 5 -19 -10.30 11.60 9 5 -19 29.80 12.80 7 5 -19 62.69 12.80 5 5 -19 -2.60 9.70 5 5 -19 -4.30 10.00 -3 5 19 -1.50 12.50 3 5 -19 -11.00 9.90 3 5 -19 -2.40 10.00 18 -6 -19 11.50 14.00 18 6 -19 8.80 14.40 16 -6 -19 17.50 11.70 16 6 -19 11.80 13.90 14 -6 -19 17.50 10.40 14 6 -19 -18.20 11.90 12 6 -19 -19.20 15.80 10 6 -19 5.30 12.20 8 6 -19 22.10 11.70 6 6 -19 8.20 11.00 6 6 -19 -1.10 10.10 4 6 -19 -2.80 10.40 17 -7 -19 7.50 10.90 17 7 -19 -2.20 13.70 15 -7 -19 1.30 9.40 15 7 -19 -5.50 12.70 13 -7 -19 -2.70 9.40 13 7 -19 0.50 11.70 9 7 -19 61.69 13.60 9 7 -19 80.79 14.60 7 7 -19 23.00 11.70 7 7 -19 15.90 11.40 5 7 -19 -4.30 10.60 5 7 -19 -23.10 10.00 16 -8 -19 33.60 12.30 16 8 -19 14.60 14.70 14 -8 -19 9.90 9.70 14 8 -19 13.90 13.20 12 8 -19 18.20 12.80 10 8 -19 -21.10 10.20 10 8 -19 15.70 14.10 8 8 -19 -7.50 10.70 8 8 -19 -2.20 13.30 6 8 -19 2.60 11.30 6 8 -19 -17.20 10.80 13 9 -19 17.50 13.20 11 9 -19 5.90 12.50 11 9 -19 10.60 11.70 9 9 -19 4.30 11.70 9 9 -19 -2.40 11.30 7 9 -19 10.10 17.10 7 9 -19 -1.60 11.20 14 0 -20 29.10 13.00 12 0 -20 14.70 11.60 10 0 -20 23.50 12.40 15 -1 -20 5.20 12.70 15 1 -20 10.60 13.70 13 -1 -20 -6.00 11.10 13 1 -20 31.80 12.60 11 -1 -20 6.00 11.40 11 1 -20 14.00 11.30 9 1 -20 -14.80 10.50 14 -2 -20 -0.20 11.50 14 2 -20 0.60 12.60 12 -2 -20 -8.20 10.10 12 2 -20 11.80 11.80 10 2 -20 5.30 10.60 8 2 -20 -7.80 10.50 15 -3 -20 15.40 11.90 15 3 -20 -2.00 12.00 13 -3 -20 0.00 10.60 13 3 -20 2.20 11.90 11 3 -20 2.10 11.10 9 3 -20 -1.30 10.70 14 4 -20 -10.70 11.90 12 -4 -20 8.10 11.00 12 4 -20 -14.80 11.60 10 4 -20 19.70 11.60 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 25266 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.5000 0.17372(3) 0.2500 0.0429(3) Uani 1 2 d S T P . . Fe2 Fe 0.58195(3) 0.32778(3) 0.49868(4) 0.0499(2) Uani 1 1 d . . . . . N1 N 0.58696(16) 0.16710(15) 0.2350(2) 0.0493(9) Uani 1 1 d . . . . . N2 N 0.54822(16) 0.09920(16) 0.3398(3) 0.0546(10) Uani 1 1 d . . . . . N3 N 0.53579(15) 0.23651(16) 0.3492(3) 0.0544(10) Uani 1 1 d . . . . . N4 N 0.6586(2) 0.2225(2) 0.6019(4) 0.0830(14) Uani 1 1 d . . . . . N5 N 0.4665(2) 0.2836(3) 0.5245(4) 0.0984(18) Uani 1 1 d . . . . . N6 N 0.65350(14) 0.35729(15) 0.4727(2) 0.0482(9) Uani 1 1 d . . . . . N7 N 0.66939(15) 0.41605(15) 0.4904(2) 0.0500(9) Uani 1 1 d . . . . . N8 N 0.53563(15) 0.39744(16) 0.4309(3) 0.0547(10) Uani 1 1 d . . . . . N9 N 0.56309(16) 0.45180(15) 0.4551(3) 0.0521(9) Uani 1 1 d . . . . . N10 N 0.60994(17) 0.37455(17) 0.6128(3) 0.0574(10) Uani 1 1 d . . . . . N11 N 0.63404(16) 0.43032(16) 0.6126(3) 0.0560(10) Uani 1 1 d . . . . . N12 N 0.5681(2) -0.00746(18) 0.4767(3) 0.102(2) Uani 0.5 1 d . . . A 4 C9 C 0.56732(17) 0.05339(17) 0.4906(2) 0.0776(17) Uani 1 1 d G . . . . C10 C 0.6021(2) 0.07724(18) 0.5744(3) 0.113(3) Uani 1 1 d G . . . . H10 H 0.6015 0.1180 0.5837 0.136 Uiso 1 1 calc R . . . . C11 C 0.6376(2) 0.0402(3) 0.6442(3) 0.143(4) Uani 1 1 d G . . . . H11 H 0.6609 0.0562 0.7003 0.171 Uiso 1 1 calc R . . . . C12 C 0.6384(2) -0.0206(2) 0.6303(3) 0.127(3) Uani 1 1 d G . . . . H12 H 0.6622 -0.0454 0.6770 0.152 Uiso 1 1 calc R . . . . C13 C 0.6037(2) -0.04447(17) 0.5465(4) 0.127(3) Uani 1 1 d G . . . . H13A H 0.6042 -0.0852 0.5372 0.152 Uiso 0.5 1 calc R . . A 4 H13 H 0.6042 -0.0852 0.5372 0.152 Uiso 0.5 1 calc R . . A 3 C1 C 0.6015(2) 0.1923(2) 0.1728(3) 0.0585(12) Uani 1 1 d . . . . . H1 H 0.5700 0.2103 0.1247 0.070 Uiso 1 1 calc R . . . . C2 C 0.6607(3) 0.1935(3) 0.1748(4) 0.0716(14) Uani 1 1 d . . . . . H2 H 0.6689 0.2122 0.1296 0.086 Uiso 1 1 calc R . . . . C3 C 0.7075(2) 0.1666(2) 0.2449(4) 0.0686(14) Uani 1 1 d . . . . . H3 H 0.7481 0.1672 0.2487 0.082 Uiso 1 1 calc R . . . . C4 C 0.6927(2) 0.1387(2) 0.3099(3) 0.0607(13) Uani 1 1 d . . . . . H4 H 0.7233 0.1193 0.3575 0.073 Uiso 1 1 calc R . . . . C5 C 0.63240(18) 0.13986(19) 0.3037(3) 0.0511(11) Uani 1 1 d . . . . . C6 C 0.61488(18) 0.1137(2) 0.3739(3) 0.0570(12) Uani 1 1 d . . . . . H6A H 0.6389 0.0778 0.3966 0.068 Uiso 1 1 calc R . . . . H6B H 0.6249 0.1415 0.4232 0.068 Uiso 1 1 calc R . . . . C7 C 0.5338(2) 0.0465(2) 0.2817(4) 0.0667(14) Uani 1 1 d . . . . . H7A H 0.5429 0.0109 0.3182 0.080 Uiso 1 1 calc R . . . . H7B H 0.5597 0.0463 0.2475 0.080 Uiso 1 1 calc R . . . . C8 C 0.5285(2) 0.0928(2) 0.4155(4) 0.0700(15) Uani 1 1 d . . . . . H8A H 0.4864 0.0777 0.3920 0.084 Uiso 1 1 calc R . . . . H8B H 0.5277 0.1320 0.4397 0.084 Uiso 1 1 calc R . . . . C12A C 0.5681(2) -0.00746(18) 0.4767(3) 0.102(2) Uani 0.5 1 d . . . A 3 H12A H 0.5449 -0.0234 0.4207 0.122 Uiso 0.5 1 calc R . . A 3 C14 C 0.55392(18) 0.2732(2) 0.4019(3) 0.0504(11) Uani 1 1 d . . . . . C15 C 0.6300(2) 0.2611(2) 0.5641(3) 0.0592(12) Uani 1 1 d . . . . . C16 C 0.5106(2) 0.2997(2) 0.5176(4) 0.0664(14) Uani 1 1 d . . . . . C17 C 0.69184(18) 0.33469(19) 0.4368(3) 0.0496(11) Uani 1 1 d . . . . . C18 C 0.73170(19) 0.3787(2) 0.4335(3) 0.0568(12) Uani 1 1 d . . . . . H18 H 0.7631 0.3747 0.4126 0.068 Uiso 1 1 calc R . . . . C19 C 0.71662(19) 0.42956(19) 0.4668(3) 0.0500(11) Uani 1 1 d . . . . . C20 C 0.6881(2) 0.2724(2) 0.4046(3) 0.0604(13) Uani 1 1 d . . . . . H20A H 0.6826 0.2461 0.4474 0.091 Uiso 1 1 calc GR . . . . H20B H 0.7257 0.2623 0.3976 0.091 Uiso 1 1 calc GR . . . . H20C H 0.6536 0.2685 0.3481 0.091 Uiso 1 1 calc GR . . . . C21 C 0.7451(2) 0.4891(2) 0.4805(4) 0.0657(13) Uani 1 1 d . . . . . H21A H 0.7143 0.5179 0.4475 0.099 Uiso 1 1 calc GR . . . . H21B H 0.7782 0.4894 0.4599 0.099 Uiso 1 1 calc GR . . . . H21C H 0.7612 0.4989 0.5431 0.099 Uiso 1 1 calc GR . . . . C22 C 0.48159(19) 0.4066(2) 0.3605(3) 0.0590(13) Uani 1 1 d . . . . . C23 C 0.4748(2) 0.4659(2) 0.3416(4) 0.0666(14) Uani 1 1 d . . . . . H23 H 0.4413 0.4840 0.2965 0.080 Uiso 1 1 calc R . . . . C24 C 0.5266(2) 0.4941(2) 0.4015(3) 0.0594(12) Uani 1 1 d . . . . . C25 C 0.4369(2) 0.3579(3) 0.3128(4) 0.087(2) Uani 1 1 d . . . . . H25A H 0.4581 0.3282 0.2931 0.131 Uiso 1 1 calc GR . . . . H25B H 0.4035 0.3741 0.2620 0.131 Uiso 1 1 calc GR . . . . H25C H 0.4207 0.3402 0.3529 0.131 Uiso 1 1 calc GR . . . . C26 C 0.5427(3) 0.5582(2) 0.4113(4) 0.0795(17) Uani 1 1 d . . . . . H26A H 0.5509 0.5706 0.4714 0.119 Uiso 1 1 calc GR . . . . H26B H 0.5088 0.5808 0.3701 0.119 Uiso 1 1 calc GR . . . . H26C H 0.5790 0.5646 0.3988 0.119 Uiso 1 1 calc GR . . . . C27 C 0.6176(2) 0.3633(2) 0.6975(4) 0.0680(14) Uani 1 1 d . . . . . C28 C 0.6473(2) 0.4113(3) 0.7513(4) 0.0705(15) Uani 1 1 d . . . . . H28 H 0.6582 0.4149 0.8126 0.085 Uiso 1 1 calc R . . . . C29 C 0.6571(2) 0.4519(2) 0.6962(4) 0.0639(14) Uani 1 1 d . . . . . C30 C 0.5962(3) 0.3084(3) 0.7291(5) 0.097(2) Uani 1 1 d . . . . . H30A H 0.5519 0.3054 0.7001 0.146 Uiso 1 1 calc GR . . . . H30B H 0.6082 0.3105 0.7928 0.146 Uiso 1 1 calc GR . . . . H30C H 0.6148 0.2741 0.7148 0.146 Uiso 1 1 calc GR . . . . C31 C 0.6871(3) 0.5122(3) 0.7165(4) 0.0850(18) Uani 1 1 d . . . . . H31A H 0.6566 0.5422 0.6881 0.127 Uiso 1 1 calc GR . . . . H31B H 0.7194 0.5144 0.6943 0.127 Uiso 1 1 calc GR . . . . H31C H 0.7045 0.5186 0.7800 0.127 Uiso 1 1 calc GR . . . . B1 B 0.6300(2) 0.4553(2) 0.5247(4) 0.0539(13) Uani 1 1 d . . . . . H1A H 0.6481 0.5052 0.5337 0.065 Uiso 1 1 calc R . . . . O1 O 0.7071(10) 0.1583(8) 0.7723(12) 0.212(7) Uani 0.5 1 d D U . . . H1B H 0.6909 0.1757 0.7243 0.317 Uiso 0.5 1 d R . . . . C32 C 0.7724(11) 0.1621(12) 0.802(2) 0.227(11) Uani 0.5 1 d D U . . . H32A H 0.7889 0.1817 0.8592 0.341 Uiso 0.5 1 d R . . . . H32B H 0.7828 0.1844 0.7597 0.341 Uiso 0.5 1 d R . . . . H32C H 0.7898 0.1230 0.8080 0.341 Uiso 0.5 1 d R . . . . O2 O 0.3321(14) 0.3283(17) 0.502(2) 0.179(8) Uani 0.242(9) 1 d D U . B 1 H2A H 0.3506 0.3351 0.5581 0.268 Uiso 0.242(9) 1 d R . . B 1 H2B H 0.3523 0.2998 0.4925 0.268 Uiso 0.242(9) 1 d R . . B 1 O3 O 0.2500(15) 0.3279(13) 0.533(2) 0.386(17) Uani 0.5 1 d . U . . . H3A H 0.2782 0.3037 0.5289 0.578 Uiso 0.5 1 d DR . . . . H3B H 0.2285 0.3443 0.4802 0.578 Uiso 0.5 1 d R . . . . O4 O 0.4237(15) 0.1747(11) 0.596(2) 0.351(14) Uani 0.5 1 d . U . . . H4A H 0.4173 0.2126 0.5808 0.526 Uiso 0.5 1 d R . . . . H4B H 0.4634 0.1664 0.6133 0.526 Uiso 0.5 1 d R . . . . O2A O 0.3466(13) 0.2681(16) 0.5281(19) 0.179(8) Uani 0.258(9) 1 d . . . B 2 H2AA H 0.3423 0.2617 0.5768 0.268 Uiso 0.258(9) 1 d R . . B 2 H2AB H 0.3830 0.2560 0.5380 0.268 Uiso 0.258(9) 1 d R . . B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.0319(4) 0.0374(4) 0.0470(5) 0.000 0.0024(3) 0.000 Fe2 0.0364(3) 0.0465(4) 0.0587(4) -0.0081(3) 0.0101(3) 0.0016(2) N1 0.0468(19) 0.046(2) 0.047(2) -0.0010(17) 0.0095(16) 0.0015(15) N2 0.0387(18) 0.052(2) 0.060(2) 0.0077(18) 0.0064(17) -0.0005(15) N3 0.0375(18) 0.048(2) 0.062(2) -0.0101(19) 0.0028(16) 0.0008(15) N4 0.074(3) 0.075(3) 0.098(4) 0.017(3) 0.031(3) 0.017(2) N5 0.070(3) 0.115(4) 0.122(5) -0.024(4) 0.051(3) -0.027(3) N6 0.0359(17) 0.0465(19) 0.053(2) -0.0048(16) 0.0074(16) 0.0025(15) N7 0.0387(18) 0.0448(19) 0.058(2) -0.0072(17) 0.0104(16) 0.0028(15) N8 0.0401(18) 0.050(2) 0.063(2) -0.0120(18) 0.0093(17) 0.0041(15) N9 0.0411(18) 0.0458(19) 0.063(2) -0.0056(18) 0.0141(17) 0.0066(15) N10 0.050(2) 0.058(2) 0.059(3) -0.0066(19) 0.0162(18) -0.0005(17) N11 0.0441(19) 0.051(2) 0.063(3) -0.0120(19) 0.0104(17) 0.0010(16) N12 0.098(4) 0.097(4) 0.113(5) 0.044(4) 0.044(4) 0.016(3) C9 0.055(3) 0.086(4) 0.091(4) 0.030(3) 0.028(3) -0.002(3) C10 0.091(4) 0.109(5) 0.096(5) 0.045(4) -0.011(4) -0.014(4) C11 0.102(6) 0.159(8) 0.115(6) 0.055(6) -0.012(5) -0.013(5) C12 0.083(5) 0.148(8) 0.144(8) 0.086(7) 0.039(5) 0.006(5) C13 0.105(6) 0.119(6) 0.168(9) 0.074(6) 0.065(6) 0.028(5) C1 0.058(3) 0.051(3) 0.060(3) 0.001(2) 0.016(2) 0.004(2) C2 0.070(3) 0.076(3) 0.074(4) 0.000(3) 0.035(3) -0.001(3) C3 0.052(3) 0.076(3) 0.077(4) -0.003(3) 0.025(3) 0.006(2) C4 0.044(2) 0.062(3) 0.065(3) -0.009(2) 0.009(2) 0.012(2) C5 0.040(2) 0.047(2) 0.053(3) -0.003(2) 0.0047(19) 0.0032(18) C6 0.038(2) 0.061(3) 0.057(3) 0.006(2) 0.002(2) 0.0051(19) C7 0.059(3) 0.041(2) 0.079(3) 0.003(2) 0.003(2) 0.003(2) C8 0.052(3) 0.074(3) 0.072(3) 0.023(3) 0.010(2) 0.002(2) C12A 0.098(4) 0.097(4) 0.113(5) 0.044(4) 0.044(4) 0.016(3) C14 0.0312(19) 0.050(2) 0.062(3) 0.001(2) 0.0100(19) 0.0048(18) C15 0.046(2) 0.056(3) 0.069(3) -0.004(2) 0.016(2) 0.003(2) C16 0.061(3) 0.064(3) 0.071(3) -0.014(3) 0.023(3) 0.000(2) C17 0.036(2) 0.056(3) 0.048(2) -0.005(2) 0.0067(18) 0.0037(18) C18 0.041(2) 0.069(3) 0.057(3) 0.001(2) 0.015(2) 0.002(2) C19 0.040(2) 0.052(2) 0.049(3) 0.003(2) 0.0089(19) 0.0031(18) C20 0.043(2) 0.060(3) 0.070(3) -0.017(2) 0.013(2) 0.006(2) C21 0.061(3) 0.061(3) 0.074(3) 0.005(3) 0.026(3) -0.004(2) C22 0.036(2) 0.065(3) 0.062(3) -0.007(2) 0.005(2) 0.012(2) C23 0.046(2) 0.071(3) 0.070(3) 0.001(3) 0.010(2) 0.020(2) C24 0.051(3) 0.058(3) 0.070(3) 0.005(2) 0.025(2) 0.017(2) C25 0.041(2) 0.086(4) 0.099(4) -0.026(3) -0.011(3) 0.010(2) C26 0.078(4) 0.060(3) 0.098(4) 0.015(3) 0.031(3) 0.015(3) C27 0.060(3) 0.074(3) 0.066(3) -0.001(3) 0.020(3) 0.012(3) C28 0.061(3) 0.084(4) 0.059(3) -0.014(3) 0.016(3) 0.009(3) C29 0.046(2) 0.074(3) 0.061(3) -0.026(3) 0.009(2) 0.003(2) C30 0.118(5) 0.089(4) 0.084(4) 0.005(4) 0.039(4) -0.001(4) C31 0.069(3) 0.082(4) 0.085(4) -0.035(3) 0.010(3) -0.012(3) B1 0.042(2) 0.047(3) 0.067(4) -0.011(3) 0.015(2) 0.004(2) O1 0.255(14) 0.205(12) 0.167(11) 0.047(10) 0.074(11) -0.004(12) C32 0.237(16) 0.178(16) 0.237(18) 0.002(14) 0.061(15) -0.005(15) O2 0.149(13) 0.214(17) 0.173(14) -0.015(14) 0.062(11) -0.060(14) O3 0.39(2) 0.41(2) 0.36(2) 0.018(17) 0.153(18) -0.023(17) O4 0.40(2) 0.297(19) 0.36(2) -0.036(15) 0.154(17) -0.103(16) O2A 0.149(13) 0.214(17) 0.173(14) -0.015(14) 0.062(11) -0.060(14) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Fe1 N1 172.06(18) . 2_655 ? N1 Fe1 N2 76.25(14) 2_655 2_655 ? N1 Fe1 N2 76.25(14) . . ? N1 Fe1 N2 97.65(14) 2_655 . ? N1 Fe1 N2 97.65(14) . 2_655 ? N2 Fe1 N2 81.77(19) . 2_655 ? N3 Fe1 N1 94.06(14) 2_655 . ? N3 Fe1 N1 94.06(14) . 2_655 ? N3 Fe1 N1 91.39(14) 2_655 2_655 ? N3 Fe1 N1 91.39(14) . . ? N3 Fe1 N2 168.37(16) . 2_655 ? N3 Fe1 N2 93.37(14) 2_655 2_655 ? N3 Fe1 N2 93.37(14) . . ? N3 Fe1 N2 168.37(16) 2_655 . ? N3 Fe1 N3 93.3(2) . 2_655 ? N6 Fe2 N10 91.44(15) . . ? N8 Fe2 N6 86.64(15) . . ? N8 Fe2 N10 90.39(15) . . ? C14 Fe2 N6 94.89(17) . . ? C14 Fe2 N8 96.68(16) . . ? C14 Fe2 N10 170.76(19) . . ? C14 Fe2 C15 83.67(19) . . ? C14 Fe2 C16 83.2(2) . . ? C15 Fe2 N6 91.05(18) . . ? C15 Fe2 N8 177.69(18) . . ? C15 Fe2 N10 89.50(18) . . ? C16 Fe2 N6 177.21(19) . . ? C16 Fe2 N8 91.6(2) . . ? C16 Fe2 N10 90.73(19) . . ? C16 Fe2 C15 90.7(2) . . ? C1 N1 Fe1 126.9(3) . . ? C1 N1 C5 118.2(4) . . ? C5 N1 Fe1 114.4(3) . . ? C6 N2 Fe1 105.7(3) . . ? C6 N2 C8 110.0(4) . . ? C7 N2 Fe1 105.0(3) . . ? C7 N2 C6 111.1(4) . . ? C7 N2 C8 112.8(4) . . ? C8 N2 Fe1 112.0(3) . . ? C14 N3 Fe1 176.9(4) . . ? N7 N6 Fe2 117.2(3) . . ? C17 N6 Fe2 136.4(3) . . ? C17 N6 N7 106.4(3) . . ? N6 N7 B1 118.5(4) . . ? C19 N7 N6 110.2(3) . . ? C19 N7 B1 131.1(4) . . ? N9 N8 Fe2 117.2(2) . . ? C22 N8 Fe2 136.2(3) . . ? C22 N8 N9 106.6(4) . . ? N8 N9 B1 119.2(3) . . ? C24 N9 N8 109.9(3) . . ? C24 N9 B1 130.3(4) . . ? N11 N10 Fe2 117.5(3) . . ? C27 N10 Fe2 135.5(4) . . ? C27 N10 N11 106.6(4) . . ? N10 N11 B1 118.1(4) . . ? C29 N11 N10 109.3(4) . . ? C29 N11 B1 132.6(4) . . ? C9 N12 C13 120.0 . . ? N12 C9 C10 120.0 . . ? N12 C9 C8 119.7(4) . . ? C10 C9 C8 120.3(4) . . ? C12A C9 C10 120.0 . . ? C12A C9 C8 119.7(4) . . ? C9 C10 H10 120.0 . . ? C11 C10 C9 120.0 . . ? C11 C10 H10 120.0 . . ? C10 C11 H11 120.0 . . ? C12 C11 C10 120.0 . . ? C12 C11 H11 120.0 . . ? C11 C12 H12 120.0 . . ? C11 C12 C13 120.0 . . ? C13 C12 H12 120.0 . . ? N12 C13 H13A 120.0 . . ? C12 C13 N12 120.0 . . ? C12 C13 H13A 120.0 . . ? C12 C13 H13 120.0 . . ? C12 C13 C12A 120.0 . . ? C12A C13 H13 120.0 . . ? N1 C1 H1 118.2 . . ? N1 C1 C2 123.6(5) . . ? C2 C1 H1 118.2 . . ? C1 C2 H2 120.7 . . ? C3 C2 C1 118.7(5) . . ? C3 C2 H2 120.7 . . ? C2 C3 H3 120.8 . . ? C2 C3 C4 118.4(5) . . ? C4 C3 H3 120.8 . . ? C3 C4 H4 120.2 . . ? C5 C4 C3 119.5(4) . . ? C5 C4 H4 120.2 . . ? N1 C5 C4 121.5(5) . . ? N1 C5 C6 116.8(4) . . ? C4 C5 C6 121.6(4) . . ? N2 C6 C5 112.0(3) . . ? N2 C6 H6A 109.2 . . ? N2 C6 H6B 109.2 . . ? C5 C6 H6A 109.2 . . ? C5 C6 H6B 109.2 . . ? H6A C6 H6B 107.9 . . ? N2 C7 C7 110.5(4) . 2_655 ? N2 C7 H7A 109.5 . . ? N2 C7 H7B 109.5 . . ? C7 C7 H7A 109.5 2_655 . ? C7 C7 H7B 109.5 2_655 . ? H7A C7 H7B 108.1 . . ? N2 C8 C9 116.6(4) . . ? N2 C8 H8A 108.2 . . ? N2 C8 H8B 108.2 . . ? C9 C8 H8A 108.2 . . ? C9 C8 H8B 108.2 . . ? H8A C8 H8B 107.3 . . ? C9 C12A C13 120.0 . . ? C9 C12A H12A 120.0 . . ? C13 C12A H12A 120.0 . . ? N3 C14 Fe2 173.1(5) . . ? N4 C15 Fe2 179.1(5) . . ? N5 C16 Fe2 176.6(5) . . ? N6 C17 C18 108.9(4) . . ? N6 C17 C20 123.4(4) . . ? C18 C17 C20 127.7(5) . . ? C17 C18 H18 126.2 . . ? C19 C18 C17 107.5(4) . . ? C19 C18 H18 126.2 . . ? N7 C19 C18 107.1(4) . . ? N7 C19 C21 122.5(4) . . ? C18 C19 C21 130.3(5) . . ? C17 C20 H20A 109.5 . . ? C17 C20 H20B 109.5 . . ? C17 C20 H20C 109.5 . . ? H20A C20 H20B 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C19 C21 H21A 109.5 . . ? C19 C21 H21B 109.5 . . ? C19 C21 H21C 109.5 . . ? H21A C21 H21B 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? N8 C22 C23 109.2(4) . . ? N8 C22 C25 123.8(4) . . ? C23 C22 C25 127.0(4) . . ? C22 C23 H23 126.3 . . ? C22 C23 C24 107.4(4) . . ? C24 C23 H23 126.3 . . ? N9 C24 C23 106.9(4) . . ? N9 C24 C26 123.2(4) . . ? C23 C24 C26 129.8(5) . . ? C22 C25 H25A 109.5 . . ? C22 C25 H25B 109.5 . . ? C22 C25 H25C 109.5 . . ? H25A C25 H25B 109.5 . . ? H25A C25 H25C 109.5 . . ? H25B C25 H25C 109.5 . . ? C24 C26 H26A 109.5 . . ? C24 C26 H26B 109.5 . . ? C24 C26 H26C 109.5 . . ? H26A C26 H26B 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? N10 C27 C28 109.3(5) . . ? N10 C27 C30 125.4(5) . . ? C28 C27 C30 125.2(6) . . ? C27 C28 H28 126.9 . . ? C29 C28 C27 106.3(5) . . ? C29 C28 H28 126.9 . . ? N11 C29 C28 108.5(5) . . ? N11 C29 C31 121.1(5) . . ? C28 C29 C31 130.4(5) . . ? C27 C30 H30A 109.5 . . ? C27 C30 H30B 109.5 . . ? C27 C30 H30C 109.5 . . ? H30A C30 H30B 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C29 C31 H31A 109.5 . . ? C29 C31 H31B 109.5 . . ? C29 C31 H31C 109.5 . . ? H31A C31 H31B 109.5 . . ? H31A C31 H31C 109.5 . . ? H31B C31 H31C 109.5 . . ? N7 B1 H1A 110.5 . . ? N9 B1 N7 106.9(4) . . ? N9 B1 H1A 110.5 . . ? N11 B1 N7 108.0(4) . . ? N11 B1 N9 110.3(4) . . ? N11 B1 H1A 110.5 . . ? C32 O1 H1B 109.2 . . ? O1 C32 H32A 109.2 . . ? O1 C32 H32B 109.5 . . ? O1 C32 H32C 109.8 . . ? H32A C32 H32B 109.5 . . ? H32A C32 H32C 109.4 . . ? H32B C32 H32C 109.5 . . ? H2A O2 H2B 104.5 . . ? H3A O3 H3B 109.3 . . ? H4A O4 H4B 109.8 . . ? H2AA O2A H2AB 104.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 N1 2.153(4) . ? Fe1 N1 2.153(4) 2_655 ? Fe1 N2 2.219(4) 2_655 ? Fe1 N2 2.219(4) . ? Fe1 N3 2.059(4) . ? Fe1 N3 2.059(4) 2_655 ? Fe2 N6 2.000(4) . ? Fe2 N8 1.978(4) . ? Fe2 N10 2.006(4) . ? Fe2 C14 1.897(5) . ? Fe2 C15 1.927(5) . ? Fe2 C16 1.924(6) . ? N1 C1 1.316(6) . ? N1 C5 1.350(5) . ? N2 C6 1.475(5) . ? N2 C7 1.471(6) . ? N2 C8 1.481(7) . ? N3 C14 1.145(6) . ? N4 C15 1.122(6) . ? N5 C16 1.144(7) . ? N6 N7 1.374(5) . ? N6 C17 1.350(6) . ? N7 C19 1.342(6) . ? N7 B1 1.534(6) . ? N8 N9 1.367(5) . ? N8 C22 1.347(5) . ? N9 C24 1.346(6) . ? N9 B1 1.533(6) . ? N10 N11 1.378(5) . ? N10 C27 1.340(7) . ? N11 C29 1.341(6) . ? N11 B1 1.502(7) . ? N12 C9 1.3900 . ? N12 C13 1.3900 . ? C9 C10 1.3900 . ? C9 C8 1.494(5) . ? C9 C12A 1.3900 . ? C10 H10 0.9300 . ? C10 C11 1.3900 . ? C11 H11 0.9300 . ? C11 C12 1.3900 . ? C12 H12 0.9300 . ? C12 C13 1.3900 . ? C13 H13A 0.9300 . ? C13 H13 0.9300 . ? C13 C12A 1.3900 . ? C1 H1 0.9300 . ? C1 C2 1.378(7) . ? C2 H2 0.9300 . ? C2 C3 1.372(7) . ? C3 H3 0.9300 . ? C3 C4 1.386(7) . ? C4 H4 0.9300 . ? C4 C5 1.379(6) . ? C5 C6 1.480(7) . ? C6 H6A 0.9700 . ? C6 H6B 0.9700 . ? C7 C7 1.515(9) 2_655 ? C7 H7A 0.9700 . ? C7 H7B 0.9700 . ? C8 H8A 0.9700 . ? C8 H8B 0.9700 . ? C12A H12A 0.9300 . ? C17 C18 1.378(6) . ? C17 C20 1.488(6) . ? C18 H18 0.9300 . ? C18 C19 1.371(6) . ? C19 C21 1.475(6) . ? C20 H20A 0.9600 . ? C20 H20B 0.9600 . ? C20 H20C 0.9600 . ? C21 H21A 0.9600 . ? C21 H21B 0.9600 . ? C21 H21C 0.9600 . ? C22 C23 1.365(7) . ? C22 C25 1.505(7) . ? C23 H23 0.9300 . ? C23 C24 1.376(7) . ? C24 C26 1.485(7) . ? C25 H25A 0.9600 . ? C25 H25B 0.9600 . ? C25 H25C 0.9600 . ? C26 H26A 0.9600 . ? C26 H26B 0.9600 . ? C26 H26C 0.9600 . ? C27 C28 1.392(7) . ? C27 C30 1.501(8) . ? C28 H28 0.9300 . ? C28 C29 1.361(8) . ? C29 C31 1.505(7) . ? C30 H30A 0.9600 . ? C30 H30B 0.9600 . ? C30 H30C 0.9600 . ? C31 H31A 0.9600 . ? C31 H31B 0.9600 . ? C31 H31C 0.9600 . ? B1 H1A 1.1900 . ? O1 H1B 0.8198 . ? O1 C32 1.416(10) . ? C32 H32A 0.9606 . ? C32 H32B 0.9599 . ? C32 H32C 0.9600 . ? O2 H2A 0.8501 . ? O2 H2B 0.8500 . ? O3 H3A 0.8813 . ? O3 H3B 0.8917 . ? O4 H4A 0.8841 . ? O4 H4B 0.8804 . ? O2A H2AA 0.8500 . ? O2A H2AB 0.8499 . ?