Crystallography Open Database

Information card for entry 7708380

Preview

Coordinates	7708380.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C70 H109 O10 Tm
Calculated formula	C70 H109 O10 Tm
Title of publication	New lanthanoid biphenolate complexes, their further reactivity with trimethylaluminium and catalytic activity for the polymerisation of rac-lactide
Authors of publication	Shephard, Angus; Ali, Safaa; Wang, Jun; Guo, Zhifang; Davies, Murray S.; Deacon, Glen B.; Junk, Peter Courtney
Journal of publication	Dalton Transactions
Year of publication	2021
a	13.2 ± 0.003 Å
b	17.53 ± 0.004 Å
c	28.42 ± 0.006 Å
α	90°
β	93.32 ± 0.03°
γ	90°
Cell volume	6565 ± 3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0512
Residual factor for significantly intense reflections	0.0463
Weighted residual factors for significantly intense reflections	0.1228
Weighted residual factors for all reflections included in the refinement	0.1271
Goodness-of-fit parameter for all reflections included in the refinement	1.05
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	Synchrotron
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
269230 (current)	2021-09-22	cif/ Adding structures of 7708372, 7708373, 7708374, 7708375, 7708376, 7708377, 7708378, 7708379, 7708380, 7708381, 7708382 via cif-deposit CGI script.	7708380.cif