Crystallography Open Database

Information card for entry 7709068

Preview

Coordinates	7709068.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	(1,1,2,2,2,3-hexacarbonyl)-(1-?5-cyclopentadienyl)-?3-[1,2-?1,?1,3-?2-(phenyl)ethenylidene]-(tri-ethyl phosphite-3κP)–rhenium–iron–platinum(Fe–Re, Fe–Pt)
Formula	C30 H41 Fe O11 P2 Pt Re
Calculated formula	C30 H36 Fe O11 P2 Pt Re
Title of publication	Trinuclear ReFePt clusters with a μ<sub>3</sub>-phenylvinylidene ligand: synthetic approaches, rearrangement of vinylidene, and redox-induced transformations.
Authors of publication	Verpekin, Victor V.; Chudin, Oleg S.; Vasiliev, Alexander D.; Kondrasenko, Alexander A.; Shor, Aleksey M.; Burmakina, Galina V.; Zimonin, Dmitry V.; Maksimov, Nikolai G.; Rubaylo, Anatoly I.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	51
Journal issue	1
Pages of publication	324 - 339
a	11.753 ± 0.0003 Å
b	20.1543 ± 0.0005 Å
c	16.4212 ± 0.0004 Å
α	90°
β	106.649 ± 0.001°
γ	90°
Cell volume	3726.68 ± 0.16 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0738
Residual factor for significantly intense reflections	0.0466
Weighted residual factors for significantly intense reflections	0.1026
Weighted residual factors for all reflections included in the refinement	0.1137
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
272642 (current)	2022-02-04	cif/ Updating files of 7709067, 7709068 Original log message: Adding full bibliography for 7709067--7709068.cif.	7709068.cif
271370	2021-12-14	cif/ Adding structures of 7709067, 7709068 via cif-deposit CGI script.	7709068.cif