#------------------------------------------------------------------------------ #$Date: 2022-02-04 21:37:57 +0200 (Fri, 04 Feb 2022) $ #$Revision: 272668 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/91/7709189.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7709189 loop_ _publ_author_name 'M\"uller, Felix' 'Wickemeyer, Lucas' 'Schwabedissen, Jan' 'Ertl, Martin' 'Neumann, Beate' 'Stammler, Hans-Georg' 'Monkowius, Uwe' 'Mitzel, Norbert W.' _publ_section_title ; Synthesis, structural and photophysical properties of dimethylphosphino(perfluoro-)phenylene-based gold(I) dimers. ; _journal_issue 5 _journal_name_full 'Dalton transactions (Cambridge, England : 2003)' _journal_page_first 1955 _journal_page_last 1967 _journal_paper_doi 10.1039/d1dt03658k _journal_volume 51 _journal_year 2022 _chemical_formula_moiety 'C16 H20 Au2 P2, C H2 Cl2' _chemical_formula_sum 'C17 H22 Au2 Cl2 P2' _chemical_formula_weight 753.12 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2021-02-18 _audit_creation_method ; Olex2 1.3-ac4 (compiled 2019.04.23 svn.r3594 for Rigaku Oxford Diffraction, GUI svn.r5739) ; _audit_update_record ; 2021-10-08 deposited with the CCDC. 2021-12-28 downloaded from the CCDC. ; _cell_angle_alpha 87.267(2) _cell_angle_beta 67.328(3) _cell_angle_gamma 68.529(3) _cell_formula_units_Z 2 _cell_length_a 9.1778(3) _cell_length_b 11.0554(3) _cell_length_c 11.4165(3) _cell_measurement_reflns_used 39362 _cell_measurement_temperature 100.01(10) _cell_measurement_theta_max 31.9280 _cell_measurement_theta_min 1.9380 _cell_volume 988.78(6) _computing_cell_refinement 'CrysAlisPro 1.171.40.82a (Rigaku OD, 2020)' _computing_data_collection 'CrysAlisPro 1.171.40.82a (Rigaku OD, 2020)' _computing_data_reduction 'CrysAlisPro 1.171.40.82a (Rigaku OD, 2020)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.01(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 8.0951 _diffrn_detector_type Eos _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.945 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 6.00 95.00 1.00 5.04 -- 26.03 57.00-150.00 89 2 \w 6.00 95.00 1.00 5.04 -- 26.03 57.00 90.00 89 3 \w -43.00 47.00 1.00 5.04 -- 26.03 -57.00 60.00 90 4 \w 1.00 98.00 1.00 5.04 -- 26.03 38.00 0.00 97 5 \w -4.00 42.00 1.00 5.04 -- 26.03 77.00-180.00 46 6 \w -4.00 42.00 1.00 5.04 -- 26.03 77.00 -60.00 46 7 \w -47.00 70.00 1.00 5.04 -- 26.03 -19.00-180.00 117 8 \w -15.00 68.00 1.00 5.04 -- 26.03 -99.00 0.00 83 9 \w 6.00 95.00 1.00 5.04 -- 26.03 57.00 150.00 89 10 \w -4.00 42.00 1.00 5.04 -- 26.03 77.00 30.00 46 11 \w 37.00 103.00 1.00 5.04 -- 26.03-178.00 -30.00 66 12 \w -15.00 68.00 1.00 5.04 -- 26.03 -99.00-180.00 83 13 \w 1.00 98.00 1.00 5.04 -- 26.03 38.00 -30.00 97 14 \w 39.00 102.00 1.00 5.04 -- 26.03 178.00 0.00 63 15 \w -15.00 68.00 1.00 5.04 -- 26.03 -99.00 60.00 83 16 \w -4.00 42.00 1.00 5.04 -- 26.03 77.00-150.00 46 17 \w -42.00 56.00 1.00 5.04 -- 26.03 -77.00-150.00 98 18 \w -47.00 99.00 1.00 5.04 -- 26.03 0.00-180.00 146 19 \w -47.00 99.00 1.00 5.04 -- 26.03 0.00-150.00 146 20 \w -47.00 99.00 1.00 5.04 -- 26.03 0.00-120.00 146 21 \w -47.00 99.00 1.00 5.04 -- 26.03 0.00 -90.00 146 22 \w -46.00 52.00 1.00 5.04 -- 26.03 -38.00 -60.00 98 23 \w -47.00 99.00 1.00 5.04 -- 26.03 0.00 -30.00 146 24 \w -47.00 95.00 1.00 5.04 -- 26.03 0.00 0.00 142 25 \w -47.00 99.00 1.00 5.04 -- 26.03 0.00 -60.00 146 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Single source at offset/far, Eos' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0096371000 _diffrn_orient_matrix_UB_12 -0.0477725000 _diffrn_orient_matrix_UB_13 -0.0446314000 _diffrn_orient_matrix_UB_21 0.0773861000 _diffrn_orient_matrix_UB_22 0.0049849000 _diffrn_orient_matrix_UB_23 -0.0424524000 _diffrn_orient_matrix_UB_31 0.0457963000 _diffrn_orient_matrix_UB_32 -0.0500301000 _diffrn_orient_matrix_UB_33 0.0281736000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0559 _diffrn_reflns_av_unetI/netI 0.0238 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.945 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 60949 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.945 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 32.312 _diffrn_reflns_theta_min 1.945 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 15.248 _exptl_absorpt_correction_T_max 0.174 _exptl_absorpt_correction_T_min 0.018 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.82a (Rigaku Oxford Diffraction, 2020) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 2.530 _exptl_crystal_description block _exptl_crystal_F_000 692 _exptl_crystal_size_max 0.359 _exptl_crystal_size_mid 0.169 _exptl_crystal_size_min 0.137 _refine_diff_density_max 2.171 _refine_diff_density_min -1.651 _refine_diff_density_rms 0.207 _refine_ls_extinction_coef 0.00185(14) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.171 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 213 _refine_ls_number_reflns 6669 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.171 _refine_ls_R_factor_all 0.0266 _refine_ls_R_factor_gt 0.0255 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0259P)^2^+3.4267P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0624 _refine_ls_wR_factor_ref 0.0629 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6448 _reflns_number_total 6669 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt03658k2.cif _cod_data_source_block compound5 _cod_depositor_comments 'Adding full bibliography for 7709188--7709191.cif.' _cod_original_cell_volume 988.78(5) _cod_database_code 7709189 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula C17H22Au2Cl2P2 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _diffrn_oxdiff_digest_frames ; 018f4e1c27edb10c34a37f8f2b9fdfd79102544cfee ; _diffrn_oxdiff_digest_hkl ; 01f65d96115106008c2b8cb39b3c2f439dd61c ; _reflns_odcompleteness_completeness 100.00 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 30.01 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Secondary CH2 refined with riding coordinates: C17(H17A,H17B) 2.b Aromatic/amide H refined with riding coordinates: C4(H4), C5(H5), C6(H6), C7(H7), C12(H12), C13(H13), C14(H14), C15(H15) 2.c Idealised Me refined as rotating group: C1(H1A,H1B,H1C), C2(H2A,H2B,H2C), C9(H9A,H9B,H9C), C10(H10A,H10B,H10C) ; _shelx_res_file ; TITL wickemeyer07_b_a.res in P-1 wickemeyer07_b.res created by SHELXL-2018/3 at 11:13:00 on 18-Feb-2021 REM Old TITL wickemeyer07_B in P9 REM SHELXT solution in P-1: R1 0.054, Rweak 0.005, Alpha 0.114 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C22 P18 Cl23 Au2 CELL 0.71073 9.177774 11.055391 11.416504 87.2672 67.3282 68.5292 ZERR 2 0.000258 0.000305 0.000321 0.0023 0.0027 0.0026 LATT 1 SFAC C H Au Cl P UNIT 34 44 4 4 4 L.S. 11 PLAN 11 MORE -1 BOND $H CONF fmap 2 acta OMIT 1 0 0 REM REM REM WGHT 0.025900 3.426700 EXTI 0.001849 FVAR 3.07946 AU1 3 0.515811 0.576926 0.393249 11.00000 0.01175 0.01160 = 0.01227 0.00332 -0.00521 -0.00336 AU2 3 0.535484 0.534130 0.104229 11.00000 0.01324 0.00981 = 0.01239 0.00216 -0.00662 -0.00361 P1 5 0.223662 0.658081 0.483010 11.00000 0.01186 0.01121 = 0.01335 0.00237 -0.00585 -0.00299 P2 5 0.650654 0.311972 0.108288 11.00000 0.01492 0.01035 = 0.01376 0.00229 -0.00772 -0.00380 C1 1 0.131506 0.618395 0.383886 11.00000 0.02009 0.03059 = 0.01758 0.00273 -0.01028 -0.00948 AFIX 137 H1A 2 0.160967 0.657938 0.305851 11.00000 -1.50000 H1B 2 0.009729 0.650882 0.428179 11.00000 -1.50000 H1C 2 0.174712 0.525218 0.364806 11.00000 -1.50000 AFIX 0 C2 1 0.128851 0.835220 0.510869 11.00000 0.02072 0.01412 = 0.02844 0.00357 -0.00620 -0.00496 AFIX 137 H2A 2 0.159640 0.864504 0.572495 11.00000 -1.50000 H2B 2 0.007026 0.863568 0.542615 11.00000 -1.50000 H2C 2 0.169721 0.871314 0.432238 11.00000 -1.50000 AFIX 0 C3 1 0.125584 0.601356 0.634352 11.00000 0.01268 0.01235 = 0.01356 0.00078 -0.00650 -0.00414 C4 1 -0.051666 0.661412 0.699396 11.00000 0.01339 0.01780 = 0.01630 0.00344 -0.00741 -0.00463 AFIX 43 H4 2 -0.112995 0.729877 0.665708 11.00000 -1.20000 AFIX 0 C5 1 -0.137434 0.620532 0.813289 11.00000 0.01302 0.02182 = 0.01588 0.00001 -0.00499 -0.00708 AFIX 43 H5 2 -0.254919 0.661780 0.856284 11.00000 -1.20000 AFIX 0 C6 1 -0.045136 0.517299 0.861826 11.00000 0.01586 0.02238 = 0.01492 0.00233 -0.00479 -0.01065 AFIX 43 H6 2 -0.101387 0.487500 0.936816 11.00000 -1.20000 AFIX 0 C7 1 0.130862 0.458079 0.799149 11.00000 0.01699 0.01606 = 0.01495 0.00442 -0.00828 -0.00629 AFIX 43 H7 2 0.190562 0.389528 0.833747 11.00000 -1.20000 AFIX 0 C8 1 0.221937 0.499102 0.684108 11.00000 0.01332 0.01317 = 0.01342 0.00035 -0.00557 -0.00409 C9 1 0.551797 0.257771 0.261157 11.00000 0.02444 0.01584 = 0.01540 0.00204 -0.00695 -0.00691 AFIX 137 H9A 2 0.557289 0.303817 0.327570 11.00000 -1.50000 H9B 2 0.611149 0.165568 0.258886 11.00000 -1.50000 H9C 2 0.434756 0.275308 0.277732 11.00000 -1.50000 AFIX 0 C10 1 0.873693 0.245748 0.083724 11.00000 0.01715 0.01493 = 0.02412 0.00108 -0.01191 -0.00274 AFIX 137 H10A 2 0.940847 0.260984 0.000418 11.00000 -1.50000 H10B 2 0.909422 0.153434 0.090360 11.00000 -1.50000 H10C 2 0.888951 0.287746 0.147382 11.00000 -1.50000 AFIX 0 C11 1 0.639081 0.211827 -0.007615 11.00000 0.01341 0.01197 = 0.01390 0.00223 -0.00659 -0.00472 C12 1 0.710508 0.075184 -0.006840 11.00000 0.02113 0.01298 = 0.02019 0.00376 -0.01141 -0.00610 AFIX 43 H12 2 0.759922 0.041238 0.050985 11.00000 -1.20000 AFIX 0 C13 1 0.707728 -0.008816 -0.091327 11.00000 0.02456 0.01115 = 0.02214 0.00170 -0.01187 -0.00562 AFIX 43 H13 2 0.754714 -0.098893 -0.090744 11.00000 -1.20000 AFIX 0 C14 1 0.633364 0.043937 -0.177151 11.00000 0.02622 0.01627 = 0.01934 0.00168 -0.01199 -0.00930 AFIX 43 H14 2 0.629591 -0.011073 -0.234142 11.00000 -1.20000 AFIX 0 C15 1 0.564902 0.178277 -0.177901 11.00000 0.02082 0.01713 = 0.01563 0.00325 -0.01035 -0.00668 AFIX 43 H15 2 0.516302 0.210831 -0.236463 11.00000 -1.20000 AFIX 0 C16 1 0.565126 0.267762 -0.094820 11.00000 0.01586 0.01162 = 0.01192 0.00272 -0.00495 -0.00566 CL1 4 0.310036 0.103817 0.490309 11.00000 0.02529 0.05028 = 0.02613 0.01136 -0.00974 -0.00704 CL2 4 0.090620 0.096548 0.752034 11.00000 0.03910 0.03682 = 0.02382 0.00675 -0.00855 -0.00456 C17 1 0.261390 0.140409 0.653373 11.00000 0.03819 0.02968 = 0.03459 -0.00119 -0.01765 -0.01209 AFIX 23 H17A 2 0.360992 0.093329 0.671851 11.00000 -1.20000 H17B 2 0.231477 0.233247 0.671235 11.00000 -1.20000 AFIX 0 HKLF 4 REM wickemeyer07_b_a.res in P-1 REM wR2 = 0.0629, GooF = S = 1.171, Restrained GooF = 1.171 for all data REM R1 = 0.0255 for 6448 Fo > 4sig(Fo) and 0.0266 for all 6669 data REM 213 parameters refined using 0 restraints END WGHT 0.0259 3.4267 REM Highest difference peak 2.171, deepest hole -1.651, 1-sigma level 0.207 Q1 1 0.5616 0.5808 0.1460 11.00000 0.05 2.17 Q2 1 0.4834 0.5362 0.3514 11.00000 0.05 2.10 Q3 1 0.4418 0.6276 0.4586 11.00000 0.05 2.05 Q4 1 0.4591 0.5840 0.1675 11.00000 0.05 2.03 Q5 1 0.5994 0.5235 0.3309 11.00000 0.05 1.96 Q6 1 0.5070 0.4974 0.0641 11.00000 0.05 1.94 Q7 1 0.5440 0.6247 0.4356 11.00000 0.05 1.90 Q8 1 0.6222 0.4847 0.0374 11.00000 0.05 1.82 Q9 1 0.5416 0.6414 0.3650 11.00000 0.05 1.75 Q10 1 0.5008 0.4735 0.1362 11.00000 0.05 1.63 Q11 1 0.4803 0.5372 0.1995 11.00000 0.05 1.52 ; _shelx_res_checksum 36550 _shelx_hkl_file ; 0 0 -1 310.674 66.5595 7 0 0 1 307.116 77.4443 1 0 0 1 246.619 55.9278 25 0 0 1 247.886 56.5764 23 0 0 1 249.649 57.2194 21 0 0 1 197.350 51.7968 20 0 0 -1 254.535 52.8613 17 0 0 2 71808.8 2501.36 7 0 0 -2 75084.5 2530.29 7 0 0 2 69282.3 2294.36 2 0 0 -2 68292.5 2296.41 2 0 0 2 71701.3 2679.84 1 0 0 -2 64206.5 2644.50 1 0 0 2 73270.2 2506.95 25 0 0 -2 70968.5 2465.31 25 0 0 -2 72863.1 2480.98 24 0 0 2 65497.8 2335.85 22 0 0 -2 72496.5 2477.55 23 0 0 -2 69699.9 2461.29 21 0 0 2 73213.6 2504.04 21 0 0 2 73921.2 2519.05 23 0 0 -2 67856.4 2371.82 12 0 0 2 69037.9 2472.25 9 0 0 2 72129.5 2395.35 12 0 0 -2 71588.9 2475.85 20 0 0 2 73951.2 2511.47 20 0 0 -2 67998.0 2414.66 17 0 0 2 68269.3 2413.77 17 0 0 -2 67762.6 2594.71 16 0 0 2 76467.2 2562.96 18 0 0 2 68559.7 2521.70 14 0 0 2 67514.3 2594.56 16 0 0 3 21710.8 1069.94 7 0 0 -3 19663.1 825.579 2 0 0 -3 18470.2 1194.44 1 0 0 3 19699.3 816.913 2 0 0 -3 19945.2 1000.54 24 0 0 -3 19365.6 984.533 25 0 0 -3 19808.2 993.768 21 0 0 3 19974.8 888.085 22 0 0 -3 18548.1 973.792 23 0 0 3 21430.0 1028.54 9 0 0 3 21300.5 957.944 12 0 0 -3 19342.8 906.027 12 0 0 -3 19882.1 1001.28 20 0 0 -3 19292.7 1140.86 16 0 0 3 19900.8 970.320 17 0 0 3 21838.9 1103.50 18 0 0 3 20304.0 1095.37 14 0 0 4 373447. 11241.0 7 0 0 -4 334559. 11563.8 1 0 0 -4 337854. 10736.8 2 0 0 4 349247. 10732.0 2 0 0 -4 323203. 11020.5 24 0 0 -4 321048. 11002.4 25 0 0 -4 314910. 10999.6 21 0 0 -4 332910. 11031.1 23 0 0 4 356257. 10967.7 12 0 0 -4 325027. 11031.3 20 0 0 4 354481. 11037.6 17 0 0 4 362894. 11236.9 18 0 0 4 350549. 11310.8 14 0 0 5 25470.2 1446.21 7 0 0 5 24417.6 1116.92 2 0 0 -5 24312.7 1698.08 1 0 0 -5 25179.8 1374.74 24 0 0 -5 23130.6 1326.82 25 0 0 -5 25009.8 1369.19 23 0 0 -5 26119.5 1389.70 21 0 0 -5 23841.5 1357.97 20 0 0 5 25668.6 1366.92 17 0 0 5 25775.6 1476.59 18 0 0 5 27326.6 1612.41 14 0 0 5 27420.8 1312.04 12 0 0 6 133896. 5253.27 7 0 0 6 147765. 4785.03 2 0 0 -6 130426. 5730.83 1 0 0 -6 131039. 5101.69 25 0 0 -6 132597. 5125.41 24 0 0 -6 131562. 5111.97 23 0 0 -6 130703. 5109.48 21 0 0 6 144534. 5487.96 11 0 0 -6 138593. 5183.17 20 0 0 6 144080. 5353.63 18 0 0 6 153182. 5253.98 17 0 0 6 142645. 5564.60 14 0 0 6 154308. 5077.05 12 0 0 7 15708.4 1249.52 7 0 0 7 17420.3 928.410 2 0 0 -7 14969.1 1481.92 1 0 0 -7 15137.0 1145.35 25 0 0 -7 14965.9 1146.79 24 0 0 -7 14652.0 1135.83 23 0 0 -7 13787.0 1109.61 21 0 0 7 15371.3 1332.58 11 0 0 -7 14560.6 1141.37 20 0 0 7 15250.6 1244.31 18 0 0 7 16431.4 1200.80 17 0 0 7 17113.0 1108.87 12 0 0 7 16213.3 1371.71 14 0 0 8 173080. 6856.07 7 0 0 -8 168516. 7430.15 1 0 0 8 201991. 6246.18 2 0 0 -8 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215.668 17 3 -5 6 448.489 250.430 8 3 -5 6 310.500 103.147 7 -3 5 -7 92879.1 3991.97 1 -3 5 -7 93676.3 3685.69 4 -3 5 -7 93254.4 3908.70 9 3 -5 7 88551.5 4292.34 11 3 -5 7 90085.0 4223.66 8 3 -5 7 85086.0 4433.94 14 -3 5 -7 105426. 4630.82 16 3 -5 7 92151.5 4388.69 15 -3 5 -7 102151. 3802.81 13 3 -5 7 91433.5 4146.73 12 3 -5 7 93558.9 4076.82 17 3 -5 7 95159.9 3444.20 7 -3 5 -7 87493.4 4145.28 5 -3 5 -8 8476.48 905.892 1 3 -5 8 7794.02 977.271 8 3 -5 8 8047.04 1035.65 11 -3 5 -8 6689.58 667.743 9 3 -5 8 6856.92 1069.71 14 3 -5 8 7810.81 965.495 12 -3 5 -8 7732.41 1052.91 16 -3 5 -8 6892.81 755.799 13 3 -5 8 8215.12 944.754 17 -3 5 -8 8005.70 941.893 5 -3 5 -9 44200.8 2552.06 1 3 -5 9 49421.1 2959.61 11 3 -5 9 54150.7 2874.21 8 -3 5 -9 44952.2 2960.25 16 3 -5 9 44416.9 2735.88 12 -3 5 -9 50701.3 2541.50 13 3 -5 9 45385.1 3132.43 14 3 -5 9 53073.6 2791.90 17 -3 5 -9 49862.0 2765.87 5 -3 5 -10 832.988 333.805 1 3 -5 10 31.5226 206.834 12 3 -5 10 376.749 308.523 11 3 -5 10 552.180 403.147 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3027.99 583.773 2 3 -4 -1 2536.99 555.677 3 3 -4 -1 2580.50 434.061 25 3 -4 -1 2499.70 426.792 24 3 -4 -1 3171.99 473.043 23 3 -4 -1 3355.94 549.426 22 3 -4 -1 3263.41 480.768 21 -3 4 1 3067.93 603.212 10 3 -4 -1 3462.41 503.826 20 -3 4 1 3412.58 609.708 18 3 -4 -1 2131.96 540.611 15 -3 4 0 51986.8 2219.38 4 -3 4 0 49561.5 2215.35 7 3 -4 0 52410.3 2871.22 3 -3 4 0 53471.9 2747.64 2 3 -4 0 47369.6 2155.89 24 3 -4 0 47388.5 2151.52 25 3 -4 0 46689.4 2144.30 23 3 -4 0 48751.6 2171.69 21 3 -4 0 49615.3 2449.52 22 3 -4 0 43927.3 2372.06 8 -3 4 0 48099.6 2614.26 10 3 -4 0 49071.2 2188.37 20 -3 4 0 49877.1 2514.26 18 3 -4 0 42873.6 2817.03 15 3 -4 0 43996.0 1897.91 13 -3 4 -1 353805. 9546.95 6 -3 4 -1 284489. 9313.51 7 -3 4 -1 304976. 9462.85 4 -3 4 -1 310556. 10307.5 2 3 -4 1 327294. 11195.5 3 3 -4 1 266647. 9331.76 25 3 -4 1 269859. 9344.52 24 3 -4 1 256384. 9318.80 23 3 -4 1 262828. 9333.38 21 3 -4 1 281043. 9753.84 22 3 -4 1 263341. 9845.88 8 -3 4 -1 282550. 10193.5 10 3 -4 1 270166. 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