Crystallography Open Database

Information card for entry 7709260

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Coordinates	7709260.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C57 H42 B F20 N S Si
Calculated formula	C57 H42 B F20 N S Si
Title of publication	Norbornene based-sulfide-stabilized silylium ions: synthesis, structure and application in catalysis.
Authors of publication	Dajnak, Aymeric; Özpınar, Gül Altınbaş; Lenk, Romaric; Saffon-Merceron, Nathalie; Baceiredo, Antoine; Kato, Tsuyoshi; Müller, Thomas; Maerten, Eddy
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2022
Journal volume	51
Journal issue	4
Pages of publication	1407 - 1414
a	12.7325 ± 0.0008 Å
b	13.4053 ± 0.0009 Å
c	16.4281 ± 0.001 Å
α	85.829 ± 0.002°
β	69.6571 ± 0.0017°
γ	89.197 ± 0.0019°
Cell volume	2622 ± 0.3 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0939
Residual factor for significantly intense reflections	0.0507
Weighted residual factors for significantly intense reflections	0.1057
Weighted residual factors for all reflections included in the refinement	0.1242
Goodness-of-fit parameter for all reflections included in the refinement	1.025
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
272683 (current)	2022-02-04	cif/ Updating files of 7709260 Original log message: Adding full bibliography for 7709260.cif.	7709260.cif
271947	2022-01-08	cif/ Adding structures of 7709260 via cif-deposit CGI script.	7709260.cif