Crystallography Open Database

Information card for entry 7709276

Preview

Coordinates	7709276.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H42 K N2 O6 P Se2
Calculated formula	C22 H42 K N2 O6 P Se2
Title of publication	Ion-bearing stairs: alkali metal complexes of 1,2-diaza-4-phospholides.
Authors of publication	Zhao, Minggang; Xue, Tingting; He, Ru-Ru; Ma, Jianping; Zheng, Wenjun
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2022
Journal volume	51
Journal issue	4
Pages of publication	1634 - 1645
a	17.1551 ± 0.0009 Å
b	13.4665 ± 0.0007 Å
c	13.0108 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	3005.7 ± 0.3 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	7
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.1124
Residual factor for significantly intense reflections	0.1088
Weighted residual factors for significantly intense reflections	0.2542
Weighted residual factors for all reflections included in the refinement	0.2558
Goodness-of-fit parameter for all reflections included in the refinement	1.118
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
272694 (current)	2022-02-04	cif/ Updating files of 7709271, 7709272, 7709273, 7709274, 7709275, 7709276, 7709277, 7709278 Original log message: Adding full bibliography for 7709271--7709278.cif.	7709276.cif
271980	2022-01-11	cif/ Adding structures of 7709271, 7709272, 7709273, 7709274, 7709275, 7709276, 7709277, 7709278 via cif-deposit CGI script.	7709276.cif