Crystallography Open Database

Information card for entry 7709291

Preview

Coordinates	7709291.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H42 Cl3 Ga N2
Calculated formula	C30 H42 Cl3 Ga N2
Title of publication	Geminal C-Cl and Si-Cl bond activation of chloromethanes and chlorosilanes by gallanediyl LGa.
Authors of publication	Helling, Christoph; Ganesamoorthy, Chelladurai; Wölper, Christoph; Schulz, Stephan
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2022
Journal volume	51
Journal issue	5
Pages of publication	2050 - 2058
a	14.7721 ± 0.0012 Å
b	21.3648 ± 0.0019 Å
c	9.6684 ± 0.0008 Å
α	90°
β	90°
γ	90°
Cell volume	3051.4 ± 0.4 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0598
Residual factor for significantly intense reflections	0.0461
Weighted residual factors for significantly intense reflections	0.1049
Weighted residual factors for all reflections included in the refinement	0.11
Goodness-of-fit parameter for all reflections included in the refinement	1.08
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
272670 (current)	2022-02-04	cif/ Updating files of 7709288, 7709289, 7709290, 7709291, 7709292, 7709293, 7709294 Original log message: Adding full bibliography for 7709288--7709294.cif.	7709291.cif
272012	2022-01-13	cif/ Adding structures of 7709288, 7709289, 7709290, 7709291, 7709292, 7709293, 7709294 via cif-deposit CGI script.	7709291.cif