Crystallography Open Database

Information card for entry 7709325

Preview

Coordinates	7709325.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C9 H13 Cl4 N O Se W
Calculated formula	C9 H13 Cl4 N O Se W
Title of publication	Tungsten(vi) selenide tetrachloride, WSeCl4 – synthesis, properties, coordination complexes and application of [WSeCl4(SenBu2)] for CVD growth of WSe2 thin films
Authors of publication	Greenacre, Victoria K.; Hector, Andrew L.; Huang, Ruomeng; Levason, William; Sethi, Vikesh; Reid, Gillian
Journal of publication	Dalton Transactions
Year of publication	2022
a	18.8765 ± 0.001 Å
b	7.3681 ± 0.0003 Å
c	22.871 ± 0.0013 Å
α	90°
β	104.559 ± 0.006°
γ	90°
Cell volume	3078.8 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0515
Residual factor for significantly intense reflections	0.0395
Weighted residual factors for significantly intense reflections	0.0888
Weighted residual factors for all reflections included in the refinement	0.0931
Goodness-of-fit parameter for all reflections included in the refinement	1.053
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Diffraction radiation X-ray symbol	K-L~3~
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
272142 (current)	2022-01-20	cif/ Adding structures of 7709323, 7709324, 7709325, 7709326, 7709327, 7709328, 7709329, 7709330 via cif-deposit CGI script.	7709325.cif