Crystallography Open Database

Information card for entry 7709328

Preview

Coordinates	7709328.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C4 H12 Cl6 S2 Se3 W2
Calculated formula	C4 H12 Cl6 S2 Se3 W2
Title of publication	Tungsten(vi) selenide tetrachloride, WSeCl4 – synthesis, properties, coordination complexes and application of [WSeCl4(SenBu2)] for CVD growth of WSe2 thin films
Authors of publication	Greenacre, Victoria K.; Hector, Andrew L.; Huang, Ruomeng; Levason, William; Sethi, Vikesh; Reid, Gillian
Journal of publication	Dalton Transactions
Year of publication	2022
a	13.5882 ± 0.00013 Å
b	19.5279 ± 0.0002 Å
c	6.69716 ± 0.00007 Å
α	90°
β	90°
γ	90°
Cell volume	1777.08 ± 0.03 Å³
Cell temperature	100 ± 0.1 K
Ambient diffraction temperature	100 ± 0.1 K
Number of distinct elements	6
Space group number	62
Hermann-Mauguin space group symbol	P n m a
Hall space group symbol	-P 2ac 2n
Residual factor for all reflections	0.0295
Residual factor for significantly intense reflections	0.0295
Weighted residual factors for significantly intense reflections	0.0705
Weighted residual factors for all reflections included in the refinement	0.0706
Goodness-of-fit parameter for all reflections included in the refinement	1.188
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
272142 (current)	2022-01-20	cif/ Adding structures of 7709323, 7709324, 7709325, 7709326, 7709327, 7709328, 7709329, 7709330 via cif-deposit CGI script.	7709328.cif