Crystallography Open Database

Information card for entry 7709404

Preview

Coordinates	7709404.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C20 H40 N4 Si4 Sn
Calculated formula	C20 H40 N4 Si4 Sn
SMILES	[Sn]1([N]([Si](C)(C)C)=C(N1[Si](C)(C)C)c1cc(C#N)ccc1)N([Si](C)(C)C)[Si](C)(C)C
Title of publication	Reversible addition of tin(II) amides to nitriles.
Authors of publication	Chlupatý, Tomáš; Brichová, Kristýna; Samsonov, Maksim A.; R°užičková, Zdeňka; R°užička, Aleš
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2022
Journal volume	51
Journal issue	5
Pages of publication	1879 - 1887
a	10.162 ± 0.0004 Å
b	11.219 ± 0.0006 Å
c	14.3991 ± 0.001 Å
α	68.279 ± 0.005°
β	73.507 ± 0.004°
γ	80.199 ± 0.004°
Cell volume	1458.38 ± 0.15 Å³
Cell temperature	150 ± 1 K
Ambient diffraction temperature	150 ± 1 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0521
Residual factor for significantly intense reflections	0.0423
Weighted residual factors for significantly intense reflections	0.0949
Weighted residual factors for all reflections included in the refinement	0.0992
Goodness-of-fit parameter for all reflections included in the refinement	1.233
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
272405 (current)	2022-02-02	cif/ Adding structures of 7709403, 7709404 via cif-deposit CGI script.	7709404.cif