Crystallography Open Database

Information card for entry 7710120

Preview

Coordinates	7710120.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H57 N2 O Sc Si2
Calculated formula	C33 H57 N2 O Sc Si2
Title of publication	Sc and Y bis(alkyl) complexes supported by bi- and tridentate amidinate ligands. Synthesis, structure and catalytic activity in polymerization of isoprene and 1-heptene.
Authors of publication	Trifonov, Alexander; Tolpygin, Aleksei; Sachkova, Anastasia; Mikhailychev, Alexander; Ob’edkov, A. M.; Glukhova, Tatyana; Cherkasov, Anton; Fukin, Georgii K.
Journal of publication	Dalton Transactions
Year of publication	2022
a	11.1928 ± 0.0005 Å
b	11.3356 ± 0.0005 Å
c	15.4964 ± 0.0004 Å
α	94.893 ± 0.003°
β	98.012 ± 0.003°
γ	111.928 ± 0.004°
Cell volume	1785.79 ± 0.13 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0564
Residual factor for significantly intense reflections	0.0421
Weighted residual factors for significantly intense reflections	0.1065
Weighted residual factors for all reflections included in the refinement	0.1161
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
274672 (current)	2022-04-26	cif/ Adding structures of 7710119, 7710120, 7710121, 7710122 via cif-deposit CGI script.	7710120.cif