Crystallography Open Database

Information card for entry 7710140

Preview

Coordinates	7710140.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H41 Cl Ge N2
Calculated formula	C30 H41 Cl Ge N2
SMILES	[Ge]1(Cl)N(C2C(=[N]1c1c(C(C)C)cccc1C(C)C)CCCC=2)c1c(cccc1C(C)C)C(C)C
Title of publication	An α-diiminato germylene family: syntheses, structures, and reactivity towards C-C coupled digermylene and digermylene oxide
Authors of publication	Liu, Jingjing; Shang, Jianxuan; Wei, Jing; Gao, Fangfang; Hou, Lei; Zeng, FanLong; Li, Anyang; Wang, Wenyuan
Journal of publication	Dalton Transactions
Year of publication	2022
a	17.622 ± 0.007 Å
b	10.372 ± 0.003 Å
c	17.159 ± 0.007 Å
α	90°
β	117.354 ± 0.011°
γ	90°
Cell volume	2785.6 ± 1.8 Å³
Cell temperature	90 K
Ambient diffraction temperature	90 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0601
Residual factor for significantly intense reflections	0.0435
Weighted residual factors for significantly intense reflections	0.1082
Weighted residual factors for all reflections included in the refinement	0.1161
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation wavelength	1.34138 Å
Diffraction radiation type	GaKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
274814 (current)	2022-05-03	cif/ Adding structures of 7710140, 7710141, 7710142, 7710143, 7710144, 7710145, 7710146, 7710147 via cif-deposit CGI script.	7710140.cif