Crystallography Open Database

Information card for entry 7710143

Preview

Coordinates	7710143.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H40 Ge N2
Calculated formula	C30 H40 Ge N2
SMILES	[Ge]1N(c2c(cccc2C(C)C)C(C)C)C2C(N1c1c(C(C)C)cccc1C(C)C)=CCCC=2
Title of publication	An α-diiminato germylene family: syntheses, structures, and reactivity towards C-C coupled digermylene and digermylene oxide
Authors of publication	Liu, Jingjing; Shang, Jianxuan; Wei, Jing; Gao, Fangfang; Hou, Lei; Zeng, FanLong; Li, Anyang; Wang, Wenyuan
Journal of publication	Dalton Transactions
Year of publication	2022
a	8.9419 ± 0.0005 Å
b	11.853 ± 0.0007 Å
c	13.4458 ± 0.0007 Å
α	101.563 ± 0.002°
β	90.578 ± 0.002°
γ	98.666 ± 0.002°
Cell volume	1379.04 ± 0.13 Å³
Cell temperature	150.15 K
Ambient diffraction temperature	150.15 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0602
Residual factor for significantly intense reflections	0.0429
Weighted residual factors for significantly intense reflections	0.108
Weighted residual factors for all reflections included in the refinement	0.118
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
274814 (current)	2022-05-03	cif/ Adding structures of 7710140, 7710141, 7710142, 7710143, 7710144, 7710145, 7710146, 7710147 via cif-deposit CGI script.	7710143.cif