Crystallography Open Database

Information card for entry 7710168

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Coordinates	7710168.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	Tetrachlorobis(diethyl ether)molybdenum(IV)
Formula	C8 H20 Cl4 Mo O2
Calculated formula	C8 H20 Cl4 Mo O2
Title of publication	Synthesis, Characterization, X-ray and Electronic Structures of Diethyl Ether and 1,2-Dimethoxyethane Adducts of Molybdenum(IV) Chloride and Tungsten(IV) Chloride
Authors of publication	Shaw, Thomas E.; Diethrich, Timothy J. J.; Stern, Charlotte L.; Scott, Brian; Jurca, Titel; Gilbert, Thomas M.; Sattelberger, Alfred P.
Journal of publication	Dalton Transactions
Year of publication	2022
a	7.5956 ± 0.0002 Å
b	11.4732 ± 0.0004 Å
c	9.0193 ± 0.0003 Å
α	90°
β	106.347 ± 0.003°
γ	90°
Cell volume	754.22 ± 0.04 Å³
Cell temperature	298.1 ± 0.5 K
Ambient diffraction temperature	298.1 ± 0.5 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0272
Residual factor for significantly intense reflections	0.0212
Weighted residual factors for significantly intense reflections	0.0494
Weighted residual factors for all reflections included in the refinement	0.0516
Goodness-of-fit parameter for all reflections included in the refinement	1.068
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
274820 (current)	2022-05-03	cif/ Adding structures of 7710167, 7710168, 7710169 via cif-deposit CGI script.	7710168.cif