#------------------------------------------------------------------------------ #$Date: 2022-06-16 01:57:54 +0300 (Thu, 16 Jun 2022) $ #$Revision: 276056 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/71/04/7710488.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7710488 loop_ _publ_author_name 'Wang, Zheng' 'Liu, Yahua' 'Mingyang, Han' 'Ma, Ning' 'Lyu, Quanming' 'Liu, Qingbin' 'Sun, Wen Hua' _publ_section_title ; Efficient transfer hydrogenation of ketones by molybdenum complexes through comprehensively verifying auxiliary ligands ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D2DT01177H _journal_year 2022 _chemical_formula_sum 'C60 H104 Ge2.9 N4 Si7.1' _chemical_formula_weight 1291.53 _space_group_crystal_system tetragonal _space_group_IT_number 114 _space_group_name_Hall 'P -4 2n' _space_group_name_H-M_alt 'P -4 21 c' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2014/7 _audit_update_record ; 2021-06-29 deposited with the CCDC. 2022-06-15 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 16.3758(5) _cell_length_b 16.3758(5) _cell_length_c 27.0498(9) _cell_measurement_reflns_used 9288 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 27.14 _cell_measurement_theta_min 2.32 _cell_volume 7253.9(4) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0401 _diffrn_reflns_av_unetI/netI 0.0231 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_h_min -21 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_l_max 34 _diffrn_reflns_limit_l_min -34 _diffrn_reflns_number 92304 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.193 _diffrn_reflns_theta_min 2.315 _exptl_absorpt_coefficient_mu 1.348 _exptl_absorpt_correction_T_max 0.7455 _exptl_absorpt_correction_T_min 0.5883 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.183 _exptl_crystal_description rod _exptl_crystal_F_000 2737 _exptl_crystal_size_max 0.566 _exptl_crystal_size_mid 0.194 _exptl_crystal_size_min 0.170 _refine_diff_density_max 0.199 _refine_diff_density_min -0.367 _refine_diff_density_rms 0.038 _refine_ls_abs_structure_details ; Refined as an inversion twin. ; _refine_ls_abs_structure_Flack 0.017(6) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.030 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 339 _refine_ls_number_reflns 8055 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.030 _refine_ls_R_factor_all 0.0188 _refine_ls_R_factor_gt 0.0179 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0263P)^2^+1.0777P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0476 _refine_ls_wR_factor_ref 0.0479 _reflns_Friedel_coverage 0.832 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.999 _reflns_number_gt 7822 _reflns_number_total 8055 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d2dt01177h2.cif _cod_data_source_block fl180216sq _cod_original_cell_volume 7253.9(5) _cod_original_formula_sum 'C60 H104 Ge2.90 N4 Si7.10' _cod_database_code 7710488 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; fl180216sq.res created by SHELXL-2014/7 TITL fl180216te1 in P-42(1)c CELL 0.71073 16.3758 16.3758 27.0498 90.000 90.000 90.000 ZERR 4.00 0.0005 0.0005 0.0009 0.000 0.000 0.000 LATT -1 SYMM Y, - X, - Z SYMM - Y, X, - Z SYMM 1/2 + X, 1/2 - Y, 1/2 - Z SYMM 1/2 - X, 1/2 + Y, 1/2 - Z SYMM - X, - Y, Z SYMM 1/2 - Y, 1/2 - X, 1/2 + Z SYMM 1/2 + Y, 1/2 + X, 1/2 + Z SFAC C H N SI GE UNIT 240 416 16 28.39 11.61 MERG 2 FMAP 2 PLAN 20 ACTA BOND $H CONF EADP GE1A SI1B TWIN OMIT 0 3 6 L.S. 19 0 13 TEMP -173.16 ABIN WGHT 0.026300 1.077700 BASF 0.01738 FVAR 0.06829 0.45179 PART 1 GE1A 5 0.574601 0.900996 1.350448 21.00000 0.01248 0.01701 = 0.01060 -0.00220 -0.00238 0.00378 PART 2 SI1B 4 0.571568 0.908315 1.346450 -21.00000 0.01248 0.01701 = 0.01060 -0.00220 -0.00238 0.00378 PART 0 GE2 5 0.559349 1.060674 1.317564 11.00000 0.01428 0.02253 = 0.01301 0.00484 0.00265 0.00403 SI3 4 0.571487 1.015392 1.404866 11.00000 0.01502 0.01282 = 0.00970 -0.00027 -0.00105 0.00006 SI4 4 0.730528 0.797416 1.325873 11.00000 0.01792 0.02129 = 0.02373 -0.00287 -0.00526 0.00337 SI5 4 0.688176 1.003394 1.495616 11.00000 0.02116 0.01836 = 0.01249 0.00091 -0.00312 -0.00192 N1 3 0.637761 0.844113 1.309348 11.00000 0.01942 0.01949 = 0.01584 -0.00017 -0.00326 0.00005 N2 3 0.643250 1.055794 1.445488 11.00000 0.01865 0.01464 = 0.01262 -0.00010 -0.00219 -0.00179 C1 1 0.598812 0.823083 1.262918 11.00000 0.01604 0.02116 = 0.01579 -0.00346 -0.00190 0.00540 C2 1 0.547023 0.754365 1.260526 11.00000 0.01609 0.02350 = 0.02441 -0.00552 -0.00123 0.00303 C3 1 0.509169 0.736263 1.215687 11.00000 0.02340 0.03276 = 0.03331 -0.01514 -0.00497 -0.00062 AFIX 43 H3 2 0.474191 0.690114 1.213568 11.00000 -1.20000 AFIX 0 C4 1 0.521400 0.783758 1.174528 11.00000 0.03606 0.04722 = 0.02166 -0.01615 -0.00901 0.00900 AFIX 43 H4 2 0.494742 0.770583 1.144372 11.00000 -1.20000 AFIX 0 C5 1 0.572494 0.850695 1.177015 11.00000 0.03528 0.03630 = 0.01457 -0.00323 -0.00023 0.01090 AFIX 43 H5 2 0.581283 0.882589 1.148166 11.00000 -1.20000 AFIX 0 C6 1 0.611477 0.872570 1.220857 11.00000 0.02256 0.02274 = 0.01760 -0.00316 0.00119 0.00768 C7 1 0.530704 0.698981 1.304546 11.00000 0.02358 0.02384 = 0.03647 0.00018 -0.00059 -0.00372 AFIX 13 H7 2 0.563891 0.719667 1.332940 11.00000 -1.20000 AFIX 0 C8 1 0.556871 0.611242 1.294472 11.00000 0.05825 0.02617 = 0.07334 0.00764 0.01659 0.00190 AFIX 33 H8A 2 0.545416 0.577544 1.323598 11.00000 -1.50000 H8B 2 0.526511 0.589937 1.266040 11.00000 -1.50000 H8C 2 0.615514 0.609821 1.287301 11.00000 -1.50000 AFIX 0 C9 1 0.440828 0.701372 1.320017 11.00000 0.02945 0.03892 = 0.05485 0.00345 0.00930 -0.00676 AFIX 33 H9A 2 0.432445 0.665118 1.348392 11.00000 -1.50000 H9B 2 0.425870 0.757309 1.329172 11.00000 -1.50000 H9C 2 0.406625 0.683219 1.292394 11.00000 -1.50000 AFIX 0 C10 1 0.666500 0.946918 1.220925 11.00000 0.03511 0.02287 = 0.01971 -0.00063 0.00857 0.00196 AFIX 13 H10 2 0.674560 0.963889 1.256101 11.00000 -1.20000 AFIX 0 C11 1 0.750382 0.927815 1.199297 11.00000 0.03981 0.03673 = 0.04951 -0.00747 0.02254 -0.00462 AFIX 33 H11A 2 0.784221 0.977162 1.199934 11.00000 -1.50000 H11B 2 0.776610 0.884946 1.218966 11.00000 -1.50000 H11C 2 0.744203 0.909065 1.165095 11.00000 -1.50000 AFIX 0 C12 1 0.629070 1.019271 1.193264 11.00000 0.07562 0.02871 = 0.02137 0.00477 0.00501 0.00713 AFIX 33 H12A 2 0.666816 1.065676 1.194344 11.00000 -1.50000 H12B 2 0.619062 1.003876 1.158782 11.00000 -1.50000 H12C 2 0.577349 1.034621 1.208943 11.00000 -1.50000 AFIX 0 C13 1 0.717891 0.733693 1.382498 11.00000 0.03472 0.03051 = 0.03769 0.00847 -0.01452 0.00189 AFIX 33 H13A 2 0.770228 0.708309 1.391013 11.00000 -1.50000 H13B 2 0.699640 0.768220 1.409950 11.00000 -1.50000 H13C 2 0.677163 0.691062 1.376288 11.00000 -1.50000 AFIX 0 C14 1 0.765156 0.730350 1.274295 11.00000 0.02647 0.03105 = 0.04025 -0.01310 -0.00356 0.00520 AFIX 33 H14A 2 0.816860 0.704190 1.283350 11.00000 -1.50000 H14B 2 0.723817 0.688342 1.268009 11.00000 -1.50000 H14C 2 0.772997 0.763255 1.244409 11.00000 -1.50000 AFIX 0 C15 1 0.809226 0.876799 1.338159 11.00000 0.02057 0.03160 = 0.03508 -0.01003 -0.00253 0.00047 AFIX 33 H15A 2 0.860744 0.850396 1.347343 11.00000 -1.50000 H15B 2 0.817459 0.909777 1.308341 11.00000 -1.50000 H15C 2 0.790930 0.912040 1.365265 11.00000 -1.50000 AFIX 0 C16 1 0.668643 1.140092 1.437574 11.00000 0.02143 0.01474 = 0.01402 0.00116 -0.00519 -0.00240 C17 1 0.623465 1.203410 1.459791 11.00000 0.02491 0.01898 = 0.01992 -0.00343 -0.00456 -0.00108 C18 1 0.652514 1.283189 1.455286 11.00000 0.03818 0.01763 = 0.03216 -0.00544 -0.00469 -0.00064 AFIX 43 H18 2 0.623452 1.326317 1.470848 11.00000 -1.20000 AFIX 0 C19 1 0.722069 1.301057 1.428927 11.00000 0.04148 0.01860 = 0.03433 0.00195 -0.00690 -0.01110 AFIX 43 H19 2 0.741011 1.355765 1.426686 11.00000 -1.20000 AFIX 0 C20 1 0.764167 1.238782 1.405734 11.00000 0.02850 0.02474 = 0.02703 0.00442 -0.00164 -0.00959 AFIX 43 H20 2 0.811197 1.251483 1.386664 11.00000 -1.20000 AFIX 0 C21 1 0.739062 1.157642 1.409730 11.00000 0.02373 0.02016 = 0.01786 0.00158 -0.00278 -0.00336 C22 1 0.544771 1.188273 1.487699 11.00000 0.02291 0.02243 = 0.02878 -0.00758 -0.00043 0.00130 AFIX 13 H22 2 0.532162 1.128712 1.484827 11.00000 -1.20000 AFIX 0 C23 1 0.473536 1.234657 1.464844 11.00000 0.03020 0.03821 = 0.03249 -0.00775 -0.00351 0.00800 AFIX 33 H23A 2 0.423705 1.223538 1.483744 11.00000 -1.50000 H23B 2 0.485109 1.293360 1.465534 11.00000 -1.50000 H23C 2 0.465960 1.216915 1.430549 11.00000 -1.50000 AFIX 0 C24 1 0.552418 1.207787 1.542707 11.00000 0.02945 0.05305 = 0.02691 -0.00830 -0.00087 0.00169 AFIX 33 H24A 2 0.500179 1.197089 1.559153 11.00000 -1.50000 H24B 2 0.594942 1.173386 1.557407 11.00000 -1.50000 H24C 2 0.567040 1.265410 1.546864 11.00000 -1.50000 AFIX 0 C25 1 0.788746 1.092161 1.383640 11.00000 0.02549 0.02310 = 0.02438 0.00420 0.00685 -0.00241 AFIX 13 H25 2 0.760653 1.038638 1.388884 11.00000 -1.20000 AFIX 0 C26 1 0.875133 1.084841 1.404186 11.00000 0.03088 0.04708 = 0.03189 0.00520 0.00263 0.00684 AFIX 33 H26A 2 0.904638 1.042019 1.386257 11.00000 -1.50000 H26B 2 0.903680 1.137011 1.400138 11.00000 -1.50000 H26C 2 0.872610 1.070788 1.439369 11.00000 -1.50000 AFIX 0 C27 1 0.792719 1.107818 1.327968 11.00000 0.03185 0.03440 = 0.02336 0.00147 0.00760 -0.00625 AFIX 33 H27A 2 0.825036 1.064790 1.312116 11.00000 -1.50000 H27B 2 0.737330 1.107750 1.314251 11.00000 -1.50000 H27C 2 0.818337 1.160951 1.321853 11.00000 -1.50000 AFIX 0 C28 1 0.757003 1.073720 1.530274 11.00000 0.02780 0.03065 = 0.02189 -0.00003 -0.00922 -0.00507 AFIX 33 H28A 2 0.781799 1.044386 1.558056 11.00000 -1.50000 H28B 2 0.800021 1.093641 1.508163 11.00000 -1.50000 H28C 2 0.725369 1.120100 1.542820 11.00000 -1.50000 AFIX 0 C29 1 0.747603 0.913841 1.473747 11.00000 0.04763 0.02833 = 0.02403 0.00160 -0.00762 0.01167 AFIX 33 H29A 2 0.771913 0.885783 1.502163 11.00000 -1.50000 H29B 2 0.711285 0.876225 1.456125 11.00000 -1.50000 H29C 2 0.790977 0.932249 1.451412 11.00000 -1.50000 AFIX 0 C30 1 0.608165 0.965401 1.538515 11.00000 0.02954 0.04553 = 0.02083 0.01166 -0.00502 -0.00968 AFIX 33 H30A 2 0.633990 0.936487 1.566115 11.00000 -1.50000 H30B 2 0.576565 1.011657 1.551259 11.00000 -1.50000 H30C 2 0.571728 0.928015 1.520803 11.00000 -1.50000 AFIX 0 HKLF 4 1.0 1.00 0.00 0.00 0.00 1.00 0.00 0.00 0.00 1.00 REM fl180216te1 in P-42(1)c REM R1 = 0.0179 for 7822 Fo > 4sig(Fo) and 0.0188 for all 8055 data REM 339 parameters refined using 0 restraints END WGHT 0.0263 1.0777 REM Highest difference peak 0.199, deepest hole -0.367, 1-sigma level 0.038 Q1 1 0.5770 0.9017 1.3827 11.00000 0.05 0.20 Q2 1 0.5000 1.0000 1.4059 10.50000 0.05 0.18 Q3 1 0.6216 1.0370 1.4137 11.00000 0.05 0.18 Q4 1 0.6455 1.0978 1.4357 11.00000 0.05 0.18 Q5 1 0.5590 1.0551 1.2843 11.00000 0.05 0.17 Q6 1 0.6823 1.1445 1.4127 11.00000 0.05 0.17 Q7 1 0.6034 0.8559 1.3466 11.00000 0.05 0.17 Q8 1 0.5655 0.9631 1.4003 11.00000 0.05 0.17 Q9 1 0.5198 0.9079 1.3470 11.00000 0.05 0.17 Q10 1 0.7730 0.8388 1.3268 11.00000 0.05 0.17 Q11 1 0.6324 0.9003 1.5562 11.00000 0.05 0.17 Q12 1 0.7621 1.1267 1.3988 11.00000 0.05 0.16 Q13 1 0.8343 0.7297 1.2704 11.00000 0.05 0.16 Q14 1 0.5049 1.0918 1.3164 11.00000 0.05 0.16 Q15 1 0.5562 0.7983 1.2658 11.00000 0.05 0.16 Q16 1 0.7349 1.0412 1.5023 11.00000 0.05 0.15 Q17 1 0.5951 0.7717 1.2603 11.00000 0.05 0.15 Q18 1 0.6062 1.0347 1.4359 11.00000 0.05 0.15 Q19 1 0.5443 0.7298 1.2807 11.00000 0.05 0.15 Q20 1 0.4900 0.7042 1.3124 11.00000 0.05 0.15 ; _shelx_res_checksum 46628 _shelx_hkl_file ; 1 -2 0 17.75 1.13 2 1 0 17.86 1.13 2 1 0 19.60 1.14 -1 2 0 18.59 1.14 -2 -1 0 19.12 1.13 -2 -1 0 17.07 1.14 -2 -1 0 18.82 1.14 -2 -1 0 19.52 1.13 -2 0 0 19.71 1.15 2 0 0 20.28 1.16 2 0 0 16.53 1.15 0 2 0 16.90 1.15 2 0 0 18.48 1.17 0 -2 0 18.70 1.16 0 2 0 20.47 1.15 -1 -2 0 19.42 1.14 1 2 0 17.52 1.13 1 2 0 19.71 1.12 -2 1 0 18.11 1.12 -2 1 0 17.99 1.14 -1 -2 0 18.88 1.13 -1 -2 0 19.41 1.12 -2 1 0 18.76 1.13 1 2 0 18.87 1.14 2 -1 0 17.93 1.12 2 -1 0 17.22 1.15 2 -1 0 17.86 1.13 -2 2 0 15.33 0.98 -2 2 0 15.15 0.99 2 2 0 15.39 0.98 2 2 0 16.72 0.99 2 2 0 16.96 0.97 2 -2 0 14.84 0.98 2 -2 0 15.41 0.99 -2 -2 0 16.11 0.99 -2 -2 0 16.74 0.97 -2 -2 0 16.14 0.98 3 2 0 9.40 0.63 2 -3 0 10.21 0.65 3 2 0 10.44 0.62 -3 -2 0 10.01 0.62 -2 3 0 10.28 0.64 2 -3 0 9.77 0.63 -3 -2 0 9.89 0.65 3 2 0 10.45 0.65 -3 -2 0 10.27 0.64 -3 -1 0 0.33 0.05 -3 -1 0 0.34 0.07 -1 3 0 0.39 0.04 -1 3 0 0.16 0.06 -1 3 0 0.23 0.07 3 1 0 0.36 0.05 3 1 0 0.28 0.07 1 -3 0 0.27 0.04 -3 -1 0 0.27 0.06 1 -3 0 0.18 0.05 -1 3 0 0.24 0.05 1 -3 0 0.24 0.07 0 3 0 -0.79 0.04 0 -3 0 -0.74 0.04 -3 0 0 -0.70 0.05 3 0 0 -0.73 0.05 0 3 0 -0.72 0.06 0 -3 0 -0.80 0.03 0 -3 0 -0.74 0.05 -3 0 0 -0.72 0.04 -3 0 0 -0.78 0.04 3 0 0 -0.76 0.04 0 3 0 -0.73 0.03 1 3 0 0.31 0.05 -1 -3 0 0.32 0.05 -3 1 0 0.26 0.05 -1 -3 0 0.37 0.08 -3 1 0 0.29 0.05 3 -1 0 0.27 0.08 1 3 0 0.39 0.05 -1 -3 0 0.32 0.05 -3 1 0 0.24 0.07 3 -1 0 0.31 0.05 3 -1 0 0.30 0.06 2 3 0 10.30 0.63 2 3 0 9.95 0.65 -2 -3 0 10.06 0.62 -3 2 0 10.55 0.64 -3 2 0 10.13 0.62 -3 2 0 9.95 0.66 3 -2 0 10.46 0.62 3 -2 0 9.83 0.64 -2 -3 0 9.97 0.65 -2 -3 0 10.16 0.64 -3 -3 0 51.47 3.08 3 3 0 54.93 3.08 -3 3 0 51.50 3.09 3 -3 0 54.20 3.09 3 -3 0 47.34 3.07 3 3 0 43.56 3.06 -3 -3 0 48.71 3.07 -3 -3 0 51.05 3.05 3 3 0 51.62 3.05 -4 -3 0 59.14 3.66 -4 -3 0 60.05 3.65 -3 4 0 62.58 3.65 3 -4 0 55.91 3.65 -3 4 0 57.38 3.67 4 3 0 62.23 3.63 3 -4 0 61.89 3.67 -4 -3 0 59.55 3.63 4 3 0 62.81 3.67 -4 -2 0 45.08 2.89 -2 4 0 51.22 2.88 2 -4 0 50.52 2.90 4 2 0 49.10 2.89 4 2 0 43.93 2.88 -4 -2 0 48.06 2.86 2 -4 0 44.67 2.88 -4 -2 0 48.16 2.88 -4 -2 0 46.46 2.86 -1 4 0 14.19 0.87 1 -4 0 13.19 0.86 4 1 0 14.67 0.88 -4 -1 0 14.50 0.87 1 -4 0 13.82 0.85 -1 4 0 12.80 0.85 -1 4 0 13.44 0.88 4 1 0 12.93 0.86 4 1 0 13.68 0.86 -4 -1 0 13.69 0.88 4 0 0 168.34 10.34 0 -4 0 167.27 10.35 0 4 0 178.85 10.34 -4 0 0 167.57 10.36 0 4 0 171.81 10.35 4 0 0 177.06 10.36 4 -1 0 13.61 0.87 -4 1 0 13.69 0.86 -4 1 0 13.97 0.87 4 -1 0 13.43 0.89 -4 1 0 13.40 0.89 4 -1 0 12.97 0.86 -1 -4 0 13.93 0.89 1 4 0 14.91 0.86 1 4 0 13.33 0.86 1 4 0 13.75 0.88 -1 -4 0 13.84 0.86 -1 -4 0 14.20 0.87 -2 -4 0 45.49 2.84 4 -2 0 46.36 2.86 4 -2 0 50.54 2.88 2 4 0 47.60 2.85 2 4 0 42.20 2.85 -4 2 0 47.49 2.84 -4 2 0 50.38 2.86 -2 -4 0 47.44 2.85 -2 -4 0 45.49 2.87 4 -2 0 46.85 2.84 -4 2 0 47.52 2.87 2 4 0 47.42 2.87 4 -3 0 60.26 3.62 -3 -4 0 59.17 3.58 -4 3 0 63.66 3.60 -3 -4 0 61.45 3.60 -3 -4 0 60.25 3.61 -4 3 0 61.04 3.57 3 4 0 54.42 3.59 4 -3 0 58.10 3.57 3 4 0 61.06 3.61 4 -3 0 56.48 3.60 -4 3 0 56.70 3.62 -4 4 0 98.25 6.13 4 4 0 89.73 6.11 4 -4 0 93.96 6.11 4 -4 0 105.54 6.13 -4 -4 0 98.32 6.13 -4 4 0 112.22 6.12 -4 -4 0 105.98 6.11 4 4 0 105.90 6.13 -4 -4 0 101.19 6.09 -4 5 0 149.10 8.59 5 4 0 148.42 8.61 -5 -4 0 140.24 8.56 -5 -4 0 139.90 8.61 -4 5 0 140.57 8.61 5 4 0 139.29 8.57 4 -5 0 136.69 8.59 5 4 0 127.09 8.59 -5 -4 0 146.64 8.59 4 -5 0 156.55 8.62 5 3 0 22.39 1.33 -5 -3 0 20.65 1.28 3 -5 0 20.42 1.30 5 3 0 19.33 1.30 -5 -3 0 21.09 1.30 -3 5 0 20.82 1.33 -5 -3 0 20.25 1.32 3 -5 0 21.43 1.33 -3 5 0 21.92 1.30 2 -5 0 61.20 3.68 5 2 0 66.75 3.74 2 -5 0 58.18 3.71 -2 5 0 58.45 3.68 -2 5 0 63.06 3.71 -5 -2 0 62.57 3.70 -5 -2 0 63.16 3.71 -2 5 0 60.34 3.73 5 2 0 57.65 3.71 2 -5 0 61.92 3.73 -5 -2 0 61.66 3.69 -5 -2 0 60.17 3.73 5 1 0 77.41 4.68 5 1 0 73.15 4.68 5 1 0 83.40 4.71 -5 -1 0 79.82 4.69 1 -5 0 73.55 4.68 -1 5 0 83.89 4.69 -1 5 0 80.85 4.70 -1 5 0 75.19 4.70 -5 -1 0 77.18 4.67 -1 5 0 73.76 4.67 -5 -1 0 74.97 4.70 -5 0 0 0.16 0.09 5 0 0 0.13 0.06 -5 0 0 0.10 0.06 0 5 0 0.35 0.06 0 -5 0 0.14 0.06 0 -5 0 0.16 0.06 5 0 0 0.05 0.09 0 -5 0 0.15 0.09 5 0 0 0.16 0.07 0 5 0 0.15 0.09 -5 0 0 0.22 0.07 0 5 0 0.14 0.07 -1 -5 0 76.11 4.66 -1 -5 0 77.44 4.64 1 5 0 78.76 4.66 -5 1 0 80.54 4.64 5 -1 0 76.84 4.64 -5 1 0 75.01 4.66 5 -1 0 74.53 4.63 1 5 0 80.61 4.64 -1 -5 0 74.58 4.63 1 5 0 70.22 4.64 5 -1 0 80.09 4.67 -5 1 0 77.56 4.63 2 5 0 56.57 3.72 -2 -5 0 64.60 3.72 2 5 0 64.07 3.71 -2 -5 0 60.27 3.71 5 -2 0 58.82 3.70 2 5 0 64.47 3.74 -5 2 0 64.15 3.72 -5 2 0 59.84 3.74 -2 -5 0 61.76 3.74 5 -2 0 59.61 3.72 5 -2 0 61.18 3.74 -5 2 0 61.55 3.70 -3 -5 0 21.88 1.30 -5 3 0 21.51 1.27 3 5 0 20.31 1.32 -3 -5 0 20.57 1.28 3 5 0 20.98 1.28 5 -3 0 19.91 1.30 -5 3 0 22.50 1.30 5 -3 0 21.04 1.32 -3 -5 0 19.90 1.32 3 5 0 20.52 1.30 5 -3 0 20.78 1.27 -5 3 0 20.42 1.32 -5 4 0 156.19 8.61 -4 -5 0 146.78 8.61 4 5 0 151.12 8.63 5 -4 0 153.40 8.63 -4 -5 0 139.84 8.58 4 5 0 124.31 8.60 -4 -5 0 135.18 8.62 4 5 0 145.79 8.59 -5 4 0 138.80 8.63 5 -4 0 136.01 8.61 5 -5 0 106.85 6.17 5 5 0 103.06 6.17 5 5 0 104.31 6.12 -5 -5 0 99.94 6.11 5 5 0 89.89 6.14 -5 5 0 97.34 6.17 -5 -5 0 105.61 6.15 -5 5 0 112.08 6.15 -5 -5 0 99.43 6.16 5 -5 0 96.54 6.14 5 -6 0 17.22 1.12 5 -6 0 18.80 1.16 -6 -5 0 18.59 1.12 6 5 0 17.84 1.15 -6 -5 0 17.22 1.08 -5 6 0 17.78 1.16 -5 6 0 18.81 1.13 -6 -5 0 16.04 1.14 6 5 0 17.38 1.08 6 5 0 15.54 1.11 -6 -4 0 7.16 0.49 -6 -4 0 7.24 0.52 6 4 0 6.52 0.48 -6 -4 0 6.89 0.45 -4 6 0 6.65 0.53 -6 -4 0 6.71 0.45 6 4 0 6.85 0.52 4 -6 0 6.48 0.48 4 -6 0 6.57 0.52 -4 6 0 7.10 0.49 6 3 0 272.96 17.68 -6 -3 0 285.90 17.71 3 -6 0 306.04 17.71 -6 -3 0 301.59 17.69 -3 6 0 314.27 17.69 3 -6 0 273.88 17.68 -3 6 0 285.44 17.71 6 3 0 317.39 17.71 -6 -3 0 290.00 17.66 -6 -2 0 21.38 1.29 2 -6 0 21.60 1.28 -2 6 0 23.00 1.32 6 2 0 20.42 1.31 6 2 0 20.41 1.30 -6 -2 0 20.01 1.33 -2 6 0 20.08 1.28 2 -6 0 19.80 1.31 -6 -2 0 22.31 1.31 -2 6 0 20.13 1.34 -6 -2 0 21.26 1.29 6 2 0 21.97 1.34 -6 -1 0 0.25 0.12 6 1 0 0.30 0.09 6 1 0 0.19 0.12 1 -6 0 0.21 0.07 -6 -1 0 0.20 0.07 1 -6 0 0.42 0.09 -1 6 0 0.24 0.11 -1 6 0 0.07 0.08 -6 -1 0 0.19 0.08 -1 6 0 0.30 0.11 6 1 0 0.28 0.09 -1 6 0 0.22 0.06 0 6 0 544.24 32.73 6 0 0 545.53 32.73 1 6 0 0.34 0.13 1 6 0 0.34 0.09 -1 -6 0 0.30 0.08 -1 -6 0 0.14 0.11 1 6 0 0.35 0.08 -1 -6 0 0.15 0.08 6 -1 0 0.17 0.13 6 -1 0 0.10 0.08 -6 1 0 0.31 0.08 6 -1 0 0.10 0.07 -6 1 0 0.28 0.09 -6 1 0 0.32 0.12 2 6 0 19.78 1.30 -6 2 0 20.85 1.29 -6 2 0 22.49 1.31 -2 -6 0 20.36 1.33 6 -2 0 21.26 1.34 6 -2 0 20.24 1.29 2 6 0 21.09 1.33 2 6 0 22.37 1.30 -6 2 0 19.77 1.34 -2 -6 0 21.05 1.30 -2 -6 0 22.49 1.31 6 -2 0 20.94 1.32 -3 -6 0 310.95 17.64 -3 -6 0 288.20 17.66 -6 3 0 285.34 17.66 6 -3 0 301.90 17.66 3 6 0 262.60 17.63 3 6 0 298.73 17.66 6 -3 0 276.72 17.64 -6 3 0 322.21 17.64 6 -4 0 6.58 0.43 -4 -6 0 6.54 0.51 -4 -6 0 6.71 0.44 -4 -6 0 7.24 0.48 6 -4 0 6.82 0.53 4 6 0 6.93 0.45 -6 4 0 7.12 0.48 4 6 0 7.28 0.52 4 6 0 6.27 0.47 6 -4 0 6.34 0.48 -6 4 0 6.54 0.52 -6 4 0 6.71 0.43 6 -5 0 17.25 1.10 5 6 0 17.35 1.06 5 6 0 17.12 1.12 -6 5 0 19.20 1.10 5 6 0 15.43 1.09 -6 5 0 16.64 1.13 -5 -6 0 16.08 1.12 -5 -6 0 16.66 1.05 6 -5 0 18.01 1.13 6 6 0 114.21 6.54 -6 -6 0 104.25 6.53 6 -6 0 112.35 6.54 6 6 0 114.02 6.47 6 -6 0 99.34 6.51 -6 6 0 100.45 6.55 -6 -6 0 106.86 6.47 -6 6 0 118.58 6.51 -6 -6 0 111.50 6.51 6 6 0 92.29 6.51 7 6 0 75.96 4.29 6 -7 0 67.05 4.33 7 6 0 62.55 4.33 7 6 0 69.75 4.36 -7 -6 0 74.12 4.34 -7 -6 0 68.71 4.36 -7 -6 0 75.23 4.30 -7 -6 0 71.49 4.29 -6 7 0 66.90 4.37 -6 7 0 78.17 4.35 -5 7 0 5.77 0.52 -7 -5 0 6.02 0.41 -7 -5 0 6.40 0.47 -5 7 0 6.83 0.48 7 5 0 6.50 0.52 -7 -5 0 6.21 0.41 7 5 0 5.22 0.45 -7 -5 0 6.13 0.51 5 -7 0 6.05 0.47 4 -7 0 110.31 7.06 -4 7 0 112.84 7.09 -7 -4 0 121.74 7.06 -4 7 0 125.07 7.06 -7 -4 0 115.53 7.03 -7 -4 0 114.26 7.08 7 4 0 111.37 7.06 4 -7 0 121.60 7.09 7 4 0 119.53 7.09 -7 -4 0 114.91 7.03 -3 7 0 93.21 5.91 -3 7 0 97.83 5.90 -7 -3 0 93.75 5.90 7 3 0 105.01 5.91 -7 -3 0 100.44 5.88 3 -7 0 91.71 5.88 -7 -3 0 95.69 5.86 -7 -3 0 97.80 5.85 7 3 0 92.78 5.88 3 -7 0 97.11 5.91 -3 7 0 102.77 5.88 -2 7 0 198.30 12.55 2 -7 0 193.13 12.58 -2 7 0 224.94 12.58 7 2 0 217.25 12.61 -2 7 0 207.47 12.61 7 2 0 199.28 12.57 -7 -2 0 207.04 12.60 -7 -2 0 206.50 12.56 7 2 0 199.40 12.58 -2 7 0 217.69 12.61 2 -7 0 211.80 12.55 -7 -2 0 224.84 12.58 -1 7 0 129.53 7.85 7 1 0 120.74 7.81 1 -7 0 119.57 7.81 -1 7 0 120.87 7.79 7 1 0 140.01 7.85 7 1 0 127.08 7.81 1 -7 0 130.68 7.80 -7 -1 0 138.30 7.82 -1 7 0 129.84 7.84 -7 -1 0 131.21 7.85 -7 -1 0 132.97 7.80 -1 7 0 134.11 7.82 7 0 0 0.03 0.10 0 -7 0 0.13 0.12 0 7 0 0.09 0.13 -7 0 0 0.06 0.08 0 -7 0 0.11 0.09 7 0 0 0.16 0.09 7 0 0 0.22 0.15 -7 0 0 0.02 0.12 -7 0 0 0.10 0.09 0 7 0 0.16 0.08 0 7 0 0.18 0.10 0 -7 0 0.07 0.08 1 7 0 128.99 7.80 1 7 0 120.11 7.77 -7 1 0 135.61 7.78 1 7 0 136.98 7.78 7 -1 0 129.13 7.78 -7 1 0 130.70 7.77 -1 -7 0 127.33 7.80 -7 1 0 124.82 7.81 7 -1 0 122.04 7.77 7 -1 0 131.99 7.81 -1 -7 0 125.12 7.77 -1 -7 0 134.54 7.77 -7 2 0 213.29 12.51 -2 -7 0 204.71 12.55 7 -2 0 204.59 12.50 -2 -7 0 215.65 12.52 2 7 0 208.60 12.55 -2 -7 0 198.77 12.51 7 -2 0 196.57 12.52 2 7 0 217.19 12.51 7 -2 0 226.74 12.56 -7 2 0 222.27 12.52 2 7 0 188.37 12.51 -7 2 0 199.63 12.55 3 7 0 88.25 5.81 -3 -7 0 96.39 5.84 3 7 0 97.85 5.84 -7 3 0 101.71 5.81 -3 -7 0 101.69 5.81 -7 3 0 95.99 5.85 -3 -7 0 92.41 5.79 7 -3 0 92.29 5.78 7 -3 0 88.53 5.81 7 -3 0 96.94 5.84 -7 3 0 98.24 5.79 3 7 0 102.04 5.80 -7 4 0 122.29 7.14 -4 -7 0 116.02 7.20 7 -4 0 117.25 7.14 4 7 0 116.74 7.19 7 -4 0 120.82 7.21 4 7 0 117.95 7.15 -4 -7 0 124.81 7.17 7 -4 0 118.60 7.18 -7 4 0 114.58 7.21 -7 4 0 132.37 7.18 4 7 0 109.78 7.17 -4 -7 0 112.23 7.14 -5 -7 0 6.04 0.42 5 7 0 6.34 0.44 -7 5 0 5.98 0.53 -5 -7 0 5.88 0.51 -7 5 0 6.91 0.41 7 -5 0 6.43 0.41 5 7 0 6.06 0.52 -5 -7 0 6.35 0.48 7 -5 0 5.42 0.52 -7 5 0 6.89 0.48 7 -5 0 6.19 0.54 7 -6 0 67.70 4.23 6 7 0 75.25 4.20 6 7 0 69.73 4.26 -6 -7 0 72.12 4.23 -6 -7 0 66.62 4.25 -7 6 0 67.50 4.27 -6 -7 0 67.34 4.18 -7 6 0 75.01 4.23 6 7 0 62.16 4.22 7 -7 0 53.27 3.43 -7 -7 0 55.74 3.46 7 7 0 61.76 3.39 -7 7 0 53.81 3.47 7 7 0 57.06 3.47 7 7 0 51.73 3.43 -7 -7 0 57.20 3.38 -8 -7 0 0.10 0.09 8 7 0 0.30 0.17 7 -8 0 0.20 0.16 -8 -7 0 0.23 0.12 -7 8 0 0.28 0.23 -8 -7 0 0.39 0.21 -8 -6 0 29.39 1.95 6 -8 0 28.77 1.91 -8 -6 0 32.34 1.87 8 6 0 33.96 2.01 -6 8 0 29.18 1.96 8 6 0 27.82 1.91 -8 -6 0 31.81 1.86 -5 8 0 25.37 1.64 5 -8 0 24.29 1.60 -8 -5 0 26.14 1.55 -8 -5 0 25.60 1.64 -8 -5 0 25.82 1.56 8 5 0 23.65 1.59 8 5 0 25.90 1.64 -4 8 0 0.32 0.19 8 4 0 0.23 0.12 4 -8 0 -0.10 0.17 -8 -4 0 0.40 0.15 -8 -4 0 0.55 0.12 -4 8 0 0.59 0.17 4 -8 0 0.38 0.14 -8 -4 0 0.44 0.10 8 4 0 0.47 0.20 -3 8 0 49.18 2.85 -8 -3 0 46.38 2.88 -3 8 0 44.11 2.88 -8 -3 0 46.68 2.82 -8 -3 0 48.64 2.85 -3 8 0 46.12 2.80 3 -8 0 43.34 2.80 -3 8 0 45.25 2.87 -8 -3 0 46.72 2.81 8 3 0 46.97 2.88 -8 -2 0 150.30 8.98 8 2 0 157.22 9.04 8 2 0 139.15 9.00 8 2 0 143.58 8.99 -8 -2 0 143.61 9.03 -2 8 0 139.51 8.97 -2 8 0 162.94 9.01 -2 8 0 153.09 9.03 2 -8 0 139.97 9.00 -8 -2 0 157.81 9.01 2 -8 0 153.90 8.97 -8 -1 0 41.95 2.41 -1 8 0 37.85 2.44 -1 8 0 36.79 2.38 -8 -1 0 38.11 2.45 8 1 0 40.45 2.45 1 -8 0 40.08 2.39 -1 8 0 41.24 2.42 1 -8 0 37.08 2.41 -8 -1 0 40.92 2.39 8 1 0 38.13 2.40 -1 8 0 38.83 2.44 8 1 0 38.37 2.41 0 -8 0 130.88 8.20 0 8 0 146.64 8.21 -8 0 0 131.64 8.24 0 -8 0 131.57 8.23 0 8 0 126.83 8.19 8 0 0 132.37 8.20 8 0 0 145.18 8.25 8 0 0 131.01 8.20 0 8 0 134.92 8.23 0 -8 0 136.10 8.19 -8 0 0 140.41 8.20 -8 0 0 142.95 8.20 -8 1 0 39.72 2.39 -8 1 0 40.36 2.38 1 8 0 42.02 2.39 1 8 0 38.88 2.43 -1 -8 0 39.51 2.38 -1 -8 0 37.97 2.38 8 -1 0 39.69 2.43 8 -1 0 37.15 2.38 8 -1 0 38.58 2.40 1 8 0 35.96 2.38 -1 -8 0 39.00 2.43 -8 1 0 37.68 2.43 2 8 0 136.50 8.97 -8 2 0 145.17 9.01 2 8 0 152.54 9.01 -2 -8 0 152.04 8.97 -2 -8 0 146.96 9.01 -2 -8 0 141.95 8.96 8 -2 0 157.46 9.02 8 -2 0 140.62 8.95 2 8 0 158.17 8.97 8 -2 0 140.52 8.98 -8 2 0 160.79 8.97 -8 2 0 152.49 8.96 -8 3 0 49.54 2.82 -3 -8 0 39.40 2.90 8 -3 0 46.22 2.82 -3 -8 0 49.20 2.84 3 8 0 44.78 2.84 -8 3 0 48.83 2.85 -3 -8 0 44.76 2.82 3 8 0 47.72 2.83 3 8 0 45.96 2.88 8 -3 0 46.27 2.85 8 -3 0 47.03 2.89 8 -4 0 0.50 0.10 4 8 0 0.29 0.20 -8 4 0 0.39 0.14 4 8 0 0.41 0.14 -4 -8 0 0.49 0.10 -4 -8 0 0.50 0.18 8 -4 0 0.39 0.20 -8 4 0 0.21 0.18 4 8 0 0.46 0.13 -4 -8 0 0.48 0.15 -8 4 0 0.30 0.09 -8 5 0 25.20 1.70 -5 -8 0 27.54 1.66 8 -5 0 26.90 1.60 -8 5 0 29.00 1.60 -8 5 0 27.69 1.66 -5 -8 0 25.16 1.69 5 8 0 25.82 1.70 5 8 0 27.06 1.63 5 8 0 23.65 1.65 -5 -8 0 25.73 1.61 8 -5 0 24.54 1.66 6 8 0 28.59 1.90 -6 -8 0 31.15 1.86 -8 6 0 29.63 1.96 -6 -8 0 30.89 1.95 6 8 0 32.16 1.87 8 -6 0 29.39 1.91 -7 -8 0 0.13 0.20 7 8 0 0.17 0.12 8 -7 0 0.29 0.17 -7 -8 0 0.14 0.10 -8 7 0 0.16 0.23 7 8 0 0.19 0.16 8 8 0 1.47 0.25 8 8 0 1.80 0.22 -8 -8 0 1.47 0.18 8 -8 0 1.17 0.23 -8 8 0 1.72 0.32 -8 -8 0 1.79 0.30 -8 9 0 27.38 1.85 8 -9 0 26.78 1.79 9 8 0 26.77 1.79 -9 -8 0 28.40 1.71 -9 -8 0 29.84 1.72 -9 -8 0 27.91 1.83 -7 9 0 8.10 0.75 -9 -7 0 9.39 0.60 9 7 0 8.85 0.68 7 -9 0 8.59 0.68 -9 -7 0 9.22 0.74 -9 -7 0 9.67 0.60 -9 -6 0 2.10 0.21 -6 9 0 1.76 0.32 -9 -6 0 1.71 0.20 -9 -6 0 1.85 0.30 9 6 0 1.48 0.23 6 -9 0 1.59 0.24 5 -9 0 20.70 1.39 -9 -5 0 21.54 1.43 -9 -5 0 22.33 1.34 9 5 0 20.56 1.39 -9 -5 0 22.69 1.34 -5 9 0 21.44 1.44 9 4 0 0.73 0.18 4 -9 0 0.75 0.17 9 4 0 0.72 0.24 -9 -4 0 0.90 0.13 -9 -4 0 0.70 0.14 -9 -4 0 0.57 0.22 -4 9 0 0.75 0.23 3 -9 0 35.17 2.04 9 3 0 33.99 2.14 -9 -3 0 35.10 2.10 -9 -3 0 34.88 2.07 -9 -3 0 34.85 2.05 -9 -3 0 33.14 2.13 9 3 0 32.73 2.09 -3 9 0 30.83 2.13 -3 9 0 34.55 2.10 -3 9 0 32.62 2.04 3 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20.36 1.20 2 9 0 17.76 1.19 -9 2 0 20.03 1.18 2 9 0 17.03 1.23 9 -2 0 18.74 1.25 -2 -9 0 17.87 1.24 2 9 0 19.70 1.19 -9 3 0 35.90 2.09 -3 -9 0 32.88 2.12 -9 3 0 35.09 2.06 3 9 0 36.05 2.08 3 9 0 31.92 2.08 3 9 0 31.48 2.12 9 -3 0 33.03 2.06 -3 -9 0 33.58 2.06 -3 -9 0 35.18 2.08 -9 3 0 31.11 2.13 9 -3 0 32.51 2.13 -9 4 0 0.59 0.23 9 -4 0 0.76 0.13 4 9 0 0.65 0.17 -4 -9 0 0.78 0.17 9 -4 0 0.59 0.18 -4 -9 0 0.66 0.13 -4 -9 0 0.68 0.22 -9 4 0 0.57 0.17 -9 4 0 0.92 0.14 4 9 0 0.80 0.16 5 9 0 20.12 1.41 -9 5 0 23.83 1.36 5 9 0 22.90 1.39 -5 -9 0 21.55 1.45 9 -5 0 21.04 1.42 9 -5 0 23.07 1.36 -5 -9 0 22.54 1.37 -9 5 0 20.84 1.47 -6 -9 0 1.82 0.19 -9 6 0 1.45 0.29 6 9 0 1.74 0.24 -6 -9 0 1.60 0.29 6 9 0 1.52 0.23 9 -6 0 1.57 0.24 9 -7 0 9.04 0.71 -7 -9 0 8.99 0.74 -7 -9 0 9.53 0.61 7 9 0 10.31 0.64 -9 7 0 9.11 0.77 7 9 0 8.38 0.69 -8 -9 0 28.90 1.70 8 9 0 29.92 1.72 -8 -9 0 26.04 1.81 -9 8 0 27.44 1.84 8 9 0 25.55 1.77 9 -8 0 27.49 1.79 9 9 0 31.64 2.07 9 -9 0 31.14 2.07 -9 -9 0 35.57 2.00 -9 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1.42 0.18 -10 4 0 1.62 0.21 -4 -10 0 1.29 0.27 4 10 0 1.64 0.21 4 10 0 1.48 0.22 -10 5 0 22.62 1.56 10 -5 0 24.85 1.45 5 10 0 23.97 1.47 -5 -10 0 23.22 1.45 -5 -10 0 21.41 1.54 5 10 0 22.02 1.50 -10 5 0 25.32 1.45 10 -5 0 22.96 1.51 -10 6 0 3.21 0.25 6 10 0 2.83 0.35 10 -6 0 2.42 0.33 10 -6 0 2.83 0.25 6 10 0 3.01 0.31 -6 -10 0 2.51 0.35 -6 -10 0 2.66 0.26 -10 6 0 3.43 0.47 10 -7 0 27.73 1.79 -10 7 0 27.56 1.85 -7 -10 0 27.99 1.70 -7 -10 0 27.38 1.82 7 10 0 25.46 1.77 7 10 0 29.75 1.73 -8 -10 0 23.73 1.42 10 -8 0 22.85 1.52 -8 -10 0 21.99 1.55 8 10 0 21.08 1.50 -10 8 0 22.00 1.58 8 10 0 25.06 1.44 9 10 0 10.36 0.80 9 10 0 11.28 0.71 10 -9 0 9.60 0.81 -9 -10 0 10.45 0.86 -10 9 0 10.56 0.91 -9 -10 0 10.53 0.68 10 10 0 46.92 3.02 -10 -10 0 50.28 2.92 10 -10 0 45.50 3.03 -10 -10 0 46.60 3.06 -10 -10 0 51.15 2.94 -10 10 0 47.56 3.10 -11 -10 0 0.63 0.14 -11 -10 0 0.37 0.13 -11 -10 0 0.27 0.30 -11 -9 0 18.08 1.11 -9 11 0 16.52 1.35 -11 -9 0 17.96 1.29 -11 -9 0 18.11 1.12 -11 -8 0 19.76 1.22 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11 -6 0 53.65 3.12 -11 6 0 50.56 3.25 6 11 0 51.38 3.14 6 11 0 48.83 3.18 -6 -11 0 49.58 3.22 -6 -11 0 51.46 3.12 -7 -11 0 1.95 0.24 -7 -11 0 1.88 0.35 7 11 0 1.62 0.29 11 -7 0 1.90 0.30 -11 7 0 2.35 0.41 7 11 0 2.34 0.25 8 11 0 20.84 1.25 -8 -11 0 19.56 1.38 11 -8 0 19.28 1.34 -8 -11 0 19.88 1.23 -11 8 0 19.24 1.41 8 11 0 18.69 1.32 -11 9 0 17.58 1.34 -9 -11 0 18.12 1.30 9 11 0 18.76 1.16 -9 -11 0 18.34 1.13 11 -9 0 17.45 1.26 9 11 0 17.81 1.24 10 11 0 0.21 0.25 -10 -11 0 0.55 0.13 -10 -11 0 0.21 0.31 -10 -11 0 0.43 0.17 11 -10 0 0.31 0.27 -11 10 0 0.23 0.33 -11 -11 0 50.07 3.33 -11 -11 0 55.68 3.17 11 11 0 47.79 3.28 -11 -11 0 54.10 3.16 -12 -11 0 48.79 3.15 -12 -10 0 3.80 0.52 -12 -9 0 0.13 0.12 -12 -9 0 -0.12 0.29 -12 -9 0 0.19 0.13 8 -12 0 0.06 0.22 -12 -8 0 0.11 0.13 -12 -8 0 0.12 0.27 -12 -8 0 -0.05 0.11 7 -12 0 16.80 1.17 -7 12 0 16.95 1.26 -12 -7 0 17.09 1.08 -12 -7 0 16.21 1.23 12 7 0 15.96 1.17 -12 -7 0 18.35 1.07 -12 -6 0 4.06 0.37 -12 -6 0 4.09 0.34 -6 12 0 3.87 0.55 12 6 0 4.15 0.46 -12 -6 0 4.27 0.55 6 -12 0 4.30 0.47 12 5 0 111.49 6.84 -12 -5 0 109.21 6.88 -12 -5 0 119.38 6.78 -5 12 0 106.31 6.89 -12 -5 0 117.31 6.79 5 -12 0 109.46 6.84 -12 -4 0 1.26 0.33 4 -12 0 1.35 0.25 -12 -4 0 1.77 0.20 -12 -4 0 1.75 0.23 12 4 0 1.74 0.27 -4 12 0 2.20 0.37 -12 -3 0 12.02 0.78 12 3 0 11.53 0.84 3 -12 0 13.10 0.77 -12 -3 0 11.48 0.80 -3 12 0 11.94 0.76 -12 -3 0 9.94 0.89 3 -12 0 11.13 0.83 -3 12 0 12.51 0.76 -3 12 0 10.89 0.90 -2 12 0 2.92 0.28 -12 -2 0 3.41 0.31 12 2 0 2.92 0.36 2 -12 0 3.24 0.29 -2 12 0 2.55 0.37 12 2 0 3.06 0.36 2 -12 0 2.72 0.35 -12 -2 0 2.20 0.36 -12 -1 0 17.25 1.07 -12 -1 0 14.90 1.16 12 1 0 16.71 1.10 -1 12 0 15.47 1.17 1 -12 0 15.70 1.09 12 1 0 17.97 1.11 1 -12 0 17.50 1.06 -1 12 0 16.35 1.06 0 -12 0 6.12 0.53 0 12 0 6.74 0.63 12 0 0 6.70 0.56 12 0 0 7.09 0.53 -12 0 0 6.41 0.64 -12 0 0 7.22 0.52 0 12 0 6.52 0.51 0 -12 0 7.44 0.51 12 -1 0 16.33 1.07 -12 1 0 16.67 1.07 -1 -12 0 16.63 1.08 -1 -12 0 17.22 1.16 12 -1 0 15.76 1.10 -12 1 0 16.89 1.08 -12 1 0 15.75 1.16 -1 -12 0 15.99 1.07 1 12 0 16.26 1.17 -12 2 0 2.87 0.41 2 12 0 3.03 0.34 12 -2 0 2.74 0.31 12 -2 0 3.03 0.39 -12 2 0 3.22 0.34 -2 -12 0 3.03 0.34 -2 -12 0 3.07 0.32 2 12 0 3.00 0.37 -2 -12 0 3.14 0.41 -3 -12 0 11.32 0.79 12 -3 0 11.87 0.87 12 -3 0 12.20 0.81 -12 3 0 11.32 0.92 3 12 0 12.36 0.84 -3 -12 0 11.82 0.91 3 12 0 11.34 0.82 -12 3 0 12.78 0.81 -4 -12 0 1.58 0.22 4 12 0 1.65 0.26 4 12 0 1.80 0.27 -12 4 0 1.93 0.28 -12 4 0 1.58 0.34 -4 -12 0 1.45 0.32 12 -4 0 1.72 0.30 12 -4 0 1.74 0.27 12 -5 0 118.40 6.89 5 12 0 116.16 6.91 -5 -12 0 112.11 6.99 -5 -12 0 114.68 6.90 5 12 0 108.53 6.94 -12 5 0 119.86 6.89 -12 5 0 110.54 7.00 12 -5 0 111.78 6.96 -12 6 0 4.91 0.36 -12 6 0 4.32 0.58 -6 -12 0 3.90 0.55 12 -6 0 4.14 0.50 12 -6 0 4.27 0.37 -6 -12 0 3.99 0.37 6 12 0 4.45 0.42 6 12 0 4.07 0.45 -7 -12 0 17.62 1.11 12 -7 0 18.61 1.11 7 12 0 17.61 1.20 -12 7 0 16.28 1.29 -7 -12 0 16.10 1.25 7 12 0 17.64 1.14 12 -7 0 17.90 1.23 -8 -12 0 0.09 0.29 8 12 0 0.14 0.20 12 -8 0 0.19 0.24 -12 8 0 0.09 0.34 -8 -12 0 0.06 0.15 8 12 0 0.22 0.23 -12 9 0 0.44 0.33 12 -9 0 0.10 0.26 -9 -12 0 0.33 0.30 9 12 0 0.09 0.24 -9 -12 0 0.11 0.14 9 12 0 0.05 0.16 10 12 0 3.98 0.35 -10 -12 0 4.36 0.35 12 -10 0 4.45 0.56 10 12 0 4.21 0.54 -10 -12 0 3.77 0.52 -12 10 0 4.34 0.60 -11 -12 0 46.52 3.12 12 -11 0 47.71 3.09 -12 11 0 46.95 3.18 -11 -12 0 52.64 2.94 11 12 0 47.14 3.07 -12 12 0 15.61 1.31 -12 -12 0 15.44 1.25 12 12 0 15.96 1.18 12 -12 0 15.37 1.20 13 12 0 28.76 1.92 -13 -12 0 27.20 1.99 12 -13 0 29.10 1.94 -12 13 0 27.74 2.04 -13 -11 0 9.30 0.94 -13 -10 0 19.63 1.46 -13 -9 0 6.43 0.46 -13 -9 0 6.54 0.74 -13 -8 0 0.59 0.16 -13 -8 0 0.68 0.34 8 -13 0 0.46 0.25 -13 -8 0 0.48 0.14 -13 -7 0 14.39 0.91 7 -13 0 13.38 1.01 -13 -7 0 13.20 1.07 -13 -7 0 14.46 0.89 13 7 0 13.34 1.02 -13 -6 0 56.29 3.23 13 6 0 53.30 3.32 -13 -6 0 49.68 3.36 -13 -6 0 54.18 3.24 6 -13 0 50.98 3.31 13 5 0 5.66 0.54 -13 -5 0 5.51 0.41 5 -13 0 5.29 0.53 -13 -5 0 5.06 0.62 -5 13 0 5.15 0.64 -13 -5 0 5.44 0.47 4 -13 0 105.15 6.65 -13 -4 0 104.52 6.70 13 4 0 109.94 6.66 -13 -4 0 115.19 6.59 -4 13 0 107.80 6.72 -13 -4 0 111.60 6.61 -13 -3 0 3.50 0.38 13 3 0 3.30 0.42 -3 13 0 2.98 0.43 -3 13 0 3.57 0.31 -13 -3 0 2.85 0.33 3 -13 0 3.77 0.41 -13 -3 0 3.25 0.44 -3 13 0 3.50 0.31 -13 -2 0 68.61 4.20 -13 -2 0 71.99 4.18 -2 13 0 68.97 4.17 13 2 0 67.21 4.22 2 -13 0 75.14 4.18 -13 -2 0 64.94 4.27 -2 13 0 68.52 4.29 13 2 0 68.36 4.21 2 -13 0 63.53 4.21 1 -13 0 34.17 2.22 13 1 0 34.78 2.23 13 1 0 33.94 2.23 -13 -1 0 37.31 2.20 1 -13 0 38.56 2.20 -1 13 0 35.72 2.19 -13 -1 0 33.67 2.30 -1 13 0 34.79 2.30 -13 0 0 0.16 0.17 0 13 0 0.06 0.24 0 -13 0 0.00 0.16 0 -13 0 0.20 0.17 13 0 0 0.14 0.20 13 0 0 -0.05 0.17 0 13 0 0.17 0.16 -13 0 0 0.40 0.27 1 13 0 33.98 2.14 -1 -13 0 32.98 2.15 -1 -13 0 34.10 2.23 -13 1 0 33.88 2.24 -1 -13 0 34.69 2.14 13 -1 0 35.83 2.18 1 13 0 34.28 2.23 13 -1 0 35.04 2.15 13 -2 0 69.13 4.27 2 13 0 66.24 4.23 -13 2 0 77.76 4.27 -2 -13 0 70.89 4.31 13 -2 0 68.05 4.23 -2 -13 0 66.28 4.23 -13 2 0 66.58 4.32 -13 3 0 3.41 0.38 -3 -13 0 3.22 0.45 13 -3 0 3.44 0.46 13 -3 0 3.46 0.35 -13 3 0 3.28 0.47 3 13 0 3.51 0.39 -3 -13 0 3.16 0.34 -13 4 0 108.72 6.77 13 -4 0 109.70 6.72 -4 -13 0 111.67 6.76 4 13 0 109.76 6.68 13 -4 0 114.12 6.66 -4 -13 0 106.19 6.66 -13 4 0 115.28 6.66 4 13 0 104.33 6.69 5 13 0 5.51 0.51 13 -5 0 5.69 0.58 -5 -13 0 4.86 0.43 5 13 0 5.34 0.52 -13 5 0 6.04 0.67 13 -5 0 5.74 0.45 -5 -13 0 4.53 0.60 -13 5 0 5.84 0.44 6 13 0 52.26 3.32 -13 6 0 49.68 3.39 13 -6 0 55.70 3.26 -6 -13 0 51.45 3.37 -13 6 0 56.15 3.25 -6 -13 0 53.23 3.26 6 13 0 53.69 3.28 13 -6 0 53.35 3.35 -7 -13 0 14.36 0.90 7 13 0 13.05 0.93 -13 7 0 12.25 1.09 13 -7 0 14.12 0.89 -13 7 0 14.15 0.88 13 -7 0 13.52 1.03 7 13 0 13.39 0.99 -7 -13 0 12.65 1.06 -8 -13 0 0.46 0.33 8 13 0 0.70 0.20 13 -8 0 0.21 0.27 -13 8 0 0.38 0.34 -8 -13 0 0.23 0.16 8 13 0 0.47 0.25 -9 -13 0 6.94 0.75 9 13 0 7.02 0.57 -13 9 0 5.60 0.78 -9 -13 0 6.84 0.50 13 -9 0 6.66 0.69 9 13 0 6.40 0.65 13 -10 0 19.75 1.42 -10 -13 0 18.34 1.45 -10 -13 0 21.05 1.25 -13 10 0 19.31 1.50 10 13 0 19.69 1.40 -11 -13 0 10.88 0.70 13 -11 0 10.70 0.93 11 13 0 10.30 0.90 -13 11 0 9.60 1.01 -11 -13 0 10.69 0.99 13 -12 0 27.95 1.93 -13 12 0 27.26 2.02 -12 -13 0 28.74 1.99 12 13 0 28.41 1.91 -13 -13 0 1.84 0.51 -13 14 0 23.20 1.78 13 -14 0 22.64 1.66 14 13 0 23.41 1.65 -14 -13 0 22.39 1.73 12 -14 0 0.59 0.40 -12 14 0 0.56 0.53 -14 -12 0 0.31 0.46 14 12 0 0.62 0.38 -14 -11 0 4.65 0.65 -11 14 0 5.54 0.74 14 11 0 5.41 0.66 11 -14 0 4.88 0.67 -14 -10 0 0.54 0.40 -14 -9 0 6.34 0.45 -14 -9 0 5.94 0.76 -14 -8 0 3.93 0.36 -14 -8 0 3.37 0.52 -14 -7 0 27.44 2.04 -14 -7 0 31.22 1.89 -14 -7 0 31.73 1.87 6 -14 0 7.77 0.72 14 6 0 8.75 0.74 -14 -6 0 8.76 0.65 -14 -6 0 8.66 0.84 -14 -6 0 9.39 0.60 -14 -5 0 40.09 2.40 -14 -5 0 36.45 2.52 5 -14 0 36.94 2.46 14 5 0 38.47 2.47 -14 -5 0 40.95 2.38 -4 14 0 0.30 0.29 -14 -4 0 0.40 0.32 4 -14 0 0.51 0.22 14 4 0 0.60 0.24 -14 -4 0 0.60 0.17 -14 -4 0 0.45 0.22 -14 -3 0 61.40 3.87 -3 14 0 60.37 3.94 14 3 0 62.96 3.88 -3 14 0 65.47 3.81 -14 -3 0 56.85 3.92 3 -14 0 61.06 3.87 -14 -3 0 66.27 3.82 -3 14 0 64.98 3.80 -2 14 0 1.29 0.21 2 -14 0 1.48 0.21 14 2 0 0.96 0.25 2 -14 0 1.27 0.25 -14 -2 0 0.91 0.34 -14 -2 0 1.12 0.23 14 2 0 1.10 0.27 -2 14 0 1.12 0.34 -14 -2 0 1.04 0.22 -1 14 0 4.31 0.41 -1 14 0 3.92 0.57 1 -14 0 4.14 0.45 -14 -1 0 3.86 0.56 14 1 0 4.26 0.48 14 1 0 4.56 0.46 1 -14 0 4.64 0.41 0 14 0 71.97 4.57 0 -14 0 77.18 4.47 14 0 0 73.76 4.51 14 0 0 75.42 4.49 0 14 0 73.07 4.47 -14 0 0 69.73 4.57 0 -14 0 71.28 4.49 14 -1 0 4.62 0.51 1 14 0 4.16 0.56 1 14 0 4.31 0.42 -1 -14 0 4.55 0.43 14 -1 0 4.37 0.44 -14 1 0 4.13 0.54 -14 2 0 0.85 0.32 -2 -14 0 1.34 0.37 2 14 0 0.99 0.23 2 14 0 0.97 0.33 -2 -14 0 1.40 0.23 14 -2 0 1.10 0.29 14 -2 0 1.06 0.22 -14 3 0 61.98 3.89 3 14 0 60.92 3.79 -3 -14 0 61.19 3.87 -3 -14 0 59.04 3.77 14 -3 0 63.79 3.83 14 -3 0 62.32 3.77 14 -4 0 0.50 0.18 -14 4 0 0.31 0.33 -14 4 0 0.52 0.21 4 14 0 0.15 0.23 14 -4 0 0.32 0.29 -4 -14 0 0.41 0.18 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0.61 -2 15 0 8.69 0.82 15 2 0 8.13 0.68 -2 15 0 8.60 0.61 2 -15 0 7.95 0.67 1 -15 0 42.93 2.58 -1 15 0 41.50 2.71 15 1 0 41.00 2.62 -15 -1 0 40.97 2.70 15 1 0 43.15 2.62 1 -15 0 39.86 2.61 0 -15 0 0.27 0.20 0 15 0 0.50 0.30 15 0 0 0.30 0.21 -15 0 0 0.18 0.32 15 0 0 -0.12 0.25 0 -15 0 -0.02 0.19 0 15 0 0.04 0.19 15 -1 0 42.58 2.64 1 15 0 41.12 2.58 -1 -15 0 40.00 2.59 1 15 0 41.02 2.69 -15 1 0 41.00 2.71 15 -1 0 42.93 2.60 2 15 0 8.20 0.79 -2 -15 0 8.35 0.80 15 -2 0 8.52 0.75 2 15 0 8.81 0.67 15 -2 0 8.76 0.66 -15 2 0 8.12 0.82 -2 -15 0 8.11 0.65 -15 3 0 7.35 0.77 -3 -15 0 7.26 0.75 15 -3 0 7.06 0.58 3 15 0 6.99 0.61 15 -3 0 6.94 0.68 -3 -15 0 6.95 0.57 4 15 0 5.09 0.52 15 -4 0 5.25 0.46 -4 -15 0 5.23 0.67 15 -4 0 4.49 0.60 -4 -15 0 4.99 0.45 -15 4 0 4.32 0.59 -15 5 0 0.09 0.34 15 -5 0 0.60 0.19 -5 -15 0 0.55 0.36 -5 -15 0 0.40 0.18 15 -5 0 0.68 0.34 -15 5 0 0.23 0.21 5 15 0 0.26 0.25 -6 -15 0 8.89 0.62 15 -6 0 7.43 0.79 -6 -15 0 8.00 0.84 15 -6 0 9.43 0.66 -15 6 0 7.31 0.87 6 15 0 8.06 0.72 -15 7 0 4.77 0.65 7 15 0 4.34 0.56 15 -7 0 4.69 0.64 -7 -15 0 4.52 0.41 15 -7 0 4.79 0.46 -7 -15 0 4.40 0.59 -8 -15 0 1.40 0.21 8 15 0 1.13 0.34 15 -8 0 1.54 0.40 -8 -15 0 1.29 0.43 -15 8 0 1.22 0.48 -15 9 0 2.46 0.55 -9 -15 0 2.57 0.36 -9 -15 0 2.29 0.51 15 -9 0 2.20 0.45 9 15 0 2.32 0.42 -10 -15 0 0.86 0.44 -15 10 0 0.40 0.45 -10 -15 0 1.17 0.21 15 -10 0 1.34 0.43 10 15 0 0.83 0.37 -15 11 0 -0.15 0.45 11 15 0 0.22 0.35 -11 -15 0 0.44 0.44 12 15 0 3.61 0.53 -15 12 0 3.28 0.66 15 -12 0 3.07 0.56 15 -13 0 0.57 0.44 -15 13 0 1.01 0.54 13 15 0 1.42 0.45 -13 -15 0 1.21 0.51 -15 14 0 3.32 0.73 -14 -15 0 2.80 0.65 14 15 0 3.57 0.55 15 -14 0 2.93 0.58 -16 -13 0 -0.06 0.52 12 -16 0 0.36 0.38 16 12 0 0.35 0.39 -12 16 0 -0.20 0.48 -16 -12 0 -0.54 0.47 11 -16 0 0.27 0.38 -11 16 0 1.39 0.52 16 11 0 1.06 0.40 -10 16 0 2.16 0.56 -16 -10 0 2.43 0.55 10 -16 0 2.29 0.46 16 10 0 1.81 0.43 -16 -9 0 0.20 0.43 -9 16 0 0.40 0.74 -8 16 0 11.72 1.14 16 8 0 13.07 1.01 -16 -8 0 11.22 1.09 8 -16 0 12.25 1.01 -16 -7 0 13.14 0.88 -16 -7 0 11.57 1.10 7 -16 0 13.54 1.01 16 7 0 12.56 1.01 -7 16 0 11.73 1.13 -16 -6 0 1.33 0.27 16 6 0 1.08 0.33 6 -16 0 0.78 0.30 -16 -6 0 1.07 0.43 -16 -5 0 1.19 0.28 -5 16 0 1.44 0.74 -16 -5 0 0.87 0.40 -16 -4 0 0.99 0.22 -4 16 0 0.53 0.38 -16 -4 0 1.04 0.39 -16 -3 0 3.05 0.39 -16 -3 0 3.25 0.52 -3 16 0 2.68 0.36 3 -16 0 2.68 0.38 16 3 0 3.79 0.49 -16 -2 0 39.44 2.59 -2 16 0 42.92 2.57 -16 -2 0 39.57 2.71 16 2 0 44.18 2.64 2 -16 0 40.85 2.62 16 1 0 4.39 0.52 -1 16 0 4.68 0.47 1 -16 0 4.55 0.51 16 1 0 4.70 0.57 -16 -1 0 5.21 0.70 1 -16 0 5.99 0.46 0 16 0 72.50 4.51 16 0 0 73.74 4.57 0 -16 0 74.16 4.54 -16 0 0 71.47 4.64 16 0 0 77.16 4.55 16 -1 0 4.98 0.50 1 16 0 4.41 0.48 -1 -16 0 4.89 0.49 16 -1 0 4.59 0.59 -16 1 0 4.62 0.62 16 -2 0 42.81 2.65 16 -2 0 43.28 2.72 -2 -16 0 42.04 2.65 -16 2 0 40.90 2.78 2 16 0 42.60 2.66 -3 -16 0 2.99 0.40 -16 3 0 2.66 0.50 16 -3 0 3.04 0.44 3 16 0 3.14 0.45 16 -3 0 2.97 0.41 -3 -16 0 3.12 0.51 16 -4 0 0.90 0.24 4 16 0 1.08 0.28 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0.96 0.34 -17 0 0 0.87 0.40 -1 -17 0 34.66 2.22 1 17 0 34.31 2.35 17 -1 0 35.92 2.23 17 -1 0 35.08 2.28 -17 1 0 35.84 2.37 1 17 0 33.59 2.21 17 -2 0 2.86 0.46 -2 -17 0 3.07 0.42 2 17 0 3.01 0.39 -17 2 0 2.95 0.56 2 17 0 3.33 0.52 17 -2 0 2.94 0.38 -3 -17 0 1.07 0.42 3 17 0 1.18 0.31 17 -3 0 1.01 0.26 -17 3 0 0.91 0.44 -3 -17 0 1.11 0.25 3 17 0 0.87 0.38 17 -3 0 0.95 0.36 -4 -17 0 2.73 0.40 4 17 0 3.97 0.52 -4 -17 0 3.39 0.56 -17 4 0 3.80 0.60 17 -4 0 3.21 0.43 17 -4 0 3.29 0.50 -17 5 0 1.36 0.47 17 -5 0 1.20 0.26 5 17 0 1.30 0.35 -5 -17 0 1.35 0.47 -5 -17 0 1.50 0.26 17 -5 0 1.41 0.41 -6 -17 0 27.63 1.95 17 -6 0 26.64 1.75 -6 -17 0 26.33 1.74 -17 6 0 27.11 1.99 17 -6 0 28.69 1.91 6 17 0 28.56 1.84 7 17 0 6.81 0.73 -17 7 0 6.12 0.81 17 -7 0 7.03 0.62 -7 -17 0 7.24 0.88 -7 -17 0 6.93 0.56 17 -7 0 7.56 0.84 -17 8 0 1.94 0.56 17 -8 0 1.77 0.50 8 17 0 2.26 0.45 -8 -17 0 2.33 0.34 -8 -17 0 2.06 0.54 -17 9 0 14.69 1.36 9 17 0 16.49 1.19 17 -9 0 12.24 1.59 -9 -17 0 14.43 1.28 -10 -17 0 4.46 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27.64 1.98 2 12 4 30.96 1.91 -2 -12 4 31.67 1.98 2 12 4 30.88 1.96 -12 2 4 30.05 1.90 12 -2 4 28.47 1.94 12 -2 4 28.23 1.89 12 -3 -4 14.38 0.98 -12 3 -4 15.05 1.06 -12 3 -4 15.14 0.94 -3 -12 -4 13.16 1.02 -3 -12 -4 13.08 0.94 12 -3 -4 15.29 0.93 3 12 -4 14.72 0.95 3 12 -4 12.36 0.95 12 -3 4 13.64 1.02 -3 -12 4 15.61 1.07 -12 3 4 13.14 1.06 3 12 4 13.90 0.97 -3 -12 4 14.30 0.94 -12 3 4 14.68 0.97 -12 4 -4 134.27 8.52 -12 4 -4 141.43 8.43 4 12 -4 148.79 8.44 -4 -12 -4 140.95 8.51 12 -4 -4 142.57 8.43 4 12 -4 135.57 8.46 -4 -12 -4 133.13 8.44 12 -4 -4 141.20 8.47 -4 -12 4 144.89 8.44 -12 4 4 149.91 8.45 12 -4 4 136.63 8.51 -4 -12 4 133.98 8.53 4 12 4 132.70 8.48 12 -4 4 142.93 8.45 -12 4 4 135.46 8.54 5 12 -4 6.18 0.49 12 -5 -4 6.91 0.51 -12 5 -4 7.76 0.48 12 -5 -4 6.25 0.57 -12 5 -4 6.85 0.66 12 -5 -4 7.29 0.48 -5 -12 -4 5.41 0.62 -5 -12 -4 5.47 0.49 5 12 -4 6.14 0.54 -5 -12 4 6.05 0.66 5 12 4 5.58 0.57 12 -5 4 6.48 0.53 -12 5 4 5.46 0.66 -5 -12 4 6.90 0.49 12 -5 4 6.22 0.63 -12 6 -4 35.39 2.07 -6 -12 -4 31.24 2.09 12 -6 -4 35.91 2.09 6 12 -4 31.70 2.13 -6 -12 -4 31.17 2.18 12 -6 -4 34.17 2.15 6 12 -4 33.71 2.08 -12 6 -4 33.90 2.22 12 -6 -4 35.49 2.07 -6 -12 4 37.28 2.08 6 12 4 31.75 2.15 -6 -12 4 32.98 2.20 6 12 4 33.35 2.13 12 -6 4 35.08 2.10 -12 6 4 31.62 2.22 12 -6 4 32.39 2.18 -7 -12 -4 12.90 0.90 12 -7 -4 13.73 0.99 7 12 -4 14.39 0.88 12 -7 -4 13.81 0.86 -7 -12 -4 12.83 1.03 -12 7 -4 13.65 1.07 -12 7 -4 14.51 0.87 7 12 -4 13.20 0.96 7 12 4 12.64 0.99 -7 -12 4 13.16 1.06 12 -7 4 14.25 0.91 -12 7 4 13.39 1.15 -7 -12 4 15.23 0.88 7 12 4 12.61 0.95 12 -7 4 12.25 1.03 -12 8 -4 2.32 0.42 12 -8 -4 2.78 0.38 8 12 -4 2.32 0.34 -8 -12 -4 2.17 0.29 -8 -12 -4 2.61 0.42 -8 -12 4 3.08 0.47 8 12 4 2.49 0.37 8 12 4 3.15 0.43 12 -8 4 2.06 0.41 -9 -12 -4 3.89 0.54 9 12 -4 4.64 0.51 12 -9 -4 4.75 0.54 -12 9 -4 5.79 0.68 -9 -12 -4 4.13 0.40 9 12 4 5.23 0.57 12 -9 4 4.11 0.60 -9 -12 4 6.04 0.68 9 12 4 5.36 0.53 12 -10 -4 39.42 2.51 -12 10 -4 39.70 2.60 -10 -12 -4 39.48 2.55 -10 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15.36 1.16 -13 -7 -4 14.11 0.97 13 7 -4 13.65 1.03 7 -13 4 12.81 1.05 13 7 4 16.65 1.09 -13 -7 4 16.05 1.15 -7 13 4 13.05 1.14 -13 -6 -4 2.76 0.35 13 6 -4 2.30 0.32 -6 13 -4 1.81 0.42 -13 -6 -4 2.81 0.41 6 -13 -4 2.10 0.31 -13 -6 -4 2.45 0.33 13 6 4 2.13 0.37 6 -13 4 2.78 0.39 -13 -6 4 2.44 0.45 -6 13 4 2.37 0.42 -13 -5 -4 59.14 3.81 13 5 -4 63.22 3.77 -13 -5 -4 59.75 3.74 5 -13 -4 58.23 3.77 -5 13 -4 59.14 3.85 -13 -5 -4 62.21 3.73 5 -13 4 60.54 3.79 -13 -5 4 65.07 3.68 -13 -5 4 58.74 3.84 -5 13 4 60.99 3.84 13 5 4 62.07 3.80 -13 -4 -4 17.57 1.23 -13 -4 -4 16.56 1.24 13 4 -4 17.10 1.26 4 -13 -4 19.23 1.27 -4 13 -4 20.93 1.19 -13 -4 -4 16.27 1.32 -4 13 -4 19.73 1.37 -4 13 -4 21.07 1.21 13 4 4 20.08 1.31 -4 13 4 16.46 1.34 -13 -4 4 20.71 1.21 4 -13 4 16.73 1.28 -13 -4 4 21.91 1.19 -13 -4 4 19.70 1.37 -13 -3 -4 102.55 6.60 -13 -3 -4 98.03 6.55 13 3 -4 106.41 6.56 13 3 -4 107.36 6.52 -3 13 -4 112.44 6.52 3 -13 -4 117.43 6.50 -3 13 -4 105.39 6.63 -13 -3 -4 104.90 6.54 -3 13 -4 112.80 6.50 3 -13 -4 102.16 6.56 -13 -3 4 121.31 6.51 3 -13 4 102.76 6.57 -13 -3 4 105.97 6.63 -3 13 4 103.21 6.62 13 3 4 108.38 6.59 -3 13 4 111.42 6.52 -13 -2 -4 5.62 0.58 2 -13 -4 4.39 0.47 -2 13 -4 4.74 0.44 -13 -2 -4 5.36 0.47 2 -13 -4 5.33 0.40 13 2 -4 6.12 0.48 -2 13 -4 4.13 0.40 13 2 -4 5.94 0.46 -2 13 -4 3.64 0.57 -2 13 4 5.83 0.59 13 2 4 4.00 0.49 -13 -2 4 3.86 0.59 -2 13 4 6.15 0.45 2 -13 4 5.24 0.50 -13 -2 4 5.42 0.42 -1 13 -4 41.68 2.26 13 1 -4 33.86 2.25 13 1 -4 33.41 2.25 -1 13 -4 40.08 2.23 -1 13 -4 38.95 2.36 -13 -1 -4 32.84 2.26 -13 -1 -4 32.08 2.31 1 -13 -4 39.15 2.23 1 -13 -4 37.55 2.27 -13 -1 4 37.15 2.36 1 -13 4 32.59 2.27 -1 13 4 30.26 2.31 -1 13 4 32.87 2.24 13 1 4 38.95 2.29 13 1 4 39.12 2.30 0 -13 -4 0.19 0.18 0 -13 -4 0.05 0.15 0 13 -4 0.14 0.25 0 13 -4 0.37 0.20 13 0 -4 0.35 0.21 13 0 -4 0.23 0.17 -13 0 -4 0.36 0.26 0 13 -4 0.22 0.16 -13 0 4 0.18 0.28 -13 0 4 0.37 0.19 0 13 4 0.23 0.24 0 -13 4 0.15 0.20 0 -13 4 0.35 0.19 0 -13 4 0.41 0.26 13 0 4 0.31 0.20 13 0 4 -0.18 0.22 -1 -13 -4 32.27 2.25 1 13 -4 31.65 2.24 -1 -13 -4 33.09 2.24 13 -1 -4 38.94 2.26 13 -1 -4 38.73 2.28 -13 1 -4 38.32 2.34 1 13 4 37.50 2.34 13 -1 4 33.42 2.30 -1 -13 4 38.52 2.27 13 -1 4 33.64 2.27 -13 1 4 40.58 2.30 -13 1 4 33.19 2.35 1 13 4 38.92 2.27 -1 -13 4 37.97 2.35 13 -2 -4 4.41 0.42 2 13 -4 5.88 0.45 -13 2 -4 3.99 0.56 13 -2 -4 4.19 0.48 2 13 -4 5.88 0.47 -2 -13 -4 4.92 0.45 -2 -13 4 5.27 0.44 13 -2 4 5.47 0.47 -2 -13 4 4.16 0.57 2 13 4 4.25 0.46 -13 2 4 6.10 0.62 2 13 4 3.59 0.54 13 -2 4 5.45 0.55 3 13 -4 112.87 6.47 -13 3 -4 108.76 6.45 13 -3 -4 111.66 6.50 13 -3 -4 115.59 6.46 -3 -13 -4 98.61 6.46 -3 -13 -4 100.69 6.53 3 13 -4 101.76 6.47 -13 3 -4 104.70 6.55 13 -3 4 100.46 6.47 -13 3 4 112.51 6.47 -3 -13 4 114.07 6.47 3 13 4 104.01 6.49 -3 -13 4 108.95 6.56 -13 3 4 99.95 6.56 13 -3 4 102.40 6.52 4 13 -4 16.39 1.23 -4 -13 -4 16.91 1.31 4 13 -4 17.99 1.21 13 -4 -4 20.50 1.27 -4 -13 -4 16.23 1.21 -13 4 -4 20.21 1.20 13 -4 -4 21.86 1.21 -13 4 -4 20.18 1.35 -4 -13 4 20.56 1.22 4 13 4 19.30 1.27 -13 4 4 18.18 1.23 -13 4 4 17.45 1.36 13 -4 4 16.78 1.30 -4 -13 4 20.65 1.36 13 -4 4 16.61 1.24 13 -5 -4 61.72 3.86 -5 -13 -4 62.87 3.90 5 13 -4 63.85 3.81 -5 -13 -4 59.56 3.81 -13 5 -4 61.28 3.92 13 -5 -4 65.82 3.80 13 -5 -4 66.82 3.82 5 13 -4 61.27 3.84 -13 5 -4 60.98 3.79 13 -5 4 64.26 3.82 5 13 4 58.33 3.86 -5 -13 4 58.94 3.92 -13 5 4 59.36 3.94 -5 -13 4 67.17 3.81 13 -5 4 61.43 3.90 -6 -13 -4 2.72 0.42 6 13 -4 3.07 0.40 -13 6 -4 2.10 0.41 13 -6 -4 2.09 0.31 -13 6 -4 2.31 0.29 13 -6 -4 2.50 0.29 13 -6 -4 2.19 0.36 -6 -13 -4 2.70 0.31 6 13 -4 2.82 0.33 13 -6 4 2.85 0.42 6 13 4 1.76 0.34 13 -6 4 2.89 0.37 -6 -13 4 2.24 0.32 -6 -13 4 1.87 0.41 -7 -13 -4 12.91 1.00 -13 7 -4 17.65 0.98 13 -7 -4 16.62 0.99 7 13 -4 13.25 1.06 13 -7 -4 15.55 1.10 7 13 -4 13.80 0.98 13 -7 -4 16.89 0.98 -7 -13 -4 13.37 1.14 -13 7 -4 16.19 1.19 -7 -13 4 15.38 1.18 7 13 4 14.72 1.10 13 -7 4 14.66 1.01 13 -7 4 13.38 1.13 -7 -13 4 17.68 0.99 8 13 -4 3.33 0.30 -8 -13 -4 2.80 0.34 -8 -13 -4 2.96 0.48 -13 8 -4 3.02 0.51 8 13 -4 3.27 0.46 13 -8 -4 3.37 0.49 -13 8 -4 3.46 0.27 13 -8 4 3.28 0.35 8 13 4 2.82 0.42 13 -8 4 3.42 0.49 -8 -13 4 3.91 0.31 -8 -13 4 2.94 0.50 -9 -13 -4 19.25 1.40 -9 -13 -4 19.00 1.23 13 -9 -4 19.55 1.35 9 13 -4 19.35 1.33 -13 9 -4 19.02 1.44 9 13 4 19.33 1.37 -9 -13 4 19.04 1.43 13 -9 4 19.11 1.41 -10 -13 -4 3.19 0.51 -10 -13 -4 2.80 0.34 10 13 -4 3.39 0.45 13 -10 -4 4.06 0.56 -13 10 -4 3.77 0.57 -10 -13 4 3.63 0.56 10 13 4 3.85 0.58 13 -10 4 3.20 0.51 11 13 -4 44.24 2.79 -11 -13 -4 47.72 2.85 -13 11 -4 40.11 2.87 13 -11 -4 41.65 2.79 -11 -13 -4 44.91 2.67 13 -11 4 45.96 2.86 -11 -13 4 39.08 2.85 11 13 4 43.21 2.82 -13 12 -4 1.00 0.46 12 13 -4 1.75 0.39 13 -12 -4 0.96 0.38 -12 -13 -4 1.72 0.44 13 -12 4 2.36 0.49 12 13 4 1.09 0.41 -13 12 4 1.32 0.49 -12 -13 4 1.01 0.46 13 13 -4 32.89 2.30 -13 -13 -4 40.13 2.39 13 -13 -4 28.47 2.31 -13 -13 -4 35.88 2.18 -13 -13 4 33.76 2.41 -13 13 4 37.77 2.43 13 13 4 31.87 2.35 13 -13 4 37.37 2.37 -13 14 -4 0.35 0.52 -14 -13 -4 -0.13 0.44 14 13 -4 0.24 0.35 13 -14 -4 0.53 0.38 14 13 4 0.68 0.41 13 -14 4 0.00 0.38 -13 14 4 0.50 0.49 -14 -13 4 0.16 0.46 12 -14 -4 15.44 1.30 -14 -12 -4 18.87 1.40 14 12 -4 20.26 1.32 -12 14 -4 13.60 1.58 -14 -12 4 16.08 1.49 -12 14 4 18.49 1.47 12 -14 4 18.97 1.38 14 12 4 15.89 1.34 -11 14 -4 2.85 0.57 -14 -11 -4 2.88 0.54 11 -14 -4 2.80 0.45 14 11 -4 2.74 0.44 11 -14 4 2.37 0.48 -11 14 4 2.61 0.61 -14 -11 4 3.37 0.57 14 11 4 2.78 0.49 14 10 -4 27.83 2.15 -14 -10 -4 31.91 2.10 -10 14 -4 31.12 2.15 -10 14 4 31.90 2.15 -14 -10 4 28.33 2.11 10 -14 4 32.06 2.08 -14 -9 -4 0.66 0.40 14 9 -4 0.88 0.35 -9 14 -4 1.38 0.48 -14 -9 4 1.50 0.45 -9 14 4 1.13 0.41 9 -14 4 1.17 0.38 -14 -8 -4 5.54 0.69 -14 -8 -4 5.29 0.47 -8 14 -4 5.21 0.67 14 8 4 5.21 0.86 -14 -8 4 5.72 0.73 -14 -7 -4 19.54 1.24 -14 -7 -4 19.35 1.25 -14 -7 -4 18.29 1.38 -14 -7 4 18.49 1.41 -14 -6 -4 22.19 1.38 6 -14 -4 18.70 1.41 -14 -6 -4 21.64 1.50 14 6 -4 21.91 1.43 -14 -6 -4 22.09 1.36 -14 -6 4 19.20 1.51 6 -14 4 21.52 1.46 14 6 4 20.61 1.46 -6 14 4 21.77 1.53 14 5 -4 2.14 0.35 -14 -5 -4 2.27 0.30 -14 -5 -4 2.57 0.38 5 -14 -4 3.46 0.44 -14 -5 -4 1.92 0.41 14 5 4 3.25 0.48 -5 14 4 2.13 0.45 -14 -5 4 3.37 0.51 5 -14 4 2.72 0.40 -14 -5 4 3.55 0.26 -14 -5 4 3.45 0.31 -14 -4 -4 56.81 3.81 4 -14 -4 58.40 3.83 14 4 -4 62.59 3.83 -4 14 -4 63.72 3.75 -14 -4 -4 58.43 3.88 -4 14 -4 63.54 3.77 14 4 4 62.26 3.86 -14 -4 4 60.54 3.91 -14 -4 4 70.39 3.76 -14 -4 4 66.54 3.77 4 -14 4 60.10 3.85 -4 14 4 57.92 3.90 -14 -3 -4 1.79 0.40 3 -14 -4 3.51 0.42 -3 14 -4 3.39 0.31 3 -14 -4 2.98 0.30 -14 -3 -4 2.32 0.33 -3 14 -4 3.56 0.37 14 3 4 3.65 0.46 -14 -3 4 3.12 0.48 -14 -3 4 3.30 0.31 -14 -3 4 2.86 0.35 14 2 -4 72.80 4.69 -14 -2 -4 68.55 4.69 14 2 -4 74.27 4.67 -2 14 -4 85.38 4.66 -14 -2 -4 70.71 4.75 2 -14 -4 83.17 4.65 -2 14 -4 81.64 4.68 2 -14 -4 72.65 4.70 -2 14 4 73.23 4.66 -2 14 4 70.53 4.77 -14 -2 4 77.20 4.79 14 2 4 79.50 4.73 -14 -2 4 87.93 4.66 2 -14 4 73.71 4.71 -1 14 -4 4.91 0.52 1 -14 -4 5.47 0.46 1 -14 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22.49 1.56 14 -6 4 23.67 1.44 7 14 -4 18.94 1.34 14 -7 -4 21.48 1.26 -7 -14 -4 19.53 1.42 -7 -14 -4 17.76 1.27 -14 7 -4 17.94 1.27 14 -7 -4 20.30 1.37 7 14 -4 18.83 1.34 -14 7 -4 19.09 1.46 14 -7 -4 21.09 1.25 -7 -14 4 18.50 1.44 -7 -14 4 22.81 1.27 7 14 4 19.48 1.38 14 -7 4 19.68 1.43 14 -7 4 19.74 1.29 -14 8 -4 6.25 0.77 14 -8 -4 6.16 0.64 -8 -14 -4 5.37 0.70 8 14 -4 5.64 0.59 -8 -14 -4 4.95 0.47 -8 -14 4 6.15 0.74 14 -8 4 5.53 0.49 14 -8 4 5.71 0.69 8 14 4 5.68 0.65 -8 -14 4 6.38 0.46 9 14 -4 1.06 0.32 -9 -14 -4 1.20 0.22 -9 -14 -4 1.25 0.40 14 -9 -4 2.07 0.39 -14 9 -4 2.29 0.49 -9 -14 4 1.54 0.45 9 14 4 1.76 0.39 14 -9 4 1.23 0.43 -14 10 -4 29.83 2.14 -10 -14 -4 31.27 2.10 10 14 -4 32.18 2.04 14 -10 -4 30.84 2.05 -10 -14 -4 30.47 1.92 -10 -14 4 29.39 2.12 14 -10 4 31.27 2.11 10 14 4 30.22 2.07 -14 11 -4 2.72 0.58 11 14 -4 2.85 0.45 -11 -14 -4 3.18 0.33 14 -11 -4 1.91 0.45 -11 -14 -4 2.86 0.52 -14 11 4 2.89 0.57 14 -11 4 2.53 0.50 11 14 4 3.04 0.52 -11 -14 4 2.95 0.57 -12 -14 -4 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28 17.25 1.36 -6 1 28 20.35 1.38 -6 2 -28 13.65 1.17 6 -2 -28 13.18 1.04 -2 -6 -28 12.84 1.12 2 6 -28 12.74 1.08 2 6 28 13.12 1.20 -2 -6 28 14.82 1.13 -2 -6 28 13.47 1.00 -6 2 28 13.15 1.00 -6 2 28 12.63 1.10 6 -2 28 12.44 1.17 3 6 -28 15.34 1.19 -6 3 -28 16.28 1.30 6 -3 -28 15.57 1.18 3 6 -28 15.51 1.26 -6 3 28 16.27 1.15 -3 -6 28 15.02 1.26 -6 3 28 16.28 1.26 -3 -6 28 16.69 1.17 6 -3 28 14.94 1.30 3 6 28 15.78 1.33 -4 -6 -28 5.29 0.79 -6 4 -28 3.88 0.64 6 -4 -28 4.15 0.64 4 6 -28 5.58 0.65 -6 4 28 5.99 0.75 -6 4 28 6.33 0.61 -4 -6 28 4.31 0.56 6 -4 28 6.69 0.80 -5 -6 -28 62.53 4.14 -6 5 -28 68.32 4.29 6 -5 -28 69.94 4.09 5 6 -28 58.08 4.10 5 6 -28 62.52 4.04 5 6 28 67.35 4.21 -5 -6 28 72.33 4.10 -6 5 28 60.85 4.04 -6 5 28 65.08 4.13 6 -5 28 63.98 4.16 6 -6 -28 23.80 1.63 6 6 -28 23.62 1.57 6 6 -28 22.15 1.65 -6 -6 -28 23.46 1.72 -6 -6 28 23.62 1.64 -6 6 28 22.89 1.68 -6 6 28 22.32 1.57 6 6 28 23.24 1.78 6 -6 28 24.10 1.71 7 6 -28 26.17 1.86 7 6 -28 27.21 1.75 -7 -6 -28 27.75 1.93 6 -7 -28 23.84 1.88 -6 7 -28 28.67 1.95 6 -7 28 27.70 1.91 7 6 28 25.99 1.99 -6 7 28 27.91 1.89 -6 7 28 26.57 1.79 7 5 -28 17.20 1.32 7 5 -28 17.01 1.20 -7 -5 -28 18.09 1.40 -5 7 -28 16.18 1.36 -5 7 28 16.74 1.20 -5 7 28 18.49 1.36 7 5 28 17.11 1.43 -7 -5 28 14.04 1.34 5 -7 28 18.10 1.36 -4 7 -28 11.96 0.89 7 4 -28 10.32 0.85 -4 7 -28 13.38 1.08 -7 -4 -28 10.24 1.05 7 4 -28 9.92 0.97 -4 7 28 10.65 1.04 4 -7 28 11.39 1.03 -4 7 28 9.30 0.83 -7 -4 28 13.43 0.98 7 4 28 11.93 1.13 -3 7 -28 9.64 0.92 3 -7 -28 9.08 0.97 -7 -3 -28 8.08 0.93 7 3 -28 8.03 0.85 -3 7 -28 9.06 0.76 7 3 -28 7.63 0.72 -7 -3 28 9.10 0.81 -3 7 28 8.52 0.94 3 -7 28 7.68 0.88 7 3 28 8.34 0.97 7 2 -28 32.58 1.97 -7 -2 -28 27.12 2.14 -2 7 -28 28.52 1.96 -2 7 -28 27.84 2.06 7 2 -28 29.53 2.33 2 -7 -28 29.30 2.11 2 -7 28 33.35 2.09 -7 -2 28 29.65 2.01 -2 7 28 34.00 2.14 7 2 28 28.42 2.52 1 -7 -28 22.26 1.67 -7 -1 -28 19.66 1.98 7 1 -28 19.48 1.53 7 1 -28 21.67 1.48 -1 7 -28 21.60 1.56 -1 7 -28 22.05 1.48 -1 7 28 21.35 1.63 1 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17.56 1.26 5 7 -28 16.10 1.34 7 -5 -28 17.66 1.29 -7 5 -28 18.70 1.44 -7 5 28 16.96 1.26 7 -5 28 18.41 1.42 -5 -7 28 18.00 1.32 5 7 28 16.50 1.47 -7 5 28 18.16 1.36 -6 -7 -28 27.71 1.96 7 -6 -28 27.91 1.88 6 7 -28 27.76 1.92 -7 6 -28 28.39 2.00 6 7 -28 26.55 1.81 -7 6 28 29.01 1.93 7 -6 28 28.57 1.97 6 7 28 26.99 2.04 -7 6 28 26.41 1.84 7 -7 -28 9.35 0.89 7 7 -28 9.05 0.99 -7 7 -28 9.13 1.03 -7 -7 -28 10.61 1.01 7 7 -28 9.57 0.92 7 7 28 10.24 1.09 -7 7 28 10.55 0.97 -7 -7 28 9.66 0.96 -7 7 28 8.26 0.83 7 -7 28 11.22 1.00 7 -8 -28 6.55 0.76 -8 -7 -28 7.61 0.90 -7 8 -28 6.10 0.90 8 7 -28 5.98 0.77 8 7 28 4.44 0.76 -7 8 28 8.13 0.86 -7 8 28 6.17 0.69 7 -8 28 8.48 1.12 -8 -7 28 5.64 0.80 6 -8 -28 14.75 1.13 -6 8 -28 12.98 1.24 -8 -6 -28 14.78 1.25 8 6 -28 13.78 1.14 -8 -6 28 15.27 1.18 -6 8 28 13.90 1.19 -6 8 28 13.31 1.06 8 6 28 13.09 1.28 6 -8 28 14.53 1.19 8 5 -28 14.59 1.09 -8 -5 -28 15.49 1.32 5 -8 -28 16.28 1.22 8 5 -28 15.20 1.23 -5 8 -28 17.12 1.20 -5 8 28 17.10 1.31 5 -8 28 15.92 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0.08 1 8 27 0.42 -0.41 0 8 27 0.02 0.25 8 9 27 0.25 -0.48 7 9 27 0.23 -0.40 6 9 27 0.51 -0.50 5 9 27 0.40 -0.49 4 9 27 0.65 -0.43 3 9 27 0.35 -0.36 2 9 27 0.64 -0.44 1 9 27 0.09 -0.30 0 9 27 0.62 0.00 8 10 27 0.21 -0.36 7 10 27 0.20 -0.41 6 10 27 0.30 -0.62 5 10 27 0.35 -0.31 4 10 27 0.35 -0.61 3 10 27 0.54 -0.25 2 10 27 0.16 -0.67 1 10 27 0.75 -0.16 0 10 27 0.02 -0.75 7 11 27 0.20 -0.55 6 11 27 0.02 -0.27 5 11 27 0.23 -0.66 4 11 27 0.13 -0.14 3 11 27 0.20 -0.75 2 11 27 0.54 -0.10 1 11 27 0.04 -0.93 0 11 27 0.80 0.00 5 12 27 -0.17 -0.14 4 12 27 0.14 -0.60 3 12 27 0.09 -0.07 2 12 27 0.07 -0.76 1 12 27 0.58 -0.03 0 12 27 -0.01 -0.86 2 13 27 0.21 -0.07 1 13 27 0.01 -0.53 0 13 27 0.47 0.02 0 0 28 0.52 -0.02 1 1 28 0.18 0.05 0 1 28 -0.01 0.08 2 2 28 -0.43 0.08 1 2 28 -0.04 0.18 0 2 28 -0.01 -0.02 3 3 28 -0.62 -0.09 2 3 28 -0.06 0.19 1 3 28 -0.35 0.00 0 3 28 -0.04 0.47 4 4 28 -0.18 -0.21 3 4 28 0.00 0.13 2 4 28 -0.43 -0.20 1 4 28 -0.08 0.55 0 4 28 -0.20 0.00 5 5 28 0.55 -0.05 4 5 28 0.08 0.04 3 5 28 -0.05 -0.35 2 5 28 0.02 0.42 1 5 28 -0.10 -0.27 0 5 28 -0.04 0.74 6 6 28 1.12 0.09 5 6 28 0.11 -0.05 4 6 28 0.63 -0.19 3 6 28 0.21 0.15 2 6 28 0.15 -0.53 1 6 28 0.05 0.61 0 6 28 0.04 0.01 7 7 28 1.18 -0.04 6 7 28 0.07 -0.12 5 7 28 1.20 0.00 4 7 28 0.29 -0.15 3 7 28 0.71 -0.42 2 7 28 0.26 0.18 1 7 28 0.20 -0.37 0 7 28 -0.01 0.42 8 8 28 0.74 -0.22 7 8 28 0.05 -0.14 6 8 28 1.26 -0.07 5 8 28 0.21 -0.36 4 8 28 1.23 -0.16 3 8 28 0.40 -0.30 2 8 28 0.62 -0.45 1 8 28 0.20 -0.10 0 8 28 0.27 0.01 8 9 28 0.06 -0.12 7 9 28 0.80 -0.23 6 9 28 0.14 -0.41 5 9 28 1.23 -0.12 4 9 28 0.37 -0.59 3 9 28 0.99 -0.25 2 9 28 0.39 -0.62 1 9 28 0.51 -0.24 0 9 28 0.01 -0.62 7 10 28 0.11 -0.33 6 10 28 0.72 -0.22 5 10 28 0.25 -0.62 4 10 28 0.84 -0.11 3 10 28 0.44 -0.82 2 10 28 0.64 -0.21 1 10 28 0.24 -0.95 0 10 28 0.51 0.00 5 11 28 0.34 -0.11 4 11 28 0.34 -0.72 3 11 28 0.37 -0.08 2 11 28 0.37 -0.91 1 11 28 0.46 -0.09 0 11 28 0.01 -1.00 3 12 28 0.34 -0.65 2 12 28 0.21 -0.06 1 12 28 0.18 -0.74 0 12 28 0.38 -0.01 0 1 29 -2.08 0.09 1 2 29 -1.73 0.16 0 2 29 0.01 0.34 2 3 29 -1.04 0.16 1 3 29 0.00 0.33 0 3 29 -1.28 0.04 3 4 29 -0.14 0.05 2 4 29 0.07 0.08 1 4 29 -0.58 -0.01 0 4 29 -0.01 0.33 4 5 29 0.72 -0.06 3 5 29 0.23 -0.10 2 5 29 0.12 -0.18 1 5 29 0.11 0.08 0 5 29 -0.08 -0.02 5 6 29 1.26 -0.11 4 6 29 0.33 -0.14 3 6 29 0.76 -0.27 2 6 29 0.37 -0.15 1 6 29 0.27 -0.26 0 6 29 -0.01 -0.03 6 7 29 1.29 -0.11 5 7 29 0.29 -0.16 4 7 29 1.21 -0.21 3 7 29 0.54 -0.29 2 7 29 0.59 -0.41 1 7 29 0.29 -0.25 0 7 29 0.24 -0.01 7 8 29 0.89 -0.11 6 8 29 0.20 -0.19 5 8 29 1.26 -0.13 4 8 29 0.50 -0.38 3 8 29 0.91 -0.33 2 8 29 0.54 -0.49 1 8 29 0.29 -0.28 0 8 29 0.02 -0.50 7 9 29 0.15 -0.19 6 9 29 0.89 -0.14 5 9 29 0.34 -0.39 4 9 29 0.94 -0.19 3 9 29 0.54 -0.60 2 9 29 0.46 -0.34 1 9 29 0.32 -0.73 0 9 29 0.17 0.02 5 10 29 0.62 -0.14 4 10 29 0.37 -0.50 3 10 29 0.46 -0.22 2 10 29 0.41 -0.71 1 10 29 0.25 -0.18 0 10 29 0.02 -0.81 3 11 29 0.30 -0.46 2 11 29 0.25 -0.18 1 11 29 0.18 -0.61 0 11 29 0.32 0.02 0 0 30 -1.47 0.05 1 1 30 -1.35 -0.12 0 1 30 -0.01 0.13 2 2 30 -1.05 -0.34 1 2 30 0.00 0.23 0 2 30 -1.24 0.02 3 3 30 -0.62 -0.28 2 3 30 0.03 0.07 1 3 30 -0.96 -0.24 0 3 30 -0.01 0.40 4 4 30 0.01 -0.04 3 4 30 0.07 -0.10 2 4 30 -0.54 -0.25 1 4 30 0.07 0.06 0 4 30 -0.71 -0.03 5 5 30 0.70 0.08 4 5 30 0.08 -0.12 3 5 30 0.07 -0.07 2 5 30 0.18 -0.29 1 5 30 -0.36 -0.17 0 5 30 0.00 -0.21 6 6 30 1.08 0.06 5 6 30 0.05 -0.05 4 6 30 0.73 0.06 3 6 30 0.24 -0.34 2 6 30 0.13 -0.12 1 6 30 0.20 -0.48 0 6 30 -0.19 -0.02 7 7 30 0.93 0.03 6 7 30 0.02 -0.02 5 7 30 1.10 0.07 4 7 30 0.19 -0.23 3 7 30 0.67 0.00 2 7 30 0.36 -0.55 1 7 30 0.03 -0.09 0 7 30 0.02 -0.63 7 8 30 0.01 -0.01 6 8 30 0.95 0.04 5 8 30 0.10 -0.15 4 8 30 0.97 0.06 3 8 30 0.37 -0.50 2 8 30 0.34 -0.08 1 8 30 0.29 -0.73 0 8 30 -0.09 0.03 5 9 30 0.84 0.05 4 9 30 0.25 -0.38 3 9 30 0.55 -0.03 2 9 30 0.43 -0.70 1 9 30 -0.01 -0.08 0 9 30 0.01 -0.81 3 10 30 0.38 -0.49 2 10 30 0.14 -0.11 1 10 30 0.27 -0.69 0 10 30 -0.07 0.03 0 1 31 -2.67 0.08 1 2 31 -1.80 -0.17 0 2 31 0.01 0.13 2 3 31 -0.75 -0.21 1 3 31 0.11 -0.05 0 3 31 -1.28 0.01 3 4 31 -0.05 0.05 2 4 31 0.23 -0.35 1 4 31 -0.59 -0.08 0 4 31 0.00 -0.41 4 5 31 0.33 0.17 3 5 31 0.28 -0.41 2 5 31 -0.03 0.07 1 5 31 0.25 -0.79 0 5 31 -0.32 -0.03 5 6 31 0.50 0.02 4 6 31 0.26 -0.23 3 6 31 0.31 0.15 2 6 31 0.44 -0.79 1 6 31 -0.04 0.03 0 6 31 -0.01 -1.07 6 7 31 0.44 -0.09 5 7 31 0.23 -0.06 4 7 31 0.42 0.04 3 7 31 0.48 -0.51 2 7 31 0.13 0.06 1 7 31 0.32 -0.98 0 7 31 -0.10 -0.02 5 8 31 0.33 -0.04 4 8 31 0.39 -0.24 3 8 31 0.16 -0.02 2 8 31 0.49 -0.69 1 8 31 -0.17 -0.03 0 8 31 -0.02 -0.88 3 9 31 0.41 -0.41 2 9 31 -0.18 -0.12 1 9 31 0.26 -0.64 0 9 31 -0.36 0.01 0 0 32 -1.22 0.05 1 1 32 -0.92 -0.14 0 1 32 0.01 -0.02 2 2 32 -0.39 -0.31 1 2 32 0.06 -0.09 0 2 32 -0.76 0.02 3 3 32 -0.08 -0.09 2 3 32 0.12 -0.20 1 3 32 -0.46 -0.16 0 3 32 0.04 -0.34 4 4 32 0.05 0.22 3 4 32 0.13 -0.25 2 4 32 -0.22 0.02 1 4 32 0.20 -0.66 0 4 32 -0.53 0.00 5 5 32 0.22 0.21 4 5 32 0.06 -0.18 3 5 32 -0.02 0.29 2 5 32 0.27 -0.76 1 5 32 -0.43 0.13 0 5 32 0.04 -1.08 5 6 32 0.01 -0.08 4 6 32 0.19 0.25 3 6 32 0.18 -0.56 2 6 32 -0.15 0.33 1 6 32 0.22 -1.15 0 6 32 -0.43 0.00 4 7 32 0.07 -0.27 3 7 32 0.09 0.26 2 7 32 0.25 -0.81 1 7 32 -0.22 0.18 0 7 32 0.01 -1.12 2 8 32 -0.07 0.13 1 8 32 0.17 -0.71 0 8 32 -0.23 0.00 0 1 33 -1.28 -0.05 1 2 33 -0.65 -0.22 0 2 33 0.01 -0.43 2 3 33 0.00 -0.23 1 3 33 0.11 -0.67 0 3 33 -0.38 -0.01 3 4 33 0.24 -0.01 2 4 33 0.20 -0.66 1 4 33 -0.09 -0.02 0 4 33 0.02 -1.15 4 5 33 0.18 0.09 3 5 33 0.17 -0.47 2 5 33 0.07 0.18 1 5 33 0.20 -1.23 0 5 33 -0.11 0.00 2 6 33 0.23 -0.90 1 6 33 -0.05 0.19 0 6 33 0.02 -1.39 0 0 34 0.65 -0.03 1 1 34 0.63 -0.06 0 1 34 0.00 -0.09 2 2 34 0.52 -0.02 1 2 34 0.02 -0.19 0 2 34 0.57 -0.03 2 3 34 0.06 -0.16 1 3 34 0.37 0.02 0 3 34 0.01 -0.44 1 4 34 0.09 -0.43 0 4 34 0.08 0.02 1 1 0 84.18 -0.19 15 15 0 -0.48 0.04 11 18 0 -0.56 -0.01 7 20 0 0.01 0.01 2 21 0 -0.05 0.00 3 21 0 0.14 0.08 0 1 1 73.24 -0.07 11 18 1 -0.50 -0.27 7 20 1 -0.15 -0.09 2 21 1 -0.05 0.07 3 21 1 -0.11 0.04 0 0 2 59.12 -0.04 0 1 2 -0.02 1.85 11 18 2 -0.34 0.10 9 19 2 -0.37 -0.38 2 21 2 0.01 0.25 11 18 3 -0.37 -0.42 9 19 3 -0.26 0.17 0 21 3 0.13 0.04 1 21 3 0.04 0.30 2 21 3 0.11 0.17 9 19 4 -0.27 -0.40 0 21 4 0.00 0.02 1 21 4 0.09 0.00 6 20 5 -0.32 0.25 0 21 5 0.16 -0.08 12 17 6 -0.15 -0.17 6 20 6 0.31 0.06 14 15 8 -0.13 -0.10 13 16 8 -0.29 -0.24 10 18 8 -0.22 0.04 8 19 8 -0.34 -0.16 5 20 8 -0.27 0.28 4 20 9 -0.08 0.05 11 17 10 -0.25 0.16 7 19 10 -0.64 0.32 3 20 10 -0.11 0.14 12 16 11 -0.12 -0.11 9 18 11 -0.32 -0.04 0 20 11 0.00 0.52 1 20 11 -0.32 -0.04 2 20 11 0.03 0.32 14 14 12 0.08 -0.14 13 15 12 -0.05 -0.08 6 19 12 -0.22 -0.02 8 18 13 -0.30 -0.09 5 19 13 -0.31 -0.13 11 16 14 0.19 0.13 7 18 14 -0.22 -0.12 4 19 14 -0.24 0.26 13 14 15 0.21 -0.18 0 19 15 -0.47 0.00 1 19 15 -0.06 0.27 2 19 15 -0.41 0.06 10 16 16 0.27 -0.23 8 17 16 -0.13 -0.14 12 14 17 0.20 -0.11 9 16 17 0.22 -0.25 7 17 17 -0.18 0.00 4 18 17 -0.22 0.20 10 15 18 -0.09 -0.13 6 17 18 -0.07 0.15 1 18 18 0.07 0.30 2 18 18 0.06 -0.05 12 13 19 0.43 -0.33 11 14 19 0.42 -0.25 5 17 19 -0.04 0.15 3 17 20 0.04 0.15 10 13 22 -0.25 0.19 4 16 22 -0.11 0.26 9 13 23 0.00 0.24 5 15 23 -0.06 0.11 0 16 23 0.00 -0.04 8 13 24 0.09 0.09 6 14 24 0.11 0.07 3 15 24 -0.19 0.00 10 11 25 0.44 -0.05 7 13 25 -0.07 -0.09 5 14 25 -0.16 -0.11 10 10 26 0.19 0.03 9 11 26 0.12 0.00 0 14 26 0.12 0.01 1 14 26 0.02 -0.26 2 14 26 0.04 -0.10 9 10 27 0.07 -0.16 6 12 27 0.08 -0.50 3 13 27 0.08 -0.43 9 9 28 0.16 -0.14 6 11 28 0.10 -0.45 4 12 28 -0.02 -0.03 6 10 29 0.20 -0.29 4 11 29 0.20 -0.11 6 9 30 0.05 -0.07 4 10 30 0.49 0.00 4 9 31 0.10 -0.06 6 6 32 0.35 0.02 5 7 32 0.29 0.05 3 8 32 0.16 -0.39 3 6 33 0.05 0.22 0 7 33 -0.05 -0.01 1 7 33 0.14 -1.00 3 3 34 0.27 0.09 2 4 34 0.12 0.16 3 4 34 0.06 -0.08 0 5 34 0.00 -0.56 1 5 34 -0.15 0.21 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 21116) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.000 0.000 211 45 ' ' 2 0.000 0.000 0.317 27 0 ' ' 3 0.000 0.000 0.500 70 1 ' ' 4 0.000 0.000 0.683 28 0 ' ' 5 0.500 0.500 0.500 211 45 ' ' 6 0.500 0.500 1.000 70 1 ' ' 7 0.500 0.500 0.816 27 0 ' ' 8 0.500 0.500 0.183 28 0 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 1 1 0 1.759 0 1 1 1.454 0 0 2 1.506 0 1 2 1.953 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL shelx P -4 21 c R = 0.03 CELL 16.3758 16.3758 27.0498 90.00 90.00 90.00 SPGR P-421c # Solvent Accessible Volume = 678 # Electrons Found in S.A.V. = 90 # Note: Atoms in Void as Cxxx and Qxxx all others C101 0.500 0.493 0.430 ! 3.40 eA-3 C102 0.461 0.502 0.479 ! 3.02 eA-3 C103 1.004 0.924 0.914 ! 2.34 eA-3 C104 0.031 0.905 0.988 ! 0.66 eA-3 ) ; _shelx_fab_checksum 96318 loop_ _space_group_symop_operation_xyz 'x, y, z' 'y, -x, -z' '-y, x, -z' 'x+1/2, -y+1/2, -z+1/2' '-x+1/2, y+1/2, -z+1/2' '-x, -y, z' '-y+1/2, -x+1/2, z+1/2' 'y+1/2, x+1/2, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ge1A Ge 0.5746(2) 0.9010(2) 1.35045(12) 0.0134(3) Uani 0.452(2) 1 d . . P A 1 Si1B Si 0.5716(5) 0.9083(5) 1.3465(3) 0.0134(3) Uani 0.548(2) 1 d . . P A 2 Ge2 Ge 0.55935(2) 1.06067(2) 1.31756(2) 0.01661(6) Uani 1 1 d . . . . . Si3 Si 0.57149(3) 1.01539(3) 1.40487(2) 0.01252(10) Uani 1 1 d . . . . . Si4 Si 0.73053(3) 0.79742(3) 1.32587(2) 0.02098(12) Uani 1 1 d . . . . . Si5 Si 0.68818(3) 1.00339(3) 1.49562(2) 0.01734(11) Uani 1 1 d . . . . . N1 N 0.63776(10) 0.84411(10) 1.30935(6) 0.0183(3) Uani 1 1 d . . . . . N2 N 0.64325(9) 1.05579(9) 1.44549(5) 0.0153(3) Uani 1 1 d . . . . . C1 C 0.59881(12) 0.82308(12) 1.26292(7) 0.0177(4) Uani 1 1 d . . . . . C2 C 0.54702(12) 0.75436(12) 1.26053(7) 0.0213(4) Uani 1 1 d . . . . . C3 C 0.50917(14) 0.73626(14) 1.21569(8) 0.0298(5) Uani 1 1 d . . . . . H3 H 0.4742 0.6901 1.2136 0.036 Uiso 1 1 calc R U . . . C4 C 0.52140(15) 0.78376(16) 1.17453(8) 0.0350(6) Uani 1 1 d . . . . . H4 H 0.4947 0.7706 1.1444 0.042 Uiso 1 1 calc R U . . . C5 C 0.57249(14) 0.85069(14) 1.17702(8) 0.0287(5) Uani 1 1 d . . . . . H5 H 0.5813 0.8826 1.1482 0.034 Uiso 1 1 calc R U . . . C6 C 0.61148(13) 0.87257(13) 1.22086(8) 0.0210(4) Uani 1 1 d . . . . . C7 C 0.53070(13) 0.69898(13) 1.30455(8) 0.0280(5) Uani 1 1 d . . . . . H7 H 0.5639 0.7197 1.3329 0.034 Uiso 1 1 calc R U . . . C8 C 0.5569(2) 0.61124(15) 1.29447(12) 0.0526(8) Uani 1 1 d . . . . . H8A H 0.5454 0.5775 1.3236 0.079 Uiso 1 1 calc R U . . . H8B H 0.5265 0.5899 1.2660 0.079 Uiso 1 1 calc R U . . . H8C H 0.6155 0.6098 1.2873 0.079 Uiso 1 1 calc R U . . . C9 C 0.44083(15) 0.70137(16) 1.32002(10) 0.0411(6) Uani 1 1 d . . . . . H9A H 0.4324 0.6651 1.3484 0.062 Uiso 1 1 calc R U . . . H9B H 0.4259 0.7573 1.3292 0.062 Uiso 1 1 calc R U . . . H9C H 0.4066 0.6832 1.2924 0.062 Uiso 1 1 calc R U . . . C10 C 0.66650(14) 0.94692(13) 1.22093(8) 0.0259(4) Uani 1 1 d . . . . . H10 H 0.6746 0.9639 1.2561 0.031 Uiso 1 1 calc R U . . . C11 C 0.75038(16) 0.92782(17) 1.19930(11) 0.0420(6) Uani 1 1 d . . . . . H11A H 0.7842 0.9772 1.1999 0.063 Uiso 1 1 calc R U . . . H11B H 0.7766 0.8849 1.2190 0.063 Uiso 1 1 calc R U . . . H11C H 0.7442 0.9091 1.1651 0.063 Uiso 1 1 calc R U . . . C12 C 0.6291(2) 1.01927(15) 1.19326(9) 0.0419(6) Uani 1 1 d . . . . . H12A H 0.6668 1.0657 1.1943 0.063 Uiso 1 1 calc R U . . . H12B H 0.6191 1.0039 1.1588 0.063 Uiso 1 1 calc R U . . . H12C H 0.5773 1.0346 1.2089 0.063 Uiso 1 1 calc R U . . . C13 C 0.71789(16) 0.73369(15) 1.38250(9) 0.0343(5) Uani 1 1 d . . . . . H13A H 0.7702 0.7083 1.3910 0.051 Uiso 1 1 calc R U . . . H13B H 0.6996 0.7682 1.4099 0.051 Uiso 1 1 calc R U . . . H13C H 0.6772 0.6911 1.3763 0.051 Uiso 1 1 calc R U . . . C14 C 0.76516(14) 0.73035(15) 1.27430(10) 0.0326(5) Uani 1 1 d . . . . . H14A H 0.8169 0.7042 1.2834 0.049 Uiso 1 1 calc R U . . . H14B H 0.7238 0.6883 1.2680 0.049 Uiso 1 1 calc R U . . . H14C H 0.7730 0.7633 1.2444 0.049 Uiso 1 1 calc R U . . . C15 C 0.80923(13) 0.87680(14) 1.33816(9) 0.0291(5) Uani 1 1 d . . . . . H15A H 0.8607 0.8504 1.3473 0.044 Uiso 1 1 calc R U . . . H15B H 0.8175 0.9098 1.3083 0.044 Uiso 1 1 calc R U . . . H15C H 0.7909 0.9120 1.3653 0.044 Uiso 1 1 calc R U . . . C16 C 0.66864(12) 1.14009(11) 1.43757(7) 0.0167(4) Uani 1 1 d . . . . . C17 C 0.62346(13) 1.20341(12) 1.45979(7) 0.0213(4) Uani 1 1 d . . . . . C18 C 0.65251(15) 1.28319(13) 1.45529(9) 0.0293(5) Uani 1 1 d . . . . . H18 H 0.6235 1.3263 1.4708 0.035 Uiso 1 1 calc R U . . . C19 C 0.72207(15) 1.30106(13) 1.42893(9) 0.0315(5) Uani 1 1 d . . . . . H19 H 0.7410 1.3558 1.4267 0.038 Uiso 1 1 calc R U . . . C20 C 0.76417(14) 1.23878(14) 1.40573(9) 0.0268(5) Uani 1 1 d . . . . . H20 H 0.8112 1.2515 1.3867 0.032 Uiso 1 1 calc R U . . . C21 C 0.73906(12) 1.15764(12) 1.40973(7) 0.0206(4) Uani 1 1 d . . . . . C22 C 0.54477(13) 1.18827(13) 1.48770(8) 0.0247(4) Uani 1 1 d . . . . . H22 H 0.5322 1.1287 1.4848 0.030 Uiso 1 1 calc R U . . . C23 C 0.47354(14) 1.23466(15) 1.46484(9) 0.0336(5) Uani 1 1 d . . . . . H23A H 0.4237 1.2235 1.4837 0.050 Uiso 1 1 calc R U . . . H23B H 0.4851 1.2934 1.4655 0.050 Uiso 1 1 calc R U . . . H23C H 0.4660 1.2169 1.4305 0.050 Uiso 1 1 calc R U . . . C24 C 0.55242(15) 1.20779(17) 1.54271(8) 0.0365(5) Uani 1 1 d . . . . . H24A H 0.5002 1.1971 1.5592 0.055 Uiso 1 1 calc R U . . . H24B H 0.5949 1.1734 1.5574 0.055 Uiso 1 1 calc R U . . . H24C H 0.5670 1.2654 1.5469 0.055 Uiso 1 1 calc R U . . . C25 C 0.78875(13) 1.09216(13) 1.38364(8) 0.0243(4) Uani 1 1 d . . . . . H25 H 0.7607 1.0386 1.3889 0.029 Uiso 1 1 calc R U . . . C26 C 0.87513(15) 1.08484(16) 1.40419(9) 0.0366(6) Uani 1 1 d . . . . . H26A H 0.9046 1.0420 1.3863 0.055 Uiso 1 1 calc R U . . . H26B H 0.9037 1.1370 1.4001 0.055 Uiso 1 1 calc R U . . . H26C H 0.8726 1.0708 1.4394 0.055 Uiso 1 1 calc R U . . . C27 C 0.79272(15) 1.10782(15) 1.32797(8) 0.0299(5) Uani 1 1 d . . . . . H27A H 0.8250 1.0648 1.3121 0.045 Uiso 1 1 calc R U . . . H27B H 0.7373 1.1077 1.3143 0.045 Uiso 1 1 calc R U . . . H27C H 0.8183 1.1610 1.3219 0.045 Uiso 1 1 calc R U . . . C28 C 0.75700(13) 1.07372(14) 1.53027(8) 0.0268(5) Uani 1 1 d . . . . . H28A H 0.7818 1.0444 1.5581 0.040 Uiso 1 1 calc R U . . . H28B H 0.8000 1.0936 1.5082 0.040 Uiso 1 1 calc R U . . . H28C H 0.7254 1.1201 1.5428 0.040 Uiso 1 1 calc R U . . . C29 C 0.74760(16) 0.91384(14) 1.47375(8) 0.0333(5) Uani 1 1 d . . . . . H29A H 0.7719 0.8858 1.5022 0.050 Uiso 1 1 calc R U . . . H29B H 0.7113 0.8762 1.4561 0.050 Uiso 1 1 calc R U . . . H29C H 0.7910 0.9322 1.4514 0.050 Uiso 1 1 calc R U . . . C30 C 0.60817(14) 0.96540(16) 1.53851(8) 0.0320(5) Uani 1 1 d . . . . . H30A H 0.6340 0.9365 1.5661 0.048 Uiso 1 1 calc R U . . . H30B H 0.5766 1.0117 1.5513 0.048 Uiso 1 1 calc R U . . . H30C H 0.5717 0.9280 1.5208 0.048 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ge1A 0.0125(3) 0.0170(6) 0.0106(6) -0.0022(4) -0.0024(3) 0.0038(3) Si1B 0.0125(3) 0.0170(6) 0.0106(6) -0.0022(4) -0.0024(3) 0.0038(3) Ge2 0.01428(9) 0.02253(10) 0.01301(9) 0.00484(8) 0.00265(7) 0.00403(8) Si3 0.0150(2) 0.0128(2) 0.0097(2) -0.00027(17) -0.00105(18) 0.0001(2) Si4 0.0179(3) 0.0213(3) 0.0237(3) -0.0029(2) -0.0053(2) 0.0034(2) Si5 0.0212(3) 0.0184(2) 0.0125(2) 0.0009(2) -0.00312(19) -0.0019(2) N1 0.0194(8) 0.0195(8) 0.0158(8) -0.0002(6) -0.0033(6) 0.0001(7) N2 0.0186(7) 0.0146(7) 0.0126(7) -0.0001(6) -0.0022(6) -0.0018(6) C1 0.0160(8) 0.0212(9) 0.0158(9) -0.0035(7) -0.0019(7) 0.0054(7) C2 0.0161(9) 0.0235(10) 0.0244(10) -0.0055(8) -0.0012(8) 0.0030(8) C3 0.0234(11) 0.0328(12) 0.0333(11) -0.0151(9) -0.0050(9) -0.0006(9) C4 0.0361(13) 0.0472(14) 0.0217(10) -0.0162(10) -0.0090(9) 0.0090(11) C5 0.0353(12) 0.0363(12) 0.0146(9) -0.0032(8) -0.0002(9) 0.0109(10) C6 0.0226(10) 0.0227(10) 0.0176(10) -0.0032(8) 0.0012(8) 0.0077(8) C7 0.0236(10) 0.0238(10) 0.0365(12) 0.0002(9) -0.0006(9) -0.0037(9) C8 0.0582(18) 0.0262(12) 0.073(2) 0.0076(13) 0.0166(16) 0.0019(13) C9 0.0294(12) 0.0389(13) 0.0548(16) 0.0034(12) 0.0093(12) -0.0068(11) C10 0.0351(11) 0.0229(10) 0.0197(10) -0.0006(8) 0.0086(8) 0.0020(9) C11 0.0398(14) 0.0367(13) 0.0495(15) -0.0075(12) 0.0225(12) -0.0046(12) C12 0.0756(19) 0.0287(12) 0.0214(11) 0.0048(9) 0.0050(12) 0.0071(13) C13 0.0347(13) 0.0305(12) 0.0377(13) 0.0085(10) -0.0145(11) 0.0019(10) C14 0.0265(11) 0.0311(12) 0.0403(14) -0.0131(10) -0.0036(10) 0.0052(10) C15 0.0206(10) 0.0316(12) 0.0351(12) -0.0100(9) -0.0025(9) 0.0005(9) C16 0.0214(9) 0.0147(8) 0.0140(9) 0.0012(7) -0.0052(7) -0.0024(7) C17 0.0249(10) 0.0190(9) 0.0199(10) -0.0034(8) -0.0046(8) -0.0011(8) C18 0.0382(12) 0.0176(10) 0.0322(12) -0.0054(8) -0.0047(10) -0.0006(9) C19 0.0415(13) 0.0186(10) 0.0343(12) 0.0020(9) -0.0069(10) -0.0111(10) C20 0.0285(11) 0.0247(11) 0.0270(11) 0.0044(9) -0.0016(9) -0.0096(9) C21 0.0237(10) 0.0202(9) 0.0179(9) 0.0016(8) -0.0028(8) -0.0034(8) C22 0.0229(10) 0.0224(10) 0.0288(11) -0.0076(8) -0.0004(8) 0.0013(8) C23 0.0302(12) 0.0382(13) 0.0325(12) -0.0077(10) -0.0035(9) 0.0080(10) C24 0.0295(12) 0.0530(15) 0.0269(11) -0.0083(11) -0.0009(10) 0.0017(11) C25 0.0255(10) 0.0231(10) 0.0244(10) 0.0042(8) 0.0069(8) -0.0024(9) C26 0.0309(12) 0.0471(15) 0.0319(13) 0.0052(11) 0.0026(10) 0.0068(11) C27 0.0319(12) 0.0344(12) 0.0234(11) 0.0015(9) 0.0076(9) -0.0063(10) C28 0.0278(10) 0.0306(11) 0.0219(10) 0.0000(9) -0.0092(8) -0.0051(9) C29 0.0476(14) 0.0283(12) 0.0240(11) 0.0016(9) -0.0076(10) 0.0117(10) C30 0.0295(11) 0.0455(14) 0.0208(10) 0.0117(9) -0.0050(9) -0.0097(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Ge1A Si3 144.0(2) . . ? N1 Ge1A Ge2 115.30(17) . 6_675 ? Si3 Ge1A Ge2 90.21(11) . 6_675 ? N1 Ge1A Ge2 110.19(16) . . ? Si3 Ge1A Ge2 56.97(8) . . ? Ge2 Ge1A Ge2 63.97(7) 6_675 . ? N1 Si1B Ge2 119.3(4) . 6_675 ? N1 Si1B Si3 143.3(4) . . ? Ge2 Si1B Si3 93.5(3) 6_675 . ? N1 Si1B Ge2 115.6(4) . . ? Ge2 Si1B Ge2 67.90(19) 6_675 . ? Si3 Si1B Ge2 59.51(19) . . ? Si1B Ge2 Si3 79.7(2) 6_675 . ? Ge1A Ge2 Si3 78.63(8) 6_675 . ? Si1B Ge2 Si1B 100.2(3) 6_675 . ? Si3 Ge2 Si1B 55.00(17) . . ? Ge1A Ge2 Ge1A 101.88(12) 6_675 . ? Si3 Ge2 Ge1A 53.57(7) . . ? Si1B Ge2 Ge2 60.9(2) 6_675 6_675 ? Ge1A Ge2 Ge2 63.70(9) 6_675 6_675 ? Si3 Ge2 Ge2 80.937(13) . 6_675 ? Si1B Ge2 Ge2 51.18(18) . 6_675 ? Ge1A Ge2 Ge2 52.33(8) . 6_675 ? N2 Si3 Si1B 134.8(2) . . ? N2 Si3 Ge1A 132.43(10) . . ? N2 Si3 Si3 137.77(5) . 6_675 ? Si1B Si3 Si3 81.0(2) . 6_675 ? Ge1A Si3 Si3 81.69(9) . 6_675 ? N2 Si3 Ge2 122.77(6) . . ? Si1B Si3 Ge2 65.50(18) . . ? Ge1A Si3 Ge2 69.45(8) . . ? Si3 Si3 Ge2 89.121(15) 6_675 . ? N1 Si4 C15 109.88(9) . . ? N1 Si4 C14 109.19(10) . . ? C15 Si4 C14 109.55(11) . . ? N1 Si4 C13 110.87(10) . . ? C15 Si4 C13 108.73(11) . . ? C14 Si4 C13 108.59(12) . . ? N2 Si5 C29 110.96(9) . . ? N2 Si5 C30 110.41(9) . . ? C29 Si5 C30 107.71(12) . . ? N2 Si5 C28 109.75(9) . . ? C29 Si5 C28 109.34(11) . . ? C30 Si5 C28 108.62(11) . . ? C1 N1 Si4 119.79(13) . . ? C1 N1 Ge1A 114.16(17) . . ? Si4 N1 Ge1A 124.77(14) . . ? C1 N1 Si1B 110.7(3) . . ? Si4 N1 Si1B 128.9(3) . . ? C16 N2 Si3 117.40(12) . . ? C16 N2 Si5 117.02(12) . . ? Si3 N2 Si5 125.58(9) . . ? C2 C1 C6 120.61(18) . . ? C2 C1 N1 119.58(17) . . ? C6 C1 N1 119.80(17) . . ? C3 C2 C1 118.5(2) . . ? C3 C2 C7 118.45(19) . . ? C1 C2 C7 123.07(18) . . ? C4 C3 C2 121.4(2) . . ? C4 C3 H3 119.3 . . ? C2 C3 H3 119.3 . . ? C3 C4 C5 119.9(2) . . ? C3 C4 H4 120.0 . . ? C5 C4 H4 120.0 . . ? C4 C5 C6 121.5(2) . . ? C4 C5 H5 119.2 . . ? C6 C5 H5 119.2 . . ? C5 C6 C1 118.09(19) . . ? C5 C6 C10 118.70(19) . . ? C1 C6 C10 123.21(18) . . ? C2 C7 C8 111.9(2) . . ? C2 C7 C9 111.58(19) . . ? C8 C7 C9 110.1(2) . . ? C2 C7 H7 107.7 . . ? C8 C7 H7 107.7 . . ? C9 C7 H7 107.7 . . ? C7 C8 H8A 109.5 . . ? C7 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C7 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C7 C9 H9A 109.5 . . ? C7 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C7 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C6 C10 C11 111.74(19) . . ? C6 C10 C12 112.6(2) . . ? C11 C10 C12 109.4(2) . . ? C6 C10 H10 107.6 . . ? C11 C10 H10 107.6 . . ? C12 C10 H10 107.6 . . ? C10 C11 H11A 109.5 . . ? C10 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C10 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C10 C12 H12A 109.5 . . ? C10 C12 H12B 109.5 . . ? H12A C12 H12B 109.5 . . ? C10 C12 H12C 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? Si4 C13 H13A 109.5 . . ? Si4 C13 H13B 109.5 . . ? H13A C13 H13B 109.5 . . ? Si4 C13 H13C 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? Si4 C14 H14A 109.5 . . ? Si4 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? Si4 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? Si4 C15 H15A 109.5 . . ? Si4 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? Si4 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C21 C16 C17 120.57(18) . . ? C21 C16 N2 120.39(17) . . ? C17 C16 N2 119.00(17) . . ? C18 C17 C16 118.2(2) . . ? C18 C17 C22 119.14(19) . . ? C16 C17 C22 122.64(17) . . ? C19 C18 C17 121.8(2) . . ? C19 C18 H18 119.1 . . ? C17 C18 H18 119.1 . . ? C18 C19 C20 119.4(2) . . ? C18 C19 H19 120.3 . . ? C20 C19 H19 120.3 . . ? C19 C20 C21 121.4(2) . . ? C19 C20 H20 119.3 . . ? C21 C20 H20 119.3 . . ? C20 C21 C16 118.52(19) . . ? C20 C21 C25 118.57(19) . . ? C16 C21 C25 122.90(18) . . ? C17 C22 C23 111.59(18) . . ? C17 C22 C24 112.45(18) . . ? C23 C22 C24 110.73(18) . . ? C17 C22 H22 107.3 . . ? C23 C22 H22 107.3 . . ? C24 C22 H22 107.3 . . ? C22 C23 H23A 109.5 . . ? C22 C23 H23B 109.5 . . ? H23A C23 H23B 109.5 . . ? C22 C23 H23C 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? C22 C24 H24A 109.5 . . ? C22 C24 H24B 109.5 . . ? H24A C24 H24B 109.5 . . ? C22 C24 H24C 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C21 C25 C26 112.52(19) . . ? C21 C25 C27 111.21(18) . . ? C26 C25 C27 109.43(18) . . ? C21 C25 H25 107.8 . . ? C26 C25 H25 107.8 . . ? C27 C25 H25 107.8 . . ? C25 C26 H26A 109.5 . . ? C25 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C25 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C25 C27 H27A 109.5 . . ? C25 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? C25 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? Si5 C28 H28A 109.5 . . ? Si5 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? Si5 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? Si5 C29 H29A 109.5 . . ? Si5 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? Si5 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? Si5 C30 H30A 109.5 . . ? Si5 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? Si5 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ge1A N1 1.781(4) . ? Ge1A Si3 2.383(4) . ? Ge1A Ge2 2.449(3) 6_675 ? Ge1A Ge2 2.773(3) . ? Si1B N1 1.813(8) . ? Si1B Ge2 2.338(8) 6_675 ? Si1B Si3 2.360(8) . ? Si1B Ge2 2.622(8) . ? Ge2 Si1B 2.338(8) 6_675 ? Ge2 Ge1A 2.449(3) 6_675 ? Ge2 Si3 2.4832(5) . ? Ge2 Ge2 2.7798(4) 6_675 ? Si3 N2 1.7396(16) . ? Si3 Si3 2.3950(10) 6_675 ? Si4 N1 1.7585(18) . ? Si4 C15 1.860(2) . ? Si4 C14 1.864(3) . ? Si4 C13 1.865(2) . ? Si5 N2 1.7653(16) . ? Si5 C29 1.857(2) . ? Si5 C30 1.858(2) . ? Si5 C28 1.864(2) . ? N1 C1 1.450(2) . ? N2 C16 1.458(2) . ? C1 C2 1.411(3) . ? C1 C6 1.412(3) . ? C2 C3 1.394(3) . ? C2 C7 1.520(3) . ? C3 C4 1.373(3) . ? C3 H3 0.9500 . ? C4 C5 1.381(4) . ? C4 H4 0.9500 . ? C5 C6 1.394(3) . ? C5 H5 0.9500 . ? C6 C10 1.515(3) . ? C7 C8 1.524(3) . ? C7 C9 1.531(3) . ? C7 H7 1.0000 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 C11 1.525(3) . ? C10 C12 1.530(3) . ? C10 H10 1.0000 . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C16 C21 1.407(3) . ? C16 C17 1.408(3) . ? C17 C18 1.396(3) . ? C17 C22 1.514(3) . ? C18 C19 1.375(3) . ? C18 H18 0.9500 . ? C19 C20 1.382(3) . ? C19 H19 0.9500 . ? C20 C21 1.395(3) . ? C20 H20 0.9500 . ? C21 C25 1.520(3) . ? C22 C23 1.523(3) . ? C22 C24 1.527(3) . ? C22 H22 1.0000 . ? C23 H23A 0.9800 . ? C23 H23B 0.9800 . ? C23 H23C 0.9800 . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? C25 C26 1.525(3) . ? C25 C27 1.529(3) . ? C25 H25 1.0000 . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C27 H27C 0.9800 . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C15 Si4 N1 C1 124.00(15) . . . . ? C14 Si4 N1 C1 3.83(18) . . . . ? C13 Si4 N1 C1 -115.78(16) . . . . ? C15 Si4 N1 Ge1A -69.7(2) . . . . ? C14 Si4 N1 Ge1A 170.17(19) . . . . ? C13 Si4 N1 Ge1A 50.6(2) . . . . ? C15 Si4 N1 Si1B -65.5(4) . . . . ? C14 Si4 N1 Si1B 174.3(4) . . . . ? C13 Si4 N1 Si1B 54.7(4) . . . . ? Si3 Ge1A N1 C1 -135.3(3) . . . . ? Ge2 Ge1A N1 C1 -4.2(2) 6_675 . . . ? Ge2 Ge1A N1 C1 -74.1(2) . . . . ? Si3 Ge1A N1 Si4 57.7(3) . . . . ? Ge2 Ge1A N1 Si4 -171.19(10) 6_675 . . . ? Ge2 Ge1A N1 Si4 118.89(13) . . . . ? Ge2 Si1B N1 C1 2.9(5) 6_675 . . . ? Si3 Si1B N1 C1 -147.6(6) . . . . ? Ge2 Si1B N1 C1 -75.0(4) . . . . ? Ge2 Si1B N1 Si4 -168.23(19) 6_675 . . . ? Si3 Si1B N1 Si4 41.2(8) . . . . ? Ge2 Si1B N1 Si4 113.9(3) . . . . ? Si1B Si3 N2 C16 116.5(3) . . . . ? Ge1A Si3 N2 C16 120.97(17) . . . . ? Si3 Si3 N2 C16 -103.33(14) 6_675 . . . ? Ge2 Si3 N2 C16 29.67(16) . . . . ? Si1B Si3 N2 Si5 -63.5(3) . . . . ? Ge1A Si3 N2 Si5 -59.00(17) . . . . ? Si3 Si3 N2 Si5 76.70(14) 6_675 . . . ? Ge2 Si3 N2 Si5 -150.31(8) . . . . ? C29 Si5 N2 C16 -117.90(15) . . . . ? C30 Si5 N2 C16 122.76(15) . . . . ? C28 Si5 N2 C16 3.06(16) . . . . ? C29 Si5 N2 Si3 62.08(15) . . . . ? C30 Si5 N2 Si3 -57.26(15) . . . . ? C28 Si5 N2 Si3 -176.97(11) . . . . ? Si4 N1 C1 C2 85.4(2) . . . . ? Ge1A N1 C1 C2 -82.4(2) . . . . ? Si1B N1 C1 C2 -86.7(3) . . . . ? Si4 N1 C1 C6 -96.1(2) . . . . ? Ge1A N1 C1 C6 96.1(2) . . . . ? Si1B N1 C1 C6 91.8(3) . . . . ? C6 C1 C2 C3 0.4(3) . . . . ? N1 C1 C2 C3 178.88(18) . . . . ? C6 C1 C2 C7 -179.75(19) . . . . ? N1 C1 C2 C7 -1.3(3) . . . . ? C1 C2 C3 C4 -0.1(3) . . . . ? C7 C2 C3 C4 -179.9(2) . . . . ? C2 C3 C4 C5 0.4(3) . . . . ? C3 C4 C5 C6 -1.1(3) . . . . ? C4 C5 C6 C1 1.4(3) . . . . ? C4 C5 C6 C10 -179.8(2) . . . . ? C2 C1 C6 C5 -1.0(3) . . . . ? N1 C1 C6 C5 -179.52(18) . . . . ? C2 C1 C6 C10 -179.76(19) . . . . ? N1 C1 C6 C10 1.7(3) . . . . ? C3 C2 C7 C8 59.9(3) . . . . ? C1 C2 C7 C8 -119.9(2) . . . . ? C3 C2 C7 C9 -63.9(3) . . . . ? C1 C2 C7 C9 116.2(2) . . . . ? C5 C6 C10 C11 -79.8(3) . . . . ? C1 C6 C10 C11 98.9(2) . . . . ? C5 C6 C10 C12 43.8(3) . . . . ? C1 C6 C10 C12 -137.5(2) . . . . ? Si3 N2 C16 C21 -94.53(19) . . . . ? Si5 N2 C16 C21 85.45(19) . . . . ? Si3 N2 C16 C17 87.90(19) . . . . ? Si5 N2 C16 C17 -92.12(19) . . . . ? C21 C16 C17 C18 -2.9(3) . . . . ? N2 C16 C17 C18 174.71(18) . . . . ? C21 C16 C17 C22 176.52(18) . . . . ? N2 C16 C17 C22 -5.9(3) . . . . ? C16 C17 C18 C19 1.7(3) . . . . ? C22 C17 C18 C19 -177.7(2) . . . . ? C17 C18 C19 C20 0.7(4) . . . . ? C18 C19 C20 C21 -2.0(3) . . . . ? C19 C20 C21 C16 0.8(3) . . . . ? C19 C20 C21 C25 -179.4(2) . . . . ? C17 C16 C21 C20 1.6(3) . . . . ? N2 C16 C21 C20 -175.90(18) . . . . ? C17 C16 C21 C25 -178.10(19) . . . . ? N2 C16 C21 C25 4.4(3) . . . . ? C18 C17 C22 C23 58.8(3) . . . . ? C16 C17 C22 C23 -120.5(2) . . . . ? C18 C17 C22 C24 -66.3(3) . . . . ? C16 C17 C22 C24 114.3(2) . . . . ? C20 C21 C25 C26 64.2(3) . . . . ? C16 C21 C25 C26 -116.1(2) . . . . ? C20 C21 C25 C27 -59.0(3) . . . . ? C16 C21 C25 C27 120.7(2) . . . . ?