Crystallography Open Database

Information card for entry 7710512

Preview

Coordinates	7710512.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H39 F3 Ge O3 S Si2
Calculated formula	C24 H39 F3 Ge O3 S Si2
SMILES	[Ge]1(OS(=O)(=O)C(F)(F)F)(C(=C(C(=C1[Si](C)(C)C)C)C)[Si](C)(C)C)c1c(c(c(c(c1C)C)C)C)C
Title of publication	Covalent triflates as synthons for silolyl- and germolyl cations
Authors of publication	Wohltmann, Wiebke Marie; Schmidtmann, Marc; Müller, Thomas
Journal of publication	Dalton Transactions
Year of publication	2022
a	9.6804 ± 0.0007 Å
b	10.4638 ± 0.0007 Å
c	14.8954 ± 0.0011 Å
α	82.721 ± 0.002°
β	80.211 ± 0.003°
γ	75.579 ± 0.002°
Cell volume	1434.36 ± 0.18 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0424
Residual factor for significantly intense reflections	0.0318
Weighted residual factors for significantly intense reflections	0.0703
Weighted residual factors for all reflections included in the refinement	0.0743
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
276073 (current)	2022-06-17	cif/ Adding structures of 7710509, 7710510, 7710511, 7710512, 7710513, 7710514, 7710515, 7710516, 7710517, 7710518, 7710519, 7710520 via cif-deposit CGI script.	7710512.cif