#------------------------------------------------------------------------------ #$Date: 2022-08-03 01:54:39 +0300 (Wed, 03 Aug 2022) $ #$Revision: 277047 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/71/08/7710881.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7710881 loop_ _publ_author_name 'Kim, Minyoung' 'Park, Seongchul' 'Song, Dayoon' 'Moon, Dohyun' 'You, Youngmin' 'Lim, Manho' 'Lee, Hong-In' _publ_section_title ; Visible-light NO photolysis of ruthenium nitrosyl complexes with N2O2 ligands bearing \p-extended rings and their photorelease dynamics. ; _journal_issue 30 _journal_name_full 'Dalton transactions (Cambridge, England : 2003)' _journal_page_first 11404 _journal_page_last 11415 _journal_paper_doi 10.1039/d2dt01019d _journal_volume 51 _journal_year 2022 _chemical_formula_moiety 'C21 H18 Cl N2 O3 Ru, C H4 O' _chemical_formula_sum 'C22 H22 Cl N2 O4 Ru' _chemical_formula_weight 514.93 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2019/2 _audit_update_record ; 2022-06-03 deposited with the CCDC. 2022-06-16 downloaded from the CCDC. ; _cell_angle_alpha 109.75(3) _cell_angle_beta 102.83(3) _cell_angle_gamma 102.50(3) _cell_formula_units_Z 2 _cell_length_a 7.4300(15) _cell_length_b 11.531(2) _cell_length_c 13.619(3) _cell_measurement_reflns_used 31150 _cell_measurement_temperature 173(2) _cell_measurement_theta_max 33.548 _cell_measurement_theta_min 0.361 _cell_volume 1015.3(5) _computing_cell_refinement 'HKL3000sm(Otwinowski & Minor, 1997)' _computing_data_collection 'PAL BL2D-SMDC Program(Shin et.al, 2016)' _computing_data_reduction 'HKL3000sm(Otwinowski & Minor, 1997)' _computing_molecular_graphics ORTEP3 _computing_publication_material CIFTAB _computing_structure_refinement 'SHELXL-2019/2(Sheldrick, 2018)' _computing_structure_solution 'SHELXT-2018(Sheldrick, 2018)' _diffrn_ambient_temperature 173(2) _diffrn_measured_fraction_theta_full 0.950 _diffrn_measured_fraction_theta_max 0.933 _diffrn_measurement_device_type 'Rayonix MX225HS CCD area detector' _diffrn_measurement_method 'omega scan' _diffrn_radiation_type synchrotron _diffrn_radiation_wavelength 0.630 _diffrn_reflns_av_R_equivalents 0.0259 _diffrn_reflns_av_unetI/netI 0.0352 _diffrn_reflns_Laue_measured_fraction_full 0.950 _diffrn_reflns_Laue_measured_fraction_max 0.933 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 11145 _diffrn_reflns_point_group_measured_fraction_full 0.950 _diffrn_reflns_point_group_measured_fraction_max 0.933 _diffrn_reflns_theta_full 22.210 _diffrn_reflns_theta_max 26.498 _diffrn_reflns_theta_min 1.487 _diffrn_source 'PLSII 2D bending magnet' _exptl_absorpt_coefficient_mu 0.670 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.935 _exptl_absorpt_correction_type empirical _exptl_absorpt_process_details 'HKL3000sm Scalepack(Otwinowski et.al,2003)' _exptl_crystal_colour green _exptl_crystal_density_diffrn 1.684 _exptl_crystal_description block _exptl_crystal_F_000 522 _exptl_crystal_size_max 0.150 _exptl_crystal_size_mid 0.130 _exptl_crystal_size_min 0.110 _refine_diff_density_max 0.825 _refine_diff_density_min -1.394 _refine_diff_density_rms 0.114 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.102 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 285 _refine_ls_number_reflns 5657 _refine_ls_number_restraints 4 _refine_ls_restrained_S_all 1.103 _refine_ls_R_factor_all 0.0364 _refine_ls_R_factor_gt 0.0340 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0569P)^2^+0.8196P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0952 _refine_ls_wR_factor_ref 0.0966 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5205 _reflns_number_total 5657 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d2dt01019d2.cif _cod_data_source_block Ru_salophenCl_MeOH_a _cod_original_cell_volume 1015.3(4) _cod_database_code 7710881 _shelx_shelxl_version_number 2019/2 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.906 _shelx_estimated_absorpt_t_max 0.930 _shelx_res_file ; TITL Ru_salophenCl_MeOH in P-1 Ru_salophenCl_MeOH_a.res created by SHELXL-2019/2 at 16:24:50 on 06-May-2022 CELL 0.63000 7.4300 11.5310 13.6190 109.746 102.830 102.505 ZERR 2.000 0.0015 0.0023 0.0027 0.030 0.030 0.030 LATT 1 SFAC C H N O CL RU DISP C 0.0021 0.0012 9.00 DISP H 0.0000 0.0000 0.66 DISP N 0.0044 0.0025 14.78 DISP O 0.0080 0.0047 23.75 DISP Cl 0.1230 0.1255 471.48 DISP Ru -1.7757 0.6751 2592.08 UNIT 44 44 4 8 2 2 OMIT 0 -2 6 OMIT 3 -12 13 OMIT -1 -3 7 OMIT -3 53 TEMP -100 SIZE 0.15 0.13 0.11 L.S. 10 BOND $H LIST 4 FMAP -2 PLAN -10 CONF EQIV $1 x+1, y, z EQIV $2 -x+1, -y, -z+1 HTAB O3 O2_$2 HTAB C21 Cl1_$1 HTAB O1SA Cl1 MERG 2 ACTA WGHT 0.056900 0.819600 FVAR 0.41114 0.43947 RU1 6 0.551087 0.240895 0.579311 11.00000 0.00389 0.00776 = 0.01084 -0.00265 -0.00131 -0.00058 CL1 5 0.376148 0.361701 0.667927 11.00000 0.00938 0.01431 = 0.01844 0.00068 0.00370 0.00401 O1 4 0.316609 0.130298 0.445220 11.00000 0.00597 0.01244 = 0.01092 -0.00239 -0.00442 -0.00174 O2 4 0.477513 0.106460 0.640274 11.00000 0.01018 0.00677 = 0.01477 -0.00112 -0.00042 -0.00295 N1 3 0.640889 0.373285 0.523771 11.00000 0.00504 0.00473 = 0.01808 -0.00199 0.00267 -0.00248 N2 3 0.788141 0.351949 0.708772 11.00000 0.00428 0.00953 = 0.01150 -0.00419 -0.00362 -0.00089 C1 1 0.279548 0.153560 0.356429 11.00000 0.00633 0.01272 = 0.01262 -0.00280 -0.00102 0.00269 C2 1 0.115730 0.061759 0.265214 11.00000 0.00788 0.01282 = 0.01670 -0.00219 -0.00132 0.00034 AFIX 43 H2 2 0.040558 -0.011483 0.271805 11.00000 -1.20000 AFIX 0 C3 1 0.063791 0.076442 0.168114 11.00000 0.01064 0.01749 = 0.01459 -0.00204 -0.00248 0.00167 AFIX 43 H3 2 -0.045438 0.012918 0.108496 11.00000 -1.20000 AFIX 0 C4 1 0.170652 0.184875 0.155550 11.00000 0.01433 0.02145 = 0.01458 0.00295 0.00083 0.00531 AFIX 43 H4 2 0.133969 0.194361 0.087985 11.00000 -1.20000 AFIX 0 C5 1 0.327761 0.276114 0.242004 11.00000 0.01183 0.01864 = 0.01576 0.00280 0.00146 0.00577 AFIX 43 H5 2 0.397966 0.349774 0.233918 11.00000 -1.20000 AFIX 0 C6 1 0.388906 0.263555 0.343931 11.00000 0.00710 0.01341 = 0.01223 -0.00066 0.00012 0.00322 C7 1 0.556072 0.366306 0.425449 11.00000 0.00931 0.01275 = 0.01458 0.00224 0.00298 0.00343 AFIX 43 H7 2 0.610533 0.435432 0.407033 11.00000 -1.20000 AFIX 0 C8 1 0.814438 0.474859 0.598976 11.00000 0.00694 0.00915 = 0.01420 -0.00241 0.00140 0.00135 C9 1 0.904900 0.581583 0.580988 11.00000 0.01115 0.01036 = 0.01925 -0.00016 0.00596 0.00226 AFIX 43 H9 2 0.847450 0.593213 0.516806 11.00000 -1.20000 AFIX 0 C10 1 1.079594 0.670652 0.657673 11.00000 0.01129 0.00862 = 0.02409 -0.00308 0.00688 -0.00026 AFIX 43 H10 2 1.140590 0.744168 0.646234 11.00000 -1.20000 AFIX 0 C11 1 1.166098 0.653530 0.750810 11.00000 0.00852 0.01283 = 0.02001 -0.00628 0.00262 -0.00260 AFIX 43 H11 2 1.287725 0.713916 0.801324 11.00000 -1.20000 AFIX 0 C12 1 1.076464 0.548767 0.770972 11.00000 0.00761 0.01306 = 0.01696 -0.00386 -0.00008 -0.00068 AFIX 43 H12 2 1.136147 0.537380 0.834882 11.00000 -1.20000 AFIX 0 C13 1 0.897543 0.460440 0.696094 11.00000 0.00661 0.00794 = 0.01491 -0.00339 0.00069 0.00039 C14 1 0.830839 0.335384 0.800295 11.00000 0.00766 0.01234 = 0.01410 -0.00217 -0.00278 -0.00018 AFIX 43 H14 2 0.942622 0.397861 0.858770 11.00000 -1.20000 AFIX 0 C15 1 0.723410 0.230731 0.820438 11.00000 0.00872 0.01344 = 0.01304 -0.00172 -0.00073 0.00278 C16 1 0.794798 0.235820 0.927871 11.00000 0.01123 0.01906 = 0.01298 -0.00062 -0.00172 0.00312 AFIX 43 H16 2 0.904967 0.306710 0.980034 11.00000 -1.20000 AFIX 0 C17 1 0.710440 0.142014 0.959174 11.00000 0.01467 0.02326 = 0.01414 0.00298 0.00109 0.00558 AFIX 43 H17 2 0.762302 0.147430 1.031518 11.00000 -1.20000 AFIX 0 C18 1 0.546176 0.037802 0.882629 11.00000 0.01699 0.01737 = 0.01803 0.00237 0.00408 0.00184 AFIX 43 H18 2 0.486455 -0.027835 0.903271 11.00000 -1.20000 AFIX 0 C19 1 0.471368 0.030274 0.778015 11.00000 0.01364 0.01399 = 0.01584 -0.00199 0.00072 -0.00035 AFIX 43 H19 2 0.358825 -0.040104 0.727824 11.00000 -1.20000 AFIX 0 C20 1 0.557183 0.124115 0.743357 11.00000 0.00932 0.01321 = 0.01153 -0.00115 0.00078 0.00391 DFIX 0.82 0.01 O3 H1O3 DANG 1.82 0.01 C21 H1O3 O3 4 0.699174 0.131587 0.495758 11.00000 0.00589 0.00937 = 0.01815 -0.00519 0.00105 0.00126 H1O3 2 0.652000 0.054819 0.456039 11.00000 -1.50000 C21 1 0.905122 0.151877 0.534022 11.00000 0.00816 0.01716 = 0.02477 0.00006 0.00223 0.00315 AFIX 137 H21A 2 0.942715 0.097201 0.474707 11.00000 -1.50000 H21B 2 0.935690 0.128810 0.597352 11.00000 -1.50000 H21C 2 0.977031 0.243420 0.556031 11.00000 -1.50000 AFIX 0 EXYZ C1SA O1SB EADP C1SA O1SB PART 1 21 DFIX 1.43 O1SA C1SA O1SA 4 0.356150 0.413563 0.907416 21.00000 0.02313 0.02211 = 0.01650 0.00527 0.00581 0.00647 AFIX 143 H1SA 2 0.361000 0.387812 0.842821 21.00000 -1.50000 AFIX 0 C1SA 1 0.309304 0.308809 0.934607 21.00000 0.06859 0.06503 = 0.11795 0.04037 0.06351 0.03478 AFIX 133 H1S1 2 0.408437 0.265151 0.929529 21.00000 -1.50000 H1S2 2 0.182142 0.247819 0.883613 21.00000 -1.50000 H1S3 2 0.303981 0.338878 1.010037 21.00000 -1.50000 AFIX 0 PART 2 -21 DFIX 1.43 O1SB C1SB O1SB 4 0.309304 0.308809 0.934607 -21.00000 0.06859 0.06503 = 0.11795 0.04037 0.06351 0.03478 AFIX 143 H1SB 2 0.212721 0.241500 0.909862 -21.00000 -1.50000 AFIX 0 C1SB 1 0.256521 0.417453 0.985126 -21.00000 0.00801 0.02272 = 0.02595 -0.00257 -0.00108 0.00198 AFIX 133 H1S4 2 0.197149 0.404464 1.039648 -21.00000 -1.50000 H1S5 2 0.162814 0.429594 0.929358 -21.00000 -1.50000 H1S6 2 0.372528 0.494609 1.021854 -21.00000 -1.50000 PART 0 AFIX 0 HKLF 4 REM Ru_salophenCl_MeOH in P-1 REM wR2 = 0.0966, GooF = S = 1.102, Restrained GooF = 1.103 for all data REM R1 = 0.0340 for 5205 Fo > 4sig(Fo) and 0.0364 for all 5657 data REM 285 parameters refined using 4 restraints END WGHT 0.0569 0.8196 REM Highest difference peak 0.825, deepest hole -1.394, 1-sigma level 0.114 Q1 1 0.5836 0.2196 0.5305 11.00000 0.05 -1.39 Q2 1 0.5165 0.2588 0.6266 11.00000 0.05 -1.31 Q3 1 0.2536 0.2678 0.8891 11.00000 0.05 -0.87 Q4 1 0.4657 0.2402 0.5433 11.00000 0.05 -0.84 Q5 1 0.5719 0.3502 0.4763 11.00000 0.05 0.83 Q6 1 0.6383 0.2359 0.6130 11.00000 0.05 -0.81 Q7 1 0.5687 0.2822 0.5506 11.00000 0.05 -0.81 Q8 1 0.6223 0.3132 0.6521 11.00000 0.05 0.81 Q9 1 0.2600 0.4343 0.9638 11.00000 0.05 0.76 Q10 1 0.5626 0.3216 0.4988 11.00000 0.05 -0.74 ; _shelx_res_checksum 89209 _shelx_hkl_file ; 0 0 1 2419.73 68.13 0 0 -1 2620.65 72.18 0 0 2 21.34 0.99 0 0 -2 21.13 1.06 0 0 3 10.71 0.70 0 0 -3 9.48 0.60 0 0 4 47.56 2.15 0 0 -4 46.96 1.95 0 0 5 213.32 7.26 0 0 -5 211.92 7.14 0 0 6 311.75 9.77 0 0 -6 320.62 9.79 0 0 7 128.43 7.09 0 0 -7 129.05 4.63 0 0 8 230.18 7.40 0 0 -8 249.40 7.89 0 0 9 92.68 3.50 0 0 -9 100.11 4.00 0 0 10 11.70 0.92 0 0 -10 11.91 1.23 0 0 11 122.37 4.94 0 0 -11 127.51 4.65 0 0 12 468.68 14.42 0 0 -12 456.40 13.02 0 0 13 302.17 8.78 0 0 -13 299.40 9.50 0 0 14 80.02 3.14 0 0 -14 74.93 3.16 0 0 15 17.34 1.86 0 0 -15 16.62 2.12 0 0 16 11.26 1.54 0 0 -16 11.79 1.52 0 0 17 61.84 3.04 0 0 -17 60.10 3.18 0 0 18 44.67 3.30 0 0 -18 42.78 4.94 0 0 19 36.56 2.94 0 0 -19 31.11 2.80 0 0 20 15.97 2.19 0 0 -20 13.19 2.12 0 1 -21 6.13 1.66 0 -1 21 6.99 1.74 0 1 -20 5.38 1.76 0 -1 20 6.61 1.86 0 1 -19 4.27 3.16 0 -1 19 2.17 2.12 0 1 -18 14.47 2.46 0 -1 18 18.21 2.56 0 1 -17 76.40 3.55 0 -1 17 71.99 3.14 0 1 -16 92.08 3.64 0 -1 16 90.03 4.44 0 1 -15 170.73 5.79 0 -1 15 154.98 5.55 0 1 -14 163.76 5.96 0 -1 14 165.33 5.91 0 1 -13 44.91 2.22 0 -1 13 43.15 2.46 0 1 -12 38.56 1.93 0 -1 12 28.99 2.27 0 1 -11 117.04 5.60 0 -1 11 118.27 4.20 0 1 -10 403.37 11.87 0 -1 10 379.40 11.77 0 1 -9 353.54 11.70 0 -1 9 361.19 10.64 0 1 -8 24.55 1.37 0 -1 8 20.38 1.09 0 1 -7 19.29 1.04 0 -1 7 18.35 1.11 0 1 -6 1.25 0.43 0 -1 6 1.45 0.29 0 1 -5 349.15 15.07 0 -1 5 339.72 11.02 0 1 -4 76.16 2.89 0 -1 4 76.28 3.09 0 1 -3 3046.91 111.57 0 -1 3 2956.25 120.88 0 1 -2 436.12 11.19 0 -1 2 427.15 11.21 0 1 0 16.35 0.68 0 -1 0 16.23 1.04 0 1 1 589.65 21.22 0 -1 -1 649.49 24.96 0 1 2 117.65 5.76 0 -1 -2 114.20 5.38 0 1 3 276.24 8.83 0 -1 -3 278.13 8.83 0 1 4 55.95 2.36 0 -1 -4 53.49 2.34 0 1 5 213.22 7.09 0 -1 -5 227.12 7.31 0 1 6 8.27 0.92 0 -1 -6 7.67 0.96 0 1 7 0.94 0.51 0 -1 -7 0.84 0.53 0 1 8 347.54 10.44 0 -1 -8 323.44 10.35 0 1 9 712.41 19.95 0 -1 -9 712.00 28.63 0 1 10 41.53 1.98 0 -1 -10 45.75 2.19 0 1 11 2.99 1.16 0 -1 -11 4.12 0.99 0 1 12 1.98 1.06 0 -1 -12 1.09 1.01 0 1 13 1.69 1.25 0 -1 -13 1.06 1.30 0 1 14 81.16 3.35 0 -1 -14 84.53 4.03 0 1 15 24.19 1.98 0 -1 -15 23.20 2.07 0 1 16 23.27 2.10 0 -1 -16 21.68 2.17 0 1 17 47.03 3.14 0 -1 -17 40.69 3.23 0 1 18 5.31 1.86 0 -1 -18 5.28 2.00 0 1 19 5.74 2.12 0 -1 -19 4.24 2.34 0 2 -22 -0.05 0.96 0 -2 22 0.58 1.04 0 2 -21 4.10 2.32 0 -2 21 4.08 1.95 0 2 -20 4.39 1.71 0 -2 20 4.61 1.93 0 2 -19 8.63 1.81 0 -2 19 6.80 1.71 0 2 -18 72.26 3.26 0 -2 18 74.84 3.18 0 2 -17 92.52 4.08 0 -2 17 90.95 3.52 0 2 -16 48.04 2.27 0 -2 16 41.77 2.34 0 2 -15 7.57 1.45 0 -2 15 6.20 1.74 0 2 -14 76.33 2.82 0 -2 14 74.09 3.04 0 2 -13 223.88 7.69 0 -2 13 220.22 7.38 0 2 -12 356.85 10.27 0 -2 12 323.51 9.86 0 2 -11 130.57 4.34 0 -2 11 118.78 4.41 0 2 -10 4.32 0.80 0 -2 10 3.86 0.68 0 2 -9 49.51 2.07 0 -2 9 45.70 2.17 0 2 -8 239.27 7.93 0 -2 8 239.73 7.67 0 2 -7 67.17 2.60 0 -2 7 64.15 2.51 0 2 -6 1.69 0.41 0 -2 6 2.24 0.53 0 2 -5 970.69 25.56 0 -2 5 943.97 25.08 0 2 -4 644.47 23.03 0 -2 4 598.99 15.63 0 2 -3 5.02 0.39 0 2 -1 934.99 23.23 0 -2 1 1009.37 24.33 0 2 0 1349.26 34.22 0 -2 0 1358.53 35.48 0 2 1 246.36 7.48 0 -2 -1 256.83 8.15 0 2 2 411.93 17.17 0 -2 -2 415.35 17.41 0 2 3 -0.53 0.65 0 -2 -3 -0.92 0.94 0 2 4 4.00 0.51 0 -2 -4 4.65 0.58 0 2 5 36.44 1.64 0 -2 -5 40.57 1.78 0 2 6 547.40 16.21 0 -2 -6 573.54 16.40 0 2 7 727.65 20.55 0 -2 -7 737.90 21.20 0 2 8 428.33 12.88 0 -2 -8 448.69 13.22 0 2 9 0.75 0.80 0 -2 -9 0.99 0.92 0 2 10 32.51 2.10 0 -2 -10 33.69 1.88 0 2 11 17.56 1.86 0 -2 -11 16.11 1.78 0 2 12 233.70 8.08 0 -2 -12 232.49 7.84 0 2 13 141.31 4.99 0 -2 -13 152.64 5.52 0 2 14 103.44 5.21 0 -2 -14 109.06 4.27 0 2 15 2.53 1.45 0 -2 -15 2.27 1.50 0 2 16 26.34 2.27 0 -2 -16 22.55 2.58 0 2 17 0.75 1.83 0 -2 -17 2.22 1.98 0 2 18 54.58 3.38 0 -2 -18 49.37 3.16 0 2 19 29.35 3.01 0 -2 -19 27.30 3.28 0 3 -22 1.74 1.50 0 -3 22 0.84 1.13 0 3 -21 7.57 1.62 0 -3 21 7.07 1.71 0 3 -20 5.14 2.48 0 -3 20 4.63 1.95 0 3 -19 0.10 1.35 0 -3 19 -0.48 1.86 0 3 -18 0.27 1.13 0 -3 18 1.66 1.06 0 3 -17 77.78 4.53 0 -3 17 72.18 3.59 0 3 -16 139.93 5.11 0 -3 16 138.60 6.68 0 3 -15 247.69 7.67 0 -3 15 250.92 8.18 0 3 -14 73.12 2.87 0 -3 14 67.14 2.82 0 3 -13 0.82 0.80 0 -3 13 0.87 1.06 0 3 -12 46.26 1.93 0 -3 12 42.30 1.74 0 3 -11 236.18 7.21 0 -3 11 246.97 8.44 0 3 -10 174.44 5.38 0 -3 10 178.18 5.81 0 3 -9 267.34 8.25 0 -3 9 282.88 8.54 0 3 -8 581.38 16.01 0 -3 8 551.62 15.77 0 3 -7 200.30 6.54 0 -3 7 208.91 6.78 0 3 -6 1.13 0.27 0 -3 6 1.42 0.27 0 3 -5 331.04 9.00 0 -3 5 341.68 13.24 0 3 -4 1715.11 40.98 0 3 -3 1672.97 56.39 0 3 -2 1393.13 34.17 0 -3 2 1394.36 49.37 0 3 -1 206.88 6.44 0 -3 1 224.63 7.07 0 3 0 18.72 0.92 0 -3 0 19.97 1.09 0 3 1 22.86 1.25 0 -3 -1 22.14 1.76 0 3 2 94.25 3.57 0 -3 -2 95.12 3.47 0 3 3 353.20 11.19 0 -3 -3 359.84 11.17 0 3 4 1476.10 52.55 0 -3 -4 1493.85 52.07 0 3 5 950.77 27.01 0 -3 -5 978.77 25.76 0 3 6 68.54 2.97 0 -3 -6 67.67 3.01 0 3 7 5.06 0.80 0 -3 -7 4.82 0.82 0 3 8 411.35 13.89 0 -3 -8 428.23 14.45 0 3 9 908.30 26.67 0 -3 -9 997.87 36.88 0 3 10 119.77 5.21 0 -3 -10 113.79 4.46 0 3 11 173.96 6.22 0 -3 -11 167.47 6.17 0 3 12 17.34 1.71 0 -3 -12 16.13 1.74 0 3 13 4.32 1.37 0 -3 -13 4.20 1.47 0 3 14 7.98 2.73 0 -3 -14 8.20 2.29 0 3 15 12.32 1.74 0 -3 -15 12.16 2.00 0 3 16 66.73 3.55 0 -3 -16 60.17 3.69 0 3 17 60.82 4.08 0 -3 -17 61.52 4.37 0 3 18 25.69 2.75 0 -3 -18 22.33 2.56 0 4 -22 -0.34 1.74 0 -4 22 0.17 1.86 0 4 -21 0.19 1.33 0 -4 21 -0.17 1.74 0 4 -20 26.77 3.30 0 -4 20 30.05 2.12 0 4 -19 16.35 1.74 0 -4 19 17.00 1.91 0 4 -18 47.05 2.48 0 -4 18 50.19 2.41 0 4 -17 123.82 4.37 0 -4 17 134.89 4.56 0 4 -16 4.20 0.92 0 -4 16 3.40 0.89 0 4 -15 20.21 1.52 0 -4 15 19.29 1.40 0 4 -14 60.61 2.51 0 -4 14 65.82 2.39 0 4 -13 2.03 0.77 0 -4 13 3.59 0.65 0 4 -12 150.47 5.23 0 -4 12 158.31 7.31 0 4 -11 219.66 7.19 0 -4 11 221.52 7.07 0 4 -10 113.86 3.93 0 -4 10 110.22 4.94 0 4 -9 7.67 0.55 0 -4 9 7.81 0.53 0 4 -8 27.57 1.23 0 -4 8 25.23 1.57 0 4 -7 385.57 11.05 0 -4 7 379.13 15.05 0 4 -6 1582.63 38.08 0 4 -3 31.74 1.45 0 -4 3 32.97 1.30 0 4 -2 15.44 1.06 0 -4 2 17.80 0.94 0 4 -1 17.92 0.94 0 -4 1 18.50 1.13 0 4 0 31.93 1.33 0 -4 0 31.30 1.42 0 4 1 1.64 0.46 0 -4 -1 1.25 0.51 0 4 2 77.88 4.03 0 -4 -2 81.73 3.21 0 4 3 85.06 3.30 0 -4 -3 82.53 3.06 0 4 4 150.20 5.23 0 -4 -4 150.45 5.31 0 4 5 230.32 10.11 0 -4 -5 233.87 10.76 0 4 6 594.26 16.35 0 -4 -6 609.33 16.42 0 4 7 354.43 13.24 0 -4 -7 368.35 12.90 0 4 8 290.62 9.89 0 -4 -8 298.14 9.50 0 4 9 7.38 1.52 0 -4 -9 6.42 1.66 0 4 10 114.17 4.39 0 -4 -10 111.35 4.22 0 4 11 46.43 2.63 0 -4 -11 46.60 2.48 0 4 12 60.20 2.99 0 -4 -12 59.11 4.37 0 4 13 115.72 4.97 0 -4 -13 125.27 5.40 0 4 14 90.75 4.15 0 -4 -14 70.98 3.76 0 4 15 9.09 2.19 0 -4 -15 6.99 2.46 0 4 16 0.72 1.81 0 -4 -16 0.46 2.00 0 4 17 19.32 2.87 0 -4 -17 19.54 2.87 0 5 -21 32.03 2.24 0 -5 21 32.12 2.24 0 5 -20 68.08 3.04 0 -5 20 95.67 5.67 0 5 -19 11.94 1.28 0 -5 19 11.34 1.23 0 5 -18 1.13 1.21 0 -5 18 0.41 1.23 0 5 -17 75.25 3.04 0 -5 17 88.46 4.78 0 5 -16 90.56 3.18 0 -5 16 83.35 2.87 0 5 -15 90.37 4.32 0 -5 15 90.75 3.33 0 5 -14 21.49 1.18 0 -5 14 20.33 1.16 0 5 -13 0.10 0.53 0 -5 13 0.19 0.60 0 5 -12 0.19 0.51 0 -5 12 -0.19 0.53 0 5 -11 19.56 1.06 0 -5 11 18.52 1.33 0 5 -10 88.90 3.21 0 -5 10 93.02 3.26 0 5 -9 645.10 17.20 0 -5 9 719.72 19.82 0 5 -8 591.20 22.43 0 -5 8 572.00 21.49 0 5 -4 473.48 12.28 0 -5 4 474.08 18.31 0 5 -3 1811.96 58.51 0 -5 3 1783.17 44.98 0 5 -2 445.72 13.00 0 -5 2 450.64 13.84 0 5 -1 8.61 0.63 0 -5 1 9.04 0.75 0 5 0 7.40 0.68 0 -5 0 7.65 0.70 0 5 1 10.78 0.87 0 -5 -1 12.01 0.89 0 5 2 24.82 1.33 0 -5 -2 22.45 1.18 0 5 3 649.10 18.06 0 -5 -3 646.04 16.98 0 5 4 774.49 21.42 0 -5 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0.70 0 -7 4 7.55 0.55 0 7 -3 219.78 6.80 0 -7 3 213.06 7.28 0 7 -2 38.01 1.69 0 -7 2 39.07 1.83 0 7 -1 356.63 11.14 0 -7 1 349.61 10.56 0 7 0 112.82 4.08 0 -7 0 110.00 3.98 0 7 1 16.50 1.16 0 -7 -1 18.09 1.13 0 7 2 429.95 12.01 0 -7 -2 443.55 13.67 0 7 3 322.89 9.57 0 -7 -3 334.92 10.90 0 7 4 319.46 9.86 0 -7 -4 323.49 11.36 0 7 5 74.64 3.04 0 -7 -5 71.36 4.32 0 7 6 2.00 1.01 0 -7 -6 1.11 1.06 0 7 7 9.19 1.59 0 -7 -7 8.66 1.76 0 7 8 3.01 1.25 0 -7 -8 0.92 1.13 0 7 9 31.23 3.64 0 -7 -9 34.80 2.34 0 7 10 88.54 4.41 0 -7 -10 87.19 4.65 0 7 11 225.04 9.02 0 -7 -11 234.64 7.93 0 7 12 130.96 5.79 0 -7 -12 125.10 6.15 0 7 13 1.13 1.95 0 -7 -13 1.45 1.98 0 7 14 16.86 3.26 0 -7 -14 16.83 3.33 0 8 -21 3.16 0.68 0 8 -20 11.07 0.94 0 -8 20 7.96 1.23 0 8 -19 2.41 0.58 0 -8 19 2.56 0.63 0 8 -18 13.02 1.23 0 -8 18 16.04 1.35 0 -8 17 48.60 1.76 0 8 -16 5.02 0.43 0 8 -6 103.30 4.08 0 -8 6 102.60 5.28 0 8 -5 23.39 1.30 0 -8 5 24.33 1.18 0 8 -4 69.29 2.44 0 8 -3 134.72 4.75 0 -8 3 126.88 4.78 0 8 -2 27.20 1.95 0 -8 2 23.08 1.66 0 8 -1 240.62 8.08 0 -8 1 234.21 7.91 0 8 0 735.35 21.08 0 -8 0 759.61 29.95 0 8 1 1253.54 32.97 0 -8 -1 1227.88 31.30 0 8 2 803.43 21.95 0 -8 -2 808.11 21.39 0 8 3 36.88 2.68 0 -8 -3 35.62 2.19 0 8 4 5.06 1.11 0 -8 -4 4.39 1.30 0 8 5 74.38 3.50 0 -8 -5 78.53 3.52 0 8 6 93.67 3.86 0 -8 -6 97.31 5.11 0 8 7 46.60 2.58 0 -8 -7 40.54 2.58 0 8 8 193.04 8.13 0 -8 -8 186.65 6.99 0 8 9 192.34 6.95 0 -8 -9 188.99 7.28 0 8 10 12.88 3.45 0 -8 -10 8.71 2.15 0 8 11 3.93 2.00 0 -8 -11 1.93 3.06 0 8 12 62.73 3.79 0 -8 -12 50.43 3.79 0 8 13 98.28 5.55 0 -8 -13 88.54 4.80 0 9 -6 8.95 0.55 0 9 -5 13.43 0.72 0 -9 5 13.12 0.80 0 9 -4 57.28 2.10 0 -9 4 57.42 2.34 0 9 -3 134.70 4.27 0 -9 3 124.76 6.54 0 9 -2 231.02 7.33 0 -9 2 253.24 7.65 0 9 -1 611.17 18.11 0 -9 1 517.35 15.70 0 9 0 144.08 4.82 0 -9 0 137.98 4.92 0 9 1 77.76 5.38 0 -9 -1 74.38 3.69 0 9 2 147.70 4.94 0 -9 -2 154.62 4.85 0 9 3 170.83 5.50 0 -9 -3 171.55 6.01 0 9 4 119.36 4.49 0 -9 -4 124.06 5.23 0 9 5 145.24 7.77 0 -9 -5 142.90 5.76 0 9 6 116.80 4.68 0 -9 -6 120.06 5.69 0 9 7 23.47 1.95 0 -9 -7 20.16 2.44 0 9 8 9.70 1.76 0 -9 -8 11.19 1.81 0 9 9 114.70 5.14 0 -9 -9 102.91 5.14 0 9 10 156.52 6.27 0 -9 -10 136.94 6.27 0 9 11 53.35 5.67 0 -9 -11 51.68 6.46 0 9 12 6.54 3.06 0 -9 -12 8.49 3.57 0 10 -7 6.08 0.43 0 -10 7 6.03 0.43 0 10 -6 29.62 1.23 0 -10 6 31.98 2.19 0 10 -5 161.47 6.25 0 -10 5 154.84 5.60 0 10 -4 113.14 3.71 0 -10 4 118.39 4.27 0 10 -3 47.17 2.07 0 -10 3 45.20 2.07 0 10 -2 29.93 1.40 0 -10 2 34.17 1.69 0 10 -1 57.13 2.48 0 -10 1 57.09 2.27 0 10 0 634.20 27.83 0 -10 0 601.98 18.69 0 10 1 524.61 15.19 0 -10 -1 494.07 13.17 0 10 2 2.12 1.18 0 -10 -2 4.17 1.18 0 10 3 3.76 1.06 0 -10 -3 2.32 1.11 0 10 4 52.17 2.89 0 -10 -4 54.84 2.94 0 10 5 1.37 1.47 0 -10 -5 0.46 1.52 0 10 6 145.98 5.81 0 -10 -6 133.71 5.28 0 10 7 169.57 6.90 0 -10 -7 173.24 7.52 0 10 8 214.96 7.93 0 -10 -8 214.77 8.42 0 10 9 79.83 4.29 0 -10 -9 81.04 4.22 0 10 10 2.85 2.65 0 -10 -10 2.34 2.97 0 10 11 3.52 2.12 0 -10 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3.96 -1 14 3 82.75 3.91 1 -14 -2 92.76 3.98 -1 14 2 86.80 4.10 1 -14 -1 83.52 4.34 -1 14 1 101.95 5.72 1 -14 0 12.01 2.03 -1 14 0 11.91 1.86 1 -14 1 6.68 1.64 -1 14 -1 9.82 2.19 1 -14 2 66.37 3.52 -1 14 -2 64.35 2.85 1 -14 3 83.81 4.32 -1 14 -3 75.03 3.04 1 -14 4 106.26 3.69 -1 14 -4 120.20 5.40 1 -14 5 29.50 1.69 -1 14 -5 31.86 1.59 1 -14 6 29.93 1.50 -1 14 -6 25.61 1.69 1 -14 7 5.33 0.72 -1 14 -7 6.56 0.89 1 -14 8 16.21 1.04 -1 14 -8 16.01 1.13 1 -13 -8 7.11 3.18 -1 13 8 10.76 3.98 1 -13 -7 19.46 2.56 -1 13 7 22.09 2.34 1 -13 -6 109.69 5.11 -1 13 6 104.67 5.14 1 -13 -5 166.48 7.07 -1 13 5 171.60 6.13 1 -13 -4 192.80 6.66 -1 13 4 212.28 7.43 1 -13 -3 60.80 3.64 -1 13 3 58.70 3.74 1 -13 -2 2.73 1.62 -1 13 2 0.55 1.74 1 -13 -1 89.50 6.56 -1 13 1 95.75 4.17 1 -13 0 50.09 3.26 -1 13 0 46.55 2.48 1 -13 1 101.92 3.91 -1 13 -1 89.74 3.57 1 -13 2 86.70 3.59 -1 13 -2 77.37 3.23 1 -13 3 31.35 1.81 -1 13 -3 28.29 1.66 1 -13 4 6.13 1.11 -1 13 -4 6.58 0.99 1 -13 5 32.41 1.93 -1 13 -5 32.12 1.45 1 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4 23.80 1.37 4 8 -3 130.40 5.38 -4 -8 3 122.86 4.82 4 8 -2 235.82 7.77 -4 -8 2 198.20 6.97 4 8 -1 127.53 5.11 -4 -8 1 124.37 4.51 4 8 0 135.78 5.57 -4 -8 0 133.54 4.65 4 8 1 0.55 1.21 -4 -8 -1 0.72 1.28 4 8 2 28.05 1.95 -4 -8 -2 26.22 1.86 4 8 3 5.26 1.42 -4 -8 -3 5.45 1.62 4 8 4 15.03 2.36 -4 -8 -4 19.00 2.12 4 8 5 212.40 7.89 -4 -8 -5 214.82 7.84 4 8 6 213.51 11.53 -4 -8 -6 211.08 8.97 4 8 7 40.32 3.23 -4 -8 -7 30.07 3.09 4 8 8 5.14 2.97 -4 -8 -8 6.01 2.34 -4 -9 12 55.59 2.68 -4 -9 11 77.88 3.01 4 9 -10 64.13 2.70 -4 -9 10 62.59 2.39 4 9 -9 9.24 1.33 -4 -9 9 9.48 0.72 4 9 -8 0.53 0.80 -4 -9 8 0.51 0.84 4 9 -7 26.34 1.40 -4 -9 7 27.98 1.57 4 9 -6 165.11 9.45 -4 -9 6 122.52 4.70 4 9 -5 339.63 10.71 -4 -9 4 283.33 9.38 4 9 -3 51.80 3.26 -4 -9 3 48.33 2.63 4 9 -2 1.42 0.94 -4 -9 2 1.21 0.92 4 9 -1 10.01 1.42 -4 -9 1 10.18 1.62 4 9 0 67.77 2.97 -4 -9 0 66.11 3.33 4 9 1 172.95 6.29 -4 -9 -1 164.65 6.56 4 9 2 28.27 2.39 -4 -9 -2 32.08 2.17 4 9 3 9.96 2.53 -4 -9 -3 10.13 1.69 4 9 4 11.91 2.22 -4 -9 -4 7.91 2.58 4 9 5 3.71 2.15 -4 -9 -5 3.28 2.05 4 9 6 183.78 7.96 -4 -9 -6 174.76 7.26 4 9 7 206.18 9.16 -4 -9 -7 189.47 8.59 4 10 -11 -0.05 0.60 -4 -10 11 0.10 0.36 4 10 -10 2.22 0.87 -4 -10 10 2.03 0.48 4 10 -9 76.38 3.50 4 10 -8 206.28 6.61 -4 -10 8 197.62 6.17 4 10 -7 398.38 11.99 -4 -10 7 468.92 13.02 4 10 -6 197.38 6.42 -4 -10 6 194.32 5.69 4 10 -5 4.05 1.09 -4 -10 5 7.52 1.30 4 10 -4 15.82 1.45 -4 -10 4 15.27 1.18 4 10 -3 81.86 5.43 -4 -10 3 115.48 4.32 4 10 -2 151.43 5.86 -4 -10 2 124.28 6.99 4 10 -1 20.91 1.83 -4 -10 1 22.53 1.81 4 10 0 20.50 1.95 -4 -10 0 20.64 2.17 4 10 1 8.56 1.74 -4 -10 -1 4.94 1.45 4 10 2 22.38 2.27 -4 -10 -2 23.66 2.58 4 10 3 -1.11 1.66 -4 -10 -3 0.29 1.52 4 10 4 88.13 4.44 -4 -10 -4 90.59 4.49 4 10 5 81.93 4.49 -4 -10 -5 82.82 4.17 4 10 6 85.81 4.39 -4 -10 -6 93.26 5.60 -4 -11 11 31.02 2.10 4 11 -10 106.02 3.96 -4 -11 10 100.11 4.27 4 11 -9 133.78 4.58 -4 -11 9 124.95 4.39 4 11 -8 16.88 1.40 -4 -11 8 18.52 1.18 4 11 -7 10.11 1.76 -4 -11 7 9.53 1.06 4 11 -6 216.89 9.77 -4 -11 6 223.04 7.04 4 11 -5 241.51 7.69 -4 -11 5 240.36 8.90 4 11 -4 50.57 2.63 -4 -11 4 47.44 2.99 4 11 -3 24.84 1.86 -4 -11 3 23.59 1.64 4 11 -2 16.91 1.66 -4 -11 2 15.24 1.40 4 11 -1 1.40 1.50 -4 -11 1 0.43 1.62 4 11 0 7.31 1.57 -4 -11 0 9.02 1.47 4 11 1 106.55 4.99 -4 -11 -1 92.18 4.24 4 11 2 111.54 5.31 -4 -11 -2 109.71 4.70 4 11 3 88.44 4.87 -4 -11 -3 96.66 4.58 4 11 4 8.18 2.29 -4 -11 -4 8.92 2.46 4 11 5 -0.48 2.03 -4 -11 -5 -0.02 2.07 4 12 -11 5.86 0.84 -4 -12 11 6.05 0.68 4 12 -10 12.01 1.42 -4 -12 10 10.73 0.80 4 12 -9 52.87 2.34 -4 -12 9 45.75 1.83 4 12 -8 67.72 3.01 -4 -12 8 65.99 2.60 4 12 -7 53.59 2.53 -4 -12 7 51.54 2.29 4 12 -6 29.21 1.74 -4 -12 6 33.38 1.86 4 12 -5 6.42 2.34 -4 -12 5 1.95 0.99 4 12 -4 -0.39 2.46 -4 -12 4 0.02 1.37 4 12 -3 29.91 2.46 -4 -12 3 30.68 2.27 4 12 -2 148.01 5.81 -4 -12 2 130.65 4.92 4 12 -1 128.55 5.52 -4 -12 1 128.81 6.03 4 12 0 81.42 3.76 -4 -12 0 90.88 4.78 4 12 1 28.68 2.56 -4 -12 -1 25.23 2.70 4 12 2 5.55 2.12 -4 -12 -2 3.62 2.05 4 12 3 49.42 3.50 -4 -12 -3 45.65 3.62 -4 -13 9 68.59 3.16 4 13 -8 -0.24 1.01 -4 -13 8 -0.63 0.82 4 13 -7 0.55 1.30 -4 -13 7 1.09 1.04 4 13 -6 9.26 1.33 -4 -13 6 10.37 1.33 4 13 -5 52.77 2.77 -4 -13 5 48.50 2.41 4 13 -4 27.59 2.12 -4 -13 4 31.02 1.95 4 13 -3 65.94 2.82 -4 -13 3 62.34 3.04 4 13 -2 39.67 2.73 -4 -13 2 40.49 2.46 4 13 -1 -0.10 1.59 -4 -13 1 1.21 1.69 4 13 0 13.10 2.70 -4 -13 0 13.82 2.75 4 13 1 50.96 3.40 -4 -13 -1 60.90 3.69 4 13 2 132.62 5.52 -4 -13 -2 156.35 6.85 -4 -14 11 0.00 0.31 4 14 -10 14.71 1.76 -4 -14 10 15.24 1.42 -4 -14 9 8.75 0.94 4 14 -8 36.71 2.34 -4 -14 8 40.83 2.03 4 14 -7 13.87 3.01 -4 -14 7 14.42 1.45 4 14 -6 3.79 1.45 -4 -14 6 4.63 1.09 4 14 -5 -0.41 1.50 -4 -14 5 0.34 1.25 4 14 -4 5.84 1.78 -4 -14 4 4.51 1.42 4 14 -3 25.47 2.32 -4 -14 3 23.83 2.34 4 14 -2 141.59 6.39 -4 -14 2 110.31 6.05 4 14 -1 157.30 6.85 -4 -14 1 163.54 6.34 4 14 0 33.76 2.80 -4 -14 0 28.75 2.80 4 14 1 1.30 2.99 -4 -14 -1 -0.05 2.44 4 15 -10 14.66 1.78 -4 -15 10 15.22 1.74 -4 -15 9 6.05 0.89 4 15 -8 0.63 1.37 -4 -15 8 0.94 1.37 4 15 -7 1.11 1.57 -4 -15 7 0.39 0.92 4 15 -6 11.43 2.63 -4 -15 6 12.73 2.00 4 15 -5 11.14 1.66 -4 -15 5 11.91 1.74 4 15 -4 12.95 2.53 -4 -15 4 17.77 2.00 4 15 -3 33.02 3.30 -4 -15 3 42.95 3.04 4 15 -2 -0.87 1.83 -4 -15 2 -0.48 1.59 4 15 -1 1.11 2.27 -4 -15 1 0.55 2.05 4 16 -7 19.05 1.86 4 16 -6 40.86 2.92 -4 -16 6 56.72 4.78 4 16 -5 6.01 2.07 -4 -16 5 6.10 1.81 4 16 -4 3.30 3.28 -4 -16 4 1.66 1.62 4 16 -3 0.19 1.13 -4 -16 3 0.58 2.27 5 -19 1 1.25 1.71 -5 19 -1 0.75 1.76 5 -19 2 3.11 1.78 -5 19 -2 3.35 1.57 5 -19 3 21.51 3.01 -5 19 -3 20.91 2.27 5 -19 4 22.57 2.44 -5 19 -4 28.72 2.58 -5 19 -5 3.83 1.95 5 -18 -1 4.68 2.32 -5 18 1 10.64 3.50 5 -18 0 54.34 3.83 -5 18 0 55.01 3.40 5 -18 1 86.97 6.01 -5 18 -1 79.78 4.08 5 -18 2 18.11 2.12 -5 18 -2 15.15 3.74 5 -18 3 0.22 1.45 -5 18 -3 0.27 1.40 5 -18 4 0.10 2.22 -5 18 -4 3.52 2.51 5 -18 5 18.86 1.88 -5 18 -5 20.67 2.12 5 -18 6 13.17 1.83 -5 18 -6 14.54 1.74 5 -18 7 12.73 1.66 -5 18 -7 10.95 1.69 5 -18 8 5.69 0.92 -5 18 -8 6.46 1.33 5 -17 -3 10.56 3.01 -5 17 3 15.39 2.29 5 -17 -2 81.59 4.87 -5 17 2 77.80 6.42 5 -17 -1 108.26 5.47 -5 17 1 104.12 4.94 5 -17 0 12.42 2.58 -5 17 0 10.64 2.60 5 -17 1 4.39 2.00 -5 17 -1 3.06 1.62 5 -17 2 38.06 3.35 -5 17 -2 43.80 2.87 5 -17 3 27.23 2.27 -5 17 -3 35.33 2.44 5 -17 4 48.72 2.73 -5 17 -4 53.69 3.79 5 -17 5 48.84 3.96 -5 17 -5 52.12 3.09 5 -17 6 39.41 2.46 -5 17 -6 34.68 2.32 5 -17 7 15.22 1.57 -5 17 -7 20.31 1.83 5 -17 8 1.93 0.96 -5 17 -8 2.87 1.98 5 -17 9 8.88 1.18 -5 17 -9 9.55 1.25 5 -17 10 11.12 1.57 -5 17 -10 14.49 1.21 5 -17 11 8.51 1.01 -5 17 -11 5.50 0.84 5 -16 -4 105.44 5.45 -5 16 4 92.61 5.11 5 -16 -3 4.27 2.36 -5 16 3 2.39 2.07 5 -16 -2 1.54 1.69 -5 16 2 -0.10 1.59 5 -16 -1 20.79 3.16 -5 16 1 25.08 2.39 5 -16 0 88.73 4.75 -5 16 0 86.94 4.75 5 -16 1 55.95 6.15 -5 16 -1 57.69 3.21 5 -16 2 7.91 1.91 -5 16 -2 12.47 1.69 5 -16 3 4.34 1.74 -5 16 -3 3.26 1.42 5 -16 4 4.41 1.66 -5 16 -4 1.42 1.47 5 -16 5 2.70 1.04 -5 16 -5 3.50 1.11 5 -16 6 28.48 1.74 -5 16 -6 29.09 2.07 5 -16 7 70.06 2.85 -5 16 -7 72.11 3.11 5 -16 8 73.08 3.21 -5 16 -8 67.72 4.05 5 -16 9 27.01 1.93 -5 16 -9 27.86 1.71 -5 16 -10 2.75 0.99 5 -16 11 -0.07 1.01 -5 16 -11 0.53 1.16 5 -16 12 5.40 0.94 -5 16 -12 4.80 0.77 5 -15 -6 27.88 3.09 -5 15 6 29.01 3.14 5 -15 -5 26.12 2.85 -5 15 5 23.10 2.39 5 -15 -4 6.73 1.91 -5 15 4 4.41 1.93 5 -15 -3 78.43 4.32 -5 15 3 60.25 4.22 5 -15 -2 26.58 2.17 -5 15 2 25.03 2.15 5 -15 -1 32.39 2.80 -5 15 1 35.16 2.77 5 -15 0 21.42 3.64 -5 15 0 18.98 2.22 5 -15 1 0.48 1.45 -5 15 -1 2.34 1.42 5 -15 2 7.50 1.93 -5 15 -2 9.84 1.78 5 -15 3 8.13 1.25 -5 15 -3 9.96 1.35 5 -15 4 110.29 4.82 -5 15 -4 110.82 4.51 5 -15 5 252.42 8.78 -5 15 -5 274.65 11.26 5 -15 6 72.33 3.30 5 -15 7 23.80 1.76 -5 15 -7 17.68 2.32 5 -15 8 1.40 2.00 -5 15 -8 2.24 1.18 5 -15 9 23.83 1.69 -5 15 -9 20.89 1.45 5 -15 10 37.36 2.70 -5 15 -10 42.57 3.47 5 -15 11 16.86 1.45 -5 15 -11 16.18 1.18 5 -15 12 12.44 1.52 -5 15 -12 12.25 1.13 -5 15 -13 0.39 0.84 -5 15 -14 0.05 0.63 5 -14 -7 2.41 2.51 -5 14 7 2.12 2.34 5 -14 -6 136.48 6.46 -5 14 6 132.07 6.73 -5 14 5 348.48 11.87 5 -14 -4 159.83 7.14 -5 14 4 172.10 6.49 5 -14 -3 11.21 1.88 -5 14 3 10.95 1.76 5 -14 -2 15.97 2.19 -5 14 2 16.40 2.22 5 -14 -1 25.25 2.22 -5 14 1 28.68 2.27 5 -14 0 40.52 2.87 -5 14 0 40.83 2.53 5 -14 1 38.42 2.85 -5 14 -1 35.62 2.56 5 -14 2 169.35 7.16 -5 14 -2 136.99 5.81 5 -14 3 161.56 5.81 -5 14 -3 175.91 8.30 5 -14 4 85.06 4.00 -5 14 -4 79.81 3.35 -5 14 -5 0.41 1.33 5 -14 6 24.43 1.54 -5 14 -6 24.99 1.69 5 -14 7 162.19 5.55 -5 14 -7 162.87 5.31 5 -14 8 182.57 9.65 -5 14 -8 186.07 6.27 5 -14 9 37.24 2.19 -5 14 -9 38.44 1.88 5 -14 10 1.28 1.66 -5 14 -10 2.22 0.99 5 -14 11 13.10 1.23 -5 14 -11 12.23 1.23 5 -14 12 4.17 1.30 -5 14 -12 5.33 0.92 5 -14 13 17.63 1.37 -5 14 -13 20.48 1.30 5 -14 14 21.08 2.29 -5 14 -14 18.62 1.28 5 -14 15 2.46 0.92 -5 14 -15 2.75 0.60 5 -13 -9 34.49 3.64 -5 13 9 30.00 3.30 5 -13 -8 119.62 8.01 -5 13 8 109.04 5.28 5 -13 -7 52.09 3.64 -5 13 7 53.32 3.30 5 -13 -6 35.31 3.42 -5 13 6 36.56 3.67 5 -13 -5 0.94 1.86 -5 13 5 -0.14 1.74 5 -13 -4 51.30 4.58 -5 13 4 52.84 3.18 5 -13 -3 139.21 5.45 -5 13 3 140.03 5.23 5 -13 -2 41.84 2.68 -5 13 2 43.53 2.56 5 -13 -1 30.82 2.44 -5 13 1 30.85 2.19 5 -13 0 46.38 2.70 -5 13 0 45.70 3.01 5 -13 1 18.67 1.59 -5 13 -1 21.49 1.59 5 -13 2 -0.02 1.01 -5 13 -2 0.82 1.01 5 -13 3 78.38 3.40 -5 13 -3 78.21 3.16 5 -13 4 191.52 6.25 -5 13 -4 162.65 8.25 5 -13 5 35.21 2.12 -5 13 -5 32.80 2.77 5 -13 6 3.21 1.57 -5 13 -6 3.28 1.13 5 -13 7 26.60 2.65 -5 13 -7 28.00 1.57 5 -13 8 12.52 1.37 -5 13 -8 11.38 1.09 5 -13 9 66.30 5.52 -5 13 -9 85.45 4.39 5 -13 10 28.92 2.22 -5 13 -10 28.39 1.71 5 -13 11 22.43 2.41 -5 13 -11 21.80 1.50 5 -13 12 20.91 2.56 -5 13 -12 19.66 1.33 5 -13 13 15.03 1.25 -5 13 -13 13.58 1.35 5 -13 14 0.22 0.87 -5 13 -14 0.84 0.77 -5 13 -15 3.74 0.84 5 -13 16 15.46 1.16 -5 13 -16 8.73 1.01 5 -12 -10 70.71 4.87 -5 12 10 72.28 4.46 5 -12 -9 75.83 4.75 -5 12 9 70.23 4.20 5 -12 -8 6.05 2.99 -5 12 8 8.18 2.41 5 -12 -7 29.35 2.80 -5 12 7 31.93 2.51 5 -12 -6 156.04 6.34 -5 12 6 161.61 9.19 5 -12 -5 191.21 7.62 -5 12 5 206.74 7.28 5 -12 -4 41.75 2.87 -5 12 4 50.41 2.70 5 -12 -3 9.96 1.78 -5 12 3 10.78 1.62 5 -12 -2 3.18 1.59 -5 12 2 3.23 1.52 5 -12 -1 0.68 1.13 -5 12 1 1.04 1.09 5 -12 0 39.31 2.24 -5 12 0 47.13 2.32 5 -12 1 66.03 2.53 -5 12 -1 69.70 3.01 5 -12 2 180.06 6.44 -5 12 -2 130.72 4.94 5 -12 3 184.52 6.51 -5 12 -3 180.74 10.49 5 -12 4 158.94 5.47 -5 12 -4 145.91 5.86 5 -12 5 9.41 1.13 -5 12 -5 10.88 1.01 5 -12 6 57.50 2.70 -5 12 -6 50.31 3.33 5 -12 7 15.75 1.40 -5 12 -7 14.06 1.37 5 -12 8 84.77 3.38 -5 12 -8 80.50 2.82 5 -12 9 55.52 2.68 -5 12 -9 58.44 4.29 5 -12 10 14.35 1.35 -5 12 -10 13.34 1.11 5 -12 11 0.17 1.52 -5 12 -11 0.84 0.94 5 -12 12 1.25 1.42 -5 12 -12 2.03 0.92 5 -12 13 28.87 2.70 -5 12 -13 33.50 2.44 5 -12 14 29.50 2.63 -5 12 -14 27.54 1.74 5 -12 15 38.56 2.34 -5 12 -15 39.91 2.51 5 -12 16 39.31 2.24 -5 12 -16 32.90 2.05 5 -11 -11 1.25 2.32 -5 11 11 4.87 2.00 5 -11 -10 3.28 2.36 -5 11 10 4.99 2.03 5 -11 -9 80.09 4.97 -5 11 9 84.10 4.53 5 -11 -8 183.17 7.09 -5 11 8 185.37 7.33 5 -11 -7 129.90 5.81 -5 11 7 135.06 5.40 5 -11 -6 7.04 2.00 -5 11 6 6.73 2.15 5 -11 -5 0.58 1.23 -5 11 5 0.60 1.23 5 -11 -4 3.86 1.69 -5 11 4 3.62 1.37 5 -11 -3 30.20 2.34 -5 11 3 31.88 2.19 5 -11 -2 170.22 6.37 -5 11 2 151.65 5.72 5 -11 -1 520.97 17.15 -5 11 1 610.68 16.91 5 -11 0 375.42 11.12 -5 11 0 446.01 19.56 5 -11 1 61.72 2.97 -5 11 -1 65.02 3.04 5 -11 2 21.80 1.54 -5 11 -2 22.67 2.00 5 -11 3 99.49 3.98 -5 11 -3 116.85 4.10 5 -11 4 145.28 5.52 5 -11 5 95.99 5.45 -5 11 -5 81.23 3.23 5 -11 6 12.44 1.35 -5 11 -6 11.26 1.95 5 -11 7 0.96 1.06 -5 11 -7 0.53 1.06 5 -11 8 2.60 0.87 -5 11 -8 3.67 0.87 5 -11 9 4.32 1.18 -5 11 -9 4.56 1.09 5 -11 10 18.91 2.00 -5 11 -10 18.86 1.30 5 -11 11 129.70 5.14 -5 11 -11 127.17 6.80 -5 11 -12 107.28 4.39 5 -11 13 92.06 3.67 -5 11 -13 109.11 6.03 5 -11 14 3.67 1.30 -5 11 -14 6.34 1.28 5 -11 15 17.82 2.70 -5 11 -15 22.09 1.59 5 -11 16 75.61 3.42 -5 11 -16 73.85 4.65 5 -11 17 26.14 2.05 -5 11 -17 26.84 1.69 5 -10 -12 42.33 4.85 -5 10 12 43.10 4.53 5 -10 -11 45.24 3.47 -5 10 11 42.13 4.10 5 -10 -10 95.94 4.85 -5 10 10 92.44 4.85 5 -10 -9 36.39 3.18 -5 10 9 30.48 2.97 5 -10 -8 0.19 1.69 -5 10 8 1.86 2.29 5 -10 -7 13.89 2.22 -5 10 7 15.68 2.19 5 -10 -6 41.70 3.23 -5 10 6 34.44 3.81 5 -10 -5 18.04 1.93 -5 10 5 21.08 1.83 5 -10 -4 137.93 5.64 -5 10 4 147.96 5.84 5 -10 -3 92.08 4.00 -5 10 3 102.89 5.72 5 -10 -2 37.62 2.53 -5 10 2 41.70 2.53 5 -10 -1 15.36 1.57 -5 10 1 16.30 1.54 5 -10 0 72.18 2.70 -5 10 0 73.90 3.16 5 -10 1 283.14 10.23 -5 10 -1 342.81 11.43 5 -10 2 278.97 8.56 -5 10 -2 233.97 7.60 5 -10 3 67.19 2.92 -5 10 -3 72.52 3.45 5 -10 4 3.71 0.89 -5 10 -4 2.60 1.06 5 -10 5 3.93 0.87 -5 10 -5 3.67 0.80 5 -10 6 51.18 2.60 -5 10 -6 50.24 2.07 5 -10 7 55.90 3.30 -5 10 -7 49.61 2.19 5 -10 8 144.83 4.90 -5 10 -8 112.63 4.03 5 -10 9 21.56 1.62 -5 10 -9 22.36 1.71 5 -10 10 36.63 1.88 -5 10 -10 41.82 1.91 5 -10 11 22.00 1.76 -5 10 -11 25.56 1.69 5 -10 12 17.49 2.29 -5 10 -12 15.48 1.50 5 -10 13 104.19 4.39 -5 10 -13 103.46 4.46 5 -10 14 53.57 3.23 -5 10 -14 60.63 2.87 5 -10 15 10.85 1.57 -5 10 -15 11.79 1.35 5 -10 16 24.26 2.03 -5 10 -16 27.86 2.12 5 -10 17 1.59 2.05 -5 10 -17 0.58 1.37 5 -9 -14 49.71 4.78 -5 9 14 54.99 5.69 5 -9 -13 165.52 7.40 -5 9 13 162.72 7.52 5 -9 -12 116.78 5.23 -5 9 12 113.62 4.78 5 -9 -11 -0.12 1.91 -5 9 11 0.43 1.57 5 -9 -10 8.54 2.94 -5 9 10 7.28 1.91 5 -9 -9 141.50 5.86 -5 9 9 152.45 5.57 5 -9 -8 234.23 10.08 -5 9 8 247.81 8.01 5 -9 -7 167.67 6.46 -5 9 7 191.47 7.48 5 -9 -6 0.55 1.30 -5 9 6 -0.70 1.54 5 -9 -5 10.71 1.50 -5 9 5 11.84 1.35 5 -9 -4 39.41 2.27 -5 9 4 38.76 2.12 5 -9 -3 8.66 1.30 -5 9 3 7.86 1.16 5 -9 -2 249.79 7.77 -5 9 2 256.40 9.60 5 -9 -1 504.04 15.68 -5 9 1 520.44 22.50 5 -9 0 431.27 13.00 -5 9 0 375.71 11.60 5 -9 1 61.60 2.97 -5 9 -1 63.26 4.03 5 -9 2 3.86 0.94 -5 9 -2 4.75 0.99 5 -9 3 93.84 3.23 -5 9 -3 106.82 3.83 5 -9 4 183.32 5.33 -5 9 -4 190.60 8.75 5 -9 5 171.74 8.83 5 -9 6 67.26 2.68 -5 9 -6 67.94 2.73 5 -9 7 67.24 2.89 -5 9 -7 67.65 2.65 5 -9 8 31.38 2.44 -5 9 -8 26.60 1.52 -5 9 -9 0.89 1.04 5 -9 10 22.00 2.41 -5 9 -10 23.30 1.47 5 -9 11 209.10 9.36 -5 9 -11 193.01 6.49 5 -9 12 94.93 3.79 -5 9 -12 94.83 3.91 5 -9 13 39.91 2.80 -5 9 -13 46.79 2.34 5 -9 14 2.10 1.81 -5 9 -14 1.33 1.01 5 -9 15 0.14 1.50 -5 9 -15 1.25 1.33 5 -9 16 1.66 1.57 -5 9 -16 1.57 0.99 5 -9 17 29.54 2.77 -5 9 -17 27.11 2.17 5 -9 18 4.20 1.54 -5 9 -18 5.23 1.57 5 -8 -15 31.02 3.18 -5 8 15 30.48 2.92 5 -8 -14 0.07 2.07 -5 8 14 -0.05 2.03 5 -8 -13 4.08 2.10 -5 8 13 5.55 2.03 5 -8 -12 165.93 7.16 -5 8 12 179.60 7.28 5 -8 -11 234.13 8.06 -5 8 11 236.84 8.49 5 -8 -10 99.17 4.17 -5 8 10 100.86 4.80 5 -8 -9 8.88 2.87 -5 8 9 10.47 1.78 5 -8 -8 1.33 1.30 -5 8 8 5.11 1.71 5 -8 -7 5.64 1.66 -5 8 7 6.01 1.69 5 -8 -6 25.95 1.83 -5 8 6 27.08 1.64 5 -8 -5 75.75 3.42 -5 8 5 69.63 3.30 5 -8 -4 231.60 8.27 -5 8 4 236.79 9.82 5 -8 -3 360.39 11.19 -5 8 3 356.99 10.64 5 -8 -2 174.54 5.91 -5 8 2 188.99 6.10 5 -8 -1 0.63 0.89 -5 8 1 0.99 0.89 5 -8 0 130.69 6.17 -5 8 0 145.72 6.03 5 -8 1 276.49 12.81 -5 8 -1 265.97 8.54 5 -8 2 95.10 3.83 -5 8 -2 74.43 2.87 5 -8 3 18.55 2.36 -5 8 -3 20.45 1.59 5 -8 4 34.17 2.51 -5 8 -4 27.45 1.57 5 -8 5 5.57 0.77 -5 8 -5 5.16 0.80 5 -8 6 12.83 1.21 -5 8 -6 14.45 1.13 5 -8 7 115.40 4.56 -5 8 -7 124.21 4.20 -5 8 -8 312.32 13.12 5 -8 9 193.74 6.44 -5 8 -9 165.09 5.79 5 -8 10 71.22 3.16 -5 8 -10 76.16 2.80 5 -8 11 15.31 1.42 -5 8 -11 12.88 1.13 5 -8 12 16.13 2.15 -5 8 -12 21.92 1.71 5 -8 13 54.36 2.87 -5 8 -13 53.64 2.80 5 -8 14 67.24 4.58 -5 8 -14 71.53 3.16 5 -8 15 5.45 1.52 -5 8 -15 4.39 1.40 5 -8 16 5.43 1.93 -5 8 -16 10.11 1.59 5 -8 17 15.97 1.88 -5 8 -17 17.20 1.74 5 -8 18 3.16 1.91 -5 8 -18 5.45 1.81 5 -7 -16 4.29 2.68 -5 7 16 2.63 2.70 5 -7 -15 4.56 2.48 -5 7 15 5.98 2.53 5 -7 -14 11.14 2.56 -5 7 14 11.36 2.36 5 -7 -13 152.50 5.98 -5 7 13 150.11 7.16 5 -7 -12 142.70 5.93 -5 7 12 156.96 6.27 5 -7 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8.73 0.87 -5 -7 19 9.14 0.77 5 7 -18 4.32 1.28 -5 -7 18 4.63 0.72 5 7 -17 0.70 0.68 -5 -7 17 0.51 0.70 5 7 -16 7.16 0.87 -5 -7 16 5.86 0.94 5 7 -15 0.02 0.68 -5 -7 15 0.22 0.65 5 7 -14 12.98 1.42 -5 -7 14 16.13 0.94 5 7 -13 46.28 2.10 -5 -7 13 47.70 2.87 5 7 -12 273.54 11.77 -5 -7 12 282.01 8.39 5 7 -11 336.10 16.01 -5 -7 11 289.97 8.92 -5 -7 10 103.27 3.79 -5 -7 9 10.42 0.96 -5 -7 8 148.15 4.94 5 7 -7 77.30 3.42 -5 -7 7 78.21 2.80 5 7 -6 92.73 3.86 -5 -7 6 82.39 3.59 5 7 -5 32.03 1.98 -5 -7 5 28.00 1.59 5 7 -4 14.37 1.71 -5 -7 4 15.19 1.21 5 7 -3 5.26 0.89 -5 -7 3 5.45 0.92 5 7 -2 0.43 1.09 -5 -7 2 -0.17 0.96 5 7 -1 129.61 6.03 -5 -7 1 120.42 4.92 5 7 0 680.24 18.86 -5 -7 0 701.37 19.92 5 7 1 576.99 18.62 -5 -7 -1 601.40 19.51 5 7 2 194.46 6.83 -5 -7 -2 206.86 7.38 5 7 3 0.39 1.59 -5 -7 -3 0.77 1.52 5 7 4 0.65 1.64 -5 -7 -4 2.15 1.52 5 7 5 145.12 6.61 -5 -7 -5 137.40 6.46 5 7 6 263.82 11.12 -5 -7 -6 275.59 10.83 5 7 7 54.92 6.90 -5 -7 -7 58.27 4.20 5 7 8 92.18 5.91 -5 -7 -8 96.35 5.35 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6.27 2.12 6 -17 -2 31.45 3.04 -6 17 2 28.99 2.58 6 -17 -1 42.81 3.79 -6 17 1 49.42 3.23 6 -17 0 23.10 3.16 -6 17 0 26.07 3.28 6 -17 1 1.83 1.52 -6 17 -1 1.40 1.71 6 -17 2 36.10 3.28 -6 17 -2 36.49 2.68 6 -17 3 53.18 3.01 -6 17 -3 51.88 2.82 6 -17 4 76.89 5.16 -6 17 -4 73.92 5.09 6 -17 5 8.10 1.59 -6 17 -5 6.90 2.94 6 -17 6 0.58 1.40 -6 17 -6 2.44 1.33 6 -17 7 2.48 2.19 -6 17 -7 2.29 2.24 6 -17 8 1.83 1.47 -6 17 -8 2.22 1.52 6 -17 9 6.51 2.10 -6 17 -9 5.88 1.23 6 -17 10 6.27 1.33 -6 17 -10 3.09 1.16 6 -16 -4 20.26 3.83 -6 16 4 19.20 2.51 6 -16 -3 6.75 2.36 -6 16 3 5.52 2.17 6 -16 -2 21.42 2.53 -6 16 2 15.03 2.39 6 -16 -1 19.27 2.27 -6 16 1 26.96 2.24 6 -16 0 48.50 3.14 -6 16 0 64.73 3.64 6 -16 1 63.84 4.39 -6 16 -1 57.93 3.52 6 -16 2 20.07 1.95 -6 16 -2 21.85 2.05 6 -16 3 0.55 1.33 -6 16 -3 2.46 1.54 6 -16 4 3.30 1.45 -6 16 -4 1.83 1.54 6 -16 5 12.88 1.81 -6 16 -5 12.90 1.78 6 -16 6 48.07 2.36 -6 16 -6 42.81 2.65 6 -16 7 64.18 3.59 -6 16 -7 76.94 3.74 6 -16 8 48.38 3.21 -6 16 -8 36.42 2.12 6 -16 9 38.73 3.33 -6 16 -9 40.08 2.12 6 -16 10 0.89 1.25 -6 16 -10 1.52 1.28 6 -16 11 4.58 1.59 -6 16 -11 4.58 1.71 -6 16 -12 23.08 2.32 6 -15 -5 8.92 2.22 -6 15 5 4.82 2.03 6 -15 -4 20.38 2.63 -6 15 4 20.64 3.76 6 -15 -3 55.08 4.80 -6 15 3 47.49 3.55 6 -15 -2 60.29 3.21 -6 15 2 55.54 3.33 6 -15 -1 54.29 3.09 -6 15 1 61.31 3.18 6 -15 0 6.42 2.12 -6 15 0 3.59 2.10 6 -15 1 3.62 1.37 -6 15 -1 3.79 1.50 6 -15 2 85.33 4.24 -6 15 -2 64.23 3.33 6 -15 3 153.20 8.73 -6 15 -3 156.48 5.67 6 -15 4 81.18 3.55 -6 15 -4 74.11 3.47 6 -15 5 2.27 1.66 -6 15 -5 5.47 2.36 6 -15 6 15.07 1.59 -6 15 -6 13.53 1.66 6 -15 7 6.46 1.40 -6 15 -7 7.57 1.28 6 -15 8 31.81 3.23 -6 15 -8 27.47 1.88 6 -15 9 78.36 4.08 -6 15 -9 70.13 3.06 -6 15 -10 54.58 2.82 6 -15 11 25.25 2.00 6 -15 12 5.93 2.03 -6 15 -12 5.62 1.11 6 -15 13 1.62 1.52 -6 15 -13 1.35 0.99 6 -14 -7 26.19 3.69 -6 14 7 24.77 2.56 6 -14 -6 100.84 5.02 -6 14 6 112.63 5.50 6 -14 -5 143.38 6.34 -6 14 5 128.64 5.62 6 -14 -4 69.12 4.46 -6 14 4 77.88 3.74 6 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1 35.77 2.44 6 -13 0 14.40 1.83 -6 13 0 15.70 1.78 6 -13 1 1.71 1.33 -6 13 -1 0.89 1.35 6 -13 2 5.81 2.12 -6 13 -2 3.42 1.66 6 -13 3 20.45 1.52 -6 13 -3 21.56 1.71 6 -13 4 86.99 4.05 -6 13 -4 102.52 3.86 6 -13 5 51.27 2.82 -6 13 -5 52.09 2.77 6 -13 6 83.71 3.62 6 -13 7 33.64 2.19 -6 13 -7 40.08 3.01 6 -13 8 36.01 3.30 -6 13 -8 32.08 1.91 6 -13 9 49.80 2.70 -6 13 -9 46.86 2.73 6 -13 10 64.97 3.30 -6 13 -10 75.03 3.06 6 -13 11 10.39 1.25 -6 13 -11 7.48 1.18 6 -13 12 5.45 1.30 -6 13 -12 6.39 1.16 6 -13 13 10.27 1.52 -6 13 -13 9.29 1.47 6 -13 14 -0.77 1.78 -6 13 -14 0.58 0.96 6 -13 15 17.90 2.34 -6 13 -15 20.79 1.54 6 -12 -10 21.97 3.33 -6 12 10 16.01 3.93 6 -12 -9 23.44 2.87 -6 12 9 19.37 2.77 6 -12 -8 0.96 1.86 -6 12 8 2.00 2.00 6 -12 -7 15.70 2.22 -6 12 7 11.46 2.12 6 -12 -6 42.83 3.30 -6 12 6 44.57 3.30 6 -12 -5 186.07 6.97 -6 12 5 205.27 7.74 6 -12 -4 66.61 3.64 -6 12 4 80.29 3.76 6 -12 -3 2.60 1.95 -6 12 3 -0.02 1.83 6 -12 -2 36.25 2.99 -6 12 2 40.81 3.98 6 -12 -1 75.92 5.60 -6 12 1 76.21 5.26 6 -12 0 77.68 4.27 -6 12 0 80.89 3.47 6 -12 1 101.03 3.83 -6 12 -1 105.97 6.39 6 -12 2 170.10 6.27 -6 12 -2 169.91 5.33 -6 12 -3 148.90 5.19 6 -12 4 46.50 2.44 -6 12 -4 48.69 3.52 6 -12 5 23.83 1.95 -6 12 -5 22.79 1.59 6 -12 6 67.34 3.45 -6 12 -6 67.77 2.99 6 -12 7 211.13 6.61 -6 12 -7 205.05 6.78 6 -12 8 106.48 4.29 -6 12 -8 110.97 4.34 6 -12 9 6.29 1.52 -6 12 -9 4.05 1.28 6 -12 10 0.07 1.78 -6 12 -10 -0.10 1.21 6 -12 11 0.92 1.45 -6 12 -11 0.51 1.01 6 -12 12 14.18 1.76 -6 12 -12 16.67 1.54 6 -12 13 34.51 2.92 -6 12 -13 32.97 2.15 6 -12 14 33.33 2.03 -6 12 -14 31.67 2.03 6 -12 15 72.28 4.49 -6 12 -16 2.56 1.11 6 -11 -11 2.34 2.53 -6 11 11 3.69 2.48 6 -11 -10 0.48 2.32 -6 11 10 0.34 2.05 6 -11 -9 65.05 6.10 -6 11 9 59.21 3.91 6 -11 -8 288.64 10.80 -6 11 8 289.68 11.31 6 -11 -7 76.69 4.41 -6 11 7 80.99 3.83 6 -11 -6 4.46 1.71 -6 11 6 4.75 1.54 6 -11 -5 18.02 1.83 -6 11 5 18.43 1.91 6 -11 -4 114.03 4.17 -6 11 4 114.22 4.70 6 -11 -3 208.79 7.28 -6 11 3 250.56 9.04 6 -11 -2 180.18 5.88 -6 11 2 168.05 5.88 6 -11 -1 102.72 4.12 -6 11 1 108.94 4.15 6 -11 0 46.21 2.63 -6 11 0 44.71 2.39 6 -11 1 10.64 1.50 -6 11 -1 13.29 2.05 6 -11 2 4.03 1.13 -6 11 -2 3.71 1.09 6 -11 3 128.67 5.50 -6 11 -3 136.72 4.94 6 -11 4 342.40 10.18 -6 11 -4 344.23 10.47 6 -11 5 243.44 11.05 -6 11 -5 287.48 8.59 6 -11 6 51.18 3.14 -6 11 -6 56.85 2.68 6 -11 7 6.85 1.30 -6 11 -7 6.22 1.16 6 -11 8 6.92 1.13 -6 11 -8 7.07 1.23 6 -11 9 1.95 1.13 -6 11 -9 0.05 0.84 6 -11 10 45.03 2.73 -6 11 -10 41.39 2.10 6 -11 11 46.04 2.82 -6 11 -11 51.90 3.74 6 -11 12 43.10 4.22 -6 11 -12 47.13 2.36 6 -11 13 6.56 1.57 -6 11 -13 8.88 1.69 6 -11 14 -0.12 2.12 -6 11 -14 0.24 1.11 6 -11 15 3.88 1.40 -6 11 -15 4.63 1.11 6 -11 16 44.18 2.68 -6 11 -16 56.72 4.34 6 -10 -12 16.79 2.94 6 -10 -11 68.45 7.43 -6 10 11 69.94 5.72 6 -10 -10 130.07 6.22 -6 10 10 134.58 6.97 6 -10 -9 45.75 3.67 -6 10 9 54.58 3.52 6 -10 -8 3.28 1.88 -6 10 8 1.28 1.86 6 -10 -7 71.41 4.03 -6 10 7 73.41 3.81 6 -10 -6 60.85 3.50 -6 10 6 60.92 3.23 6 -10 -5 23.08 2.22 -6 10 5 27.06 2.58 6 -10 -4 8.13 1.62 -6 10 4 11.19 2.63 6 -10 -3 5.31 1.62 -6 10 3 7.57 1.37 6 -10 -2 2.99 1.33 -6 10 2 3.09 1.13 6 -10 -1 0.75 1.25 -6 10 1 -0.39 1.18 6 -10 0 136.02 5.57 -6 10 0 144.51 5.06 6 -10 1 345.20 10.85 -6 10 -1 365.72 11.09 6 -10 2 255.48 8.18 -6 10 -2 224.08 7.45 6 -10 3 124.25 6.39 -6 10 -3 110.75 5.50 6 -10 4 0.82 1.04 -6 10 -4 -0.10 1.09 6 -10 5 25.66 2.10 -6 10 -5 36.78 2.24 6 -10 6 128.47 6.83 -6 10 -6 139.33 4.92 6 -10 7 70.25 2.92 -6 10 -7 68.64 2.87 6 -10 8 1.93 1.25 -6 10 -8 -0.02 1.25 6 -10 9 1.45 1.18 -6 10 -9 1.52 1.06 6 -10 10 26.12 2.39 -6 10 -10 30.44 1.76 6 -10 11 2.29 1.11 -6 10 -11 3.64 1.04 6 -10 12 8.73 1.47 -6 10 -12 10.01 1.25 6 -10 13 52.12 4.03 -6 10 -13 50.45 2.85 6 -10 14 41.65 2.89 -6 10 -14 42.88 2.77 6 -10 15 32.87 2.19 -6 10 -15 32.53 1.93 6 -10 16 3.59 1.50 -6 10 -16 3.69 1.37 6 -10 17 1.66 2.05 -6 10 -17 2.10 1.47 6 -9 -13 184.91 12.06 -6 9 13 186.33 7.38 6 -9 -12 29.09 3.26 -6 9 12 25.61 3.06 6 -9 -11 1.76 2.15 -6 9 11 0.39 2.15 6 -9 -10 53.54 6.44 -6 9 10 66.44 4.10 6 -9 -9 218.55 8.08 -6 9 9 212.14 10.68 6 -9 -8 183.54 7.38 -6 9 8 203.12 7.55 6 -9 -7 33.60 2.94 -6 9 7 32.80 2.36 6 -9 -6 2.15 1.23 -6 9 6 3.62 1.28 6 -9 -5 19.39 1.76 -6 9 5 20.14 1.64 6 -9 -4 38.97 2.44 -6 9 4 37.65 2.24 6 -9 -3 24.41 1.62 -6 9 3 27.95 1.86 6 -9 -2 254.92 13.02 -6 9 2 256.06 7.98 6 -9 -1 321.59 10.83 -6 9 1 350.98 10.93 6 -9 0 253.50 8.78 -6 9 0 241.97 9.14 6 -9 1 27.25 1.62 -6 9 -1 26.92 1.74 6 -9 2 5.79 0.96 -6 9 -2 5.79 1.45 6 -9 3 192.77 7.62 -6 9 -3 197.50 7.04 6 -9 4 297.27 10.32 -6 9 -4 335.14 14.11 6 -9 5 130.11 4.56 -6 9 -5 131.15 4.87 6 -9 6 41.39 2.48 -6 9 -6 44.88 2.32 6 -9 7 19.99 1.50 -6 9 -7 17.56 1.37 6 -9 8 0.05 0.89 -6 9 -8 1.04 0.87 6 -9 9 23.25 1.64 -6 9 -9 23.15 1.40 6 -9 10 62.03 3.21 -6 9 -10 54.14 3.71 6 -9 11 118.39 7.55 -6 9 -11 128.38 4.87 6 -9 12 113.21 5.02 -6 9 -12 110.43 4.53 6 -9 13 72.40 3.88 -6 9 -13 72.55 5.14 6 -9 14 0.10 1.50 -6 9 -14 -0.22 1.16 6 -9 15 5.84 2.24 -6 9 -15 7.33 1.57 6 -9 16 14.86 3.18 -6 9 -16 14.78 1.81 -6 9 -17 6.32 1.81 6 -8 -14 -0.77 1.91 -6 8 14 -1.98 2.29 6 -8 -13 11.05 2.58 -6 8 13 8.97 2.41 6 -8 -12 118.54 6.01 -6 8 12 127.92 6.78 6 -8 -11 156.16 7.31 -6 8 11 160.33 6.44 6 -8 -10 95.34 4.53 -6 8 10 91.04 5.81 6 -8 -9 -0.14 2.27 -6 8 9 3.18 1.45 6 -8 -8 35.26 2.85 -6 8 8 37.09 2.89 6 -8 -7 127.32 5.33 -6 8 7 120.35 4.37 6 -8 -6 16.76 1.86 -6 8 6 16.38 1.64 6 -8 -5 187.11 9.16 -6 8 5 172.49 7.81 6 -8 -4 265.75 9.02 -6 8 4 280.10 9.62 6 -8 -3 110.48 4.65 -6 8 3 110.05 4.61 6 -8 -2 60.90 3.11 -6 8 2 65.05 3.33 6 -8 -1 -0.36 1.04 -6 8 1 -0.89 1.18 6 -8 0 75.34 3.30 -6 8 0 85.21 4.08 6 -8 1 241.80 8.68 -6 8 -1 279.07 9.09 6 -8 2 68.74 3.47 -6 8 -2 73.68 3.11 6 -8 3 92.93 3.64 -6 8 -3 91.65 3.88 6 -8 4 11.09 1.30 -6 8 -4 12.37 1.28 6 -8 5 40.32 2.34 -6 8 -5 38.81 2.19 6 -8 6 43.97 2.24 -6 8 -6 49.51 2.24 6 -8 7 44.42 4.20 -6 8 -7 54.96 2.70 6 -8 8 183.56 6.25 -6 8 -8 148.37 5.60 6 -8 9 82.84 3.42 -6 8 -9 82.58 3.76 6 -8 10 76.81 3.50 -6 8 -10 82.34 3.33 -6 8 -11 1.25 1.42 6 -8 12 58.97 3.04 -6 8 -12 59.47 2.80 6 -8 13 100.33 6.10 -6 8 -13 98.30 4.29 6 -8 14 41.89 3.21 -6 8 -14 41.46 3.23 6 -8 15 6.70 1.62 -6 8 -15 8.10 1.50 6 -8 16 1.33 1.88 -6 8 -16 2.75 1.69 6 -8 17 0.70 1.52 -6 8 -17 0.68 1.42 6 -7 -15 10.23 2.56 -6 7 15 9.70 2.12 6 -7 -14 122.16 5.33 -6 7 14 111.16 5.69 6 -7 -13 165.76 9.41 -6 7 13 157.44 6.54 6 -7 -12 45.05 3.67 -6 7 12 46.57 3.35 6 -7 -11 1.42 2.24 -6 7 11 0.41 2.75 6 -7 -10 106.96 5.67 -6 7 10 105.88 5.09 6 -7 -9 119.77 4.65 -6 7 9 130.45 5.04 6 -7 -8 20.86 1.83 -6 7 8 21.63 1.76 6 -7 -7 66.69 4.41 -6 7 7 69.72 4.80 6 -7 -6 201.89 7.16 -6 7 6 191.37 9.62 6 -7 -5 127.39 4.61 -6 7 5 121.14 4.27 6 -7 -4 13.19 1.40 -6 7 4 15.19 1.45 6 -7 -3 6.37 1.50 -6 7 3 8.44 1.47 6 -7 -2 182.02 6.46 -6 7 2 191.21 6.58 6 -7 -1 373.32 11.99 -6 7 1 367.48 11.07 6 -7 0 258.90 7.98 -6 7 0 256.11 7.79 6 -7 1 18.81 1.45 -6 7 -1 17.73 1.47 6 -7 2 58.08 2.68 -6 7 -2 53.57 2.63 6 -7 3 29.79 1.66 -6 7 -3 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12.76 1.98 -7 -9 4 17.92 2.05 7 9 -3 4.56 2.39 -7 -9 3 5.45 2.00 7 9 -2 3.21 1.81 -7 -9 2 4.56 1.64 7 9 -1 50.91 3.69 -7 -9 1 49.18 3.96 7 9 0 120.64 6.68 -7 -9 0 130.52 7.28 7 9 1 110.41 4.99 -7 -9 -1 116.71 5.26 7 9 2 38.71 5.04 -7 -9 -2 36.68 4.44 -7 -10 16 4.97 0.68 7 10 -15 7.62 1.18 -7 -10 15 8.44 0.96 7 10 -14 39.50 2.94 -7 -10 14 34.56 2.39 7 10 -13 0.84 1.16 -7 -10 13 0.87 0.84 7 10 -12 17.00 2.36 -7 -10 12 18.35 2.17 7 10 -11 25.47 2.15 -7 -10 11 27.37 1.66 7 10 -10 72.81 3.40 -7 -10 10 69.46 4.00 7 10 -9 61.55 3.40 -7 -10 9 65.84 3.55 7 10 -8 16.52 1.50 -7 -10 8 20.31 1.54 7 10 -7 0.10 2.68 -7 -10 7 0.58 1.64 7 10 -6 2.10 2.63 -7 -10 6 3.04 1.45 7 10 -5 53.08 3.67 -7 -10 5 52.50 3.01 7 10 -4 149.14 9.72 -7 -10 4 135.64 5.45 7 10 -3 148.30 6.63 -7 -10 3 166.85 7.96 7 10 -2 68.01 4.61 -7 -10 2 78.86 3.76 7 10 -1 15.00 2.65 -7 -10 1 15.68 2.22 7 10 0 3.28 2.22 -7 -10 0 1.57 1.81 -7 -11 14 16.81 1.59 -7 -11 13 48.14 3.59 7 11 -12 58.34 3.09 -7 -11 12 47.92 2.53 7 11 -11 13.94 1.83 -7 -11 11 10.08 1.40 7 11 -10 0.80 2.27 -7 -11 10 1.35 1.25 7 11 -9 9.72 2.00 -7 -11 9 12.57 1.83 7 11 -8 24.50 2.41 -7 -11 8 25.71 1.78 7 11 -7 10.13 2.36 -7 -11 7 10.78 1.66 7 11 -6 53.66 3.30 -7 -11 6 59.47 3.30 7 11 -5 57.57 3.45 -7 -11 5 62.87 2.97 7 11 -4 2.24 2.73 -7 -11 4 3.50 1.88 7 11 -3 1.13 2.03 -7 -11 3 0.31 1.86 7 11 -2 0.51 1.91 -7 -11 2 0.84 1.69 7 11 -1 54.24 4.12 -7 -11 1 57.86 4.24 7 12 -12 1.04 1.83 -7 -12 12 1.01 0.99 7 12 -11 9.53 2.27 -7 -12 11 9.12 1.16 7 12 -10 20.60 2.10 -7 -12 10 23.32 2.24 7 12 -9 29.04 4.00 -7 -12 9 24.17 1.83 7 12 -8 16.93 2.51 -7 -12 8 18.69 1.71 7 12 -7 -0.10 2.05 -7 -12 7 -0.34 1.45 7 12 -6 6.20 2.68 -7 -12 6 5.79 1.69 7 12 -5 3.30 2.05 -7 -12 5 3.04 1.69 7 12 -4 27.37 2.60 -7 -12 4 26.87 2.60 7 12 -3 24.41 4.56 -7 -12 3 40.18 3.67 7 13 -9 1.59 2.82 -7 -13 9 3.40 1.21 7 13 -8 12.98 2.22 -7 -13 8 10.68 1.33 7 13 -7 8.15 2.27 -7 -13 7 6.87 1.66 7 13 -6 13.29 1.93 -7 -13 6 10.93 1.64 7 13 -5 46.26 4.61 -7 -13 5 58.05 3.57 7 13 -4 16.52 4.05 -7 -13 4 17.90 2.48 8 -18 3 0.39 2.22 -8 18 -3 1.25 3.69 8 -18 4 4.51 1.74 -8 18 -4 3.83 1.74 -8 18 -5 15.51 3.09 8 -17 0 1.62 3.62 8 -17 1 34.58 2.94 -8 17 -1 35.86 3.21 8 -17 2 48.19 3.83 -8 17 -2 44.64 3.50 8 -17 3 10.42 2.58 -8 17 -3 8.63 2.68 8 -17 4 4.05 1.57 -8 17 -4 4.27 1.64 8 -17 5 12.78 3.26 -8 17 -5 9.31 2.87 8 -17 6 12.64 2.12 -8 17 -6 12.32 1.81 8 -17 7 25.88 3.98 -8 17 -7 18.64 2.32 8 -16 -2 24.53 4.10 8 -16 -1 16.21 2.65 -8 16 1 14.74 2.53 8 -16 0 25.28 2.92 -8 16 0 22.36 2.60 8 -16 1 16.57 2.41 -8 16 -1 9.38 2.32 8 -16 2 27.64 3.16 -8 16 -2 31.16 3.04 8 -16 3 1.16 1.66 -8 16 -3 -0.60 1.76 8 -16 4 13.84 2.27 -8 16 -4 16.04 2.27 8 -16 5 51.61 3.59 -8 16 -5 47.39 3.38 8 -16 6 56.48 3.52 -8 16 -6 48.84 2.77 -8 16 -7 8.54 2.05 8 -16 8 0.46 1.81 -8 16 -8 -0.41 1.81 8 -16 9 2.00 1.50 -8 16 -9 1.23 1.13 8 -15 -3 54.46 4.15 -8 15 3 51.03 5.98 8 -15 -2 8.06 2.07 -8 15 2 7.91 2.05 8 -15 -1 13.24 2.12 -8 15 1 11.17 2.03 8 -15 0 9.82 2.27 -8 15 0 9.14 2.19 8 -15 1 24.84 3.01 -8 15 -1 22.82 2.82 8 -15 2 51.73 3.16 -8 15 -2 61.55 3.47 8 -15 3 45.51 2.99 -8 15 -3 46.81 2.97 8 -15 4 5.72 3.04 -8 15 -4 7.24 2.39 8 -15 5 6.68 1.81 -8 15 -5 6.20 1.78 8 -15 6 6.01 2.27 -8 15 -6 4.90 3.11 8 -15 7 14.95 1.86 -8 15 -7 15.29 1.66 8 -15 8 15.72 3.59 -8 15 -8 10.30 1.81 8 -15 9 10.08 2.82 -8 15 -9 12.78 2.00 8 -15 10 8.01 2.15 -8 15 -10 13.58 1.59 8 -15 11 7.84 2.19 -8 15 -11 16.01 1.69 8 -14 -5 4.27 2.17 -8 14 5 3.57 2.36 8 -14 -4 -0.70 1.98 -8 14 4 1.88 1.83 8 -14 -3 -0.43 2.36 -8 14 3 0.72 2.07 8 -14 -2 27.93 2.82 -8 14 2 26.07 2.92 8 -14 -1 84.68 4.37 -8 14 1 86.61 4.39 8 -14 0 168.56 6.68 -8 14 0 148.44 5.84 8 -14 1 72.81 3.42 -8 14 -1 76.57 3.62 8 -14 2 15.94 2.58 -8 14 -2 14.21 2.46 8 -14 3 8.73 2.46 -8 14 -3 8.68 2.34 8 -14 4 35.48 2.75 -8 14 -4 35.21 2.63 8 -14 5 42.25 3.33 -8 14 -5 46.81 2.99 8 -14 6 46.74 3.09 -8 14 -6 51.73 3.09 8 -14 7 9.36 2.05 -8 14 -7 8.47 1.83 8 -14 8 9.72 2.32 -8 14 -8 10.11 1.64 8 -14 9 8.15 2.22 -8 14 -9 5.62 1.59 8 -14 10 4.56 2.39 -8 14 -10 4.97 1.47 8 -14 11 23.90 3.35 -8 14 -11 20.67 2.19 8 -14 12 17.49 2.32 -8 14 -12 14.04 1.47 8 -13 -7 3.30 2.41 -8 13 7 3.04 2.12 8 -13 -6 5.72 2.48 -8 13 6 4.80 2.68 8 -13 -5 32.32 3.11 -8 13 5 36.76 3.16 8 -13 -4 104.41 7.79 -8 13 4 105.39 4.94 8 -13 -3 179.48 7.40 -8 13 3 161.76 8.90 8 -13 -2 103.30 4.92 -8 13 2 101.82 5.55 8 -13 -1 18.23 2.68 -8 13 1 20.21 2.29 8 -13 0 7.36 2.12 -8 13 0 6.99 1.98 8 -13 1 69.97 4.20 -8 13 -1 72.40 3.59 8 -13 2 177.96 7.33 -8 13 -2 135.59 5.88 8 -13 3 109.74 5.40 -8 13 -3 99.27 4.22 8 -13 4 23.59 2.32 -8 13 -4 24.74 2.32 8 -13 5 0.36 1.62 -8 13 -5 0.87 1.37 8 -13 6 1.59 1.93 -8 13 -6 1.30 1.86 8 -13 7 3.38 1.45 -8 13 -7 2.70 1.45 8 -13 8 9.62 1.69 -8 13 -8 11.07 1.76 8 -13 9 78.04 4.24 -8 13 -9 71.48 4.08 8 -13 10 31.06 2.60 -8 13 -10 34.83 2.41 8 -13 11 10.71 2.00 -8 13 -11 12.52 1.88 8 -13 12 0.31 1.35 -8 13 -12 1.86 1.42 8 -13 13 1.33 1.16 -8 13 -13 2.80 1.57 8 -12 -8 13.67 2.58 -8 12 8 14.81 2.41 8 -12 -7 6.61 2.24 -8 12 7 4.70 2.70 8 -12 -6 36.56 2.94 -8 12 6 36.59 2.73 8 -12 -5 66.08 4.92 -8 12 5 67.79 4.20 8 -12 -4 72.59 4.00 -8 12 4 74.35 3.83 8 -12 -3 0.12 2.05 -8 12 3 1.40 1.76 8 -12 -2 49.95 3.11 -8 12 2 50.94 3.45 8 -12 -1 253.33 9.19 -8 12 1 222.46 10.32 8 -12 0 87.79 5.26 -8 12 0 89.16 4.03 8 -12 1 12.35 1.83 -8 12 -1 13.19 1.86 8 -12 2 0.46 1.64 -8 12 -2 1.06 1.64 8 -12 3 9.26 1.66 -8 12 -3 9.38 1.64 8 -12 4 11.60 1.78 -8 12 -4 11.41 1.71 8 -12 5 30.03 2.65 -8 12 -5 29.13 2.58 8 -12 6 35.91 3.62 -8 12 -6 38.32 2.63 8 -12 7 21.34 2.12 -8 12 -7 18.18 1.88 8 -12 8 54.02 2.70 -8 12 -8 35.16 2.73 8 -12 9 10.93 2.03 -8 12 -9 13.92 1.81 8 -12 10 4.87 1.45 -8 12 -10 5.06 1.59 8 -12 11 20.96 2.51 -8 12 -11 26.53 2.63 8 -12 12 23.15 2.29 -8 12 -12 21.18 2.07 8 -12 13 -0.80 1.69 -8 12 -13 3.30 1.78 8 -11 -10 6.73 3.40 -8 11 10 45.15 4.49 8 -11 -9 29.83 4.27 -8 11 9 24.24 3.04 8 -11 -8 5.86 2.17 -8 11 8 4.73 2.07 8 -11 -7 21.66 2.87 -8 11 7 19.27 2.44 8 -11 -6 -1.69 1.83 -8 11 6 -1.91 1.76 8 -11 -5 9.31 1.95 -8 11 5 6.95 1.88 8 -11 -4 138.46 5.69 -8 11 4 128.31 5.76 8 -11 -3 196.17 9.12 -8 11 3 235.94 8.32 8 -11 -2 75.87 3.57 -8 11 2 73.61 4.22 8 -11 -1 1.09 1.64 -8 11 1 2.15 1.74 8 -11 0 20.69 2.22 -8 11 0 18.67 2.05 8 -11 1 26.67 2.12 -8 11 -1 25.18 2.00 8 -11 2 94.83 3.74 -8 11 -2 111.69 4.44 8 -11 3 130.60 6.05 -8 11 -3 130.31 5.14 8 -11 4 109.59 4.20 -8 11 -4 112.92 4.70 8 -11 5 104.33 4.97 -8 11 -5 102.84 4.94 8 -11 6 24.77 1.69 -8 11 -6 25.23 2.10 8 -11 7 9.33 1.83 -8 11 -7 7.81 1.83 8 -11 8 55.59 3.06 -8 11 -8 55.28 2.77 8 -11 9 75.51 4.90 -8 11 -9 74.52 3.45 8 -11 10 41.17 2.65 -8 11 -10 36.37 3.33 8 -11 11 15.46 2.87 -8 11 -11 15.99 1.93 8 -11 12 0.87 2.03 -8 11 -12 1.09 1.52 8 -11 13 1.30 1.47 -8 11 -13 1.50 1.37 -8 11 -14 1.86 1.54 8 -10 -11 0.36 4.51 -8 10 11 0.75 4.00 8 -10 -10 3.14 5.14 -8 10 10 3.93 3.88 8 -10 -9 -0.34 2.10 -8 10 9 -0.41 2.29 8 -10 -8 2.65 2.73 -8 10 8 3.67 2.56 8 -10 -7 65.07 4.24 -8 10 7 54.82 3.98 8 -10 -6 353.76 13.46 -8 10 6 410.15 15.15 8 -10 -5 122.76 6.87 -8 10 5 130.72 5.55 8 -10 -4 5.57 1.81 -8 10 4 7.14 2.03 8 -10 -3 4.87 1.81 -8 10 3 1.93 1.76 8 -10 -2 49.42 3.14 -8 10 2 43.60 2.80 8 -10 -1 83.11 4.10 -8 10 1 79.76 4.05 8 -10 0 36.10 2.70 -8 10 0 37.14 2.48 8 -10 1 17.75 2.24 -8 10 -1 21.25 2.53 8 -10 2 88.75 4.10 -8 10 -2 89.45 4.08 8 -10 3 10.49 1.86 -8 10 -3 9.91 1.78 8 -10 4 10.95 2.44 -8 10 -4 8.92 2.29 8 -10 5 63.16 3.16 -8 10 -5 60.80 3.01 8 -10 6 150.49 5.72 -8 10 -6 157.85 5.28 8 -10 7 131.30 5.38 -8 10 -7 130.79 5.74 8 -10 8 20.67 2.10 -8 10 -8 19.63 2.05 8 -10 9 0.94 1.74 -8 10 -9 1.83 1.52 8 -10 10 23.44 2.41 -8 10 -10 27.37 2.17 8 -10 11 47.63 2.94 -8 10 -11 39.96 2.70 8 -10 12 14.76 2.39 -8 10 -12 19.37 2.29 8 -10 13 5.62 2.65 -8 10 -13 10.18 1.93 8 -10 14 7.09 1.50 -8 10 -14 8.25 1.66 8 -9 -12 6.54 2.48 -8 9 12 9.84 2.65 8 -9 -11 13.96 3.14 -8 9 11 17.68 3.21 8 -9 -10 14.86 2.70 -8 9 10 13.31 2.65 8 -9 -9 94.03 7.52 -8 9 9 109.40 5.19 8 -9 -8 264.96 10.13 -8 9 8 260.74 9.94 8 -9 -7 150.45 6.51 -8 9 7 155.97 6.25 8 -9 -6 0.80 1.71 -8 9 6 0.65 1.50 8 -9 -5 51.18 3.09 -8 9 5 56.17 3.06 8 -9 -4 22.91 2.07 -8 9 4 20.81 1.91 8 -9 -3 109.40 4.80 -8 9 3 111.01 6.78 8 -9 -2 49.08 2.87 -8 9 2 51.93 2.77 8 -9 -1 29.23 1.98 -8 9 1 25.81 2.03 8 -9 0 0.27 1.37 -8 9 0 0.77 1.33 8 -9 1 0.07 1.69 -8 9 -1 -0.55 1.35 8 -9 2 24.07 2.07 -8 9 -2 24.21 1.95 8 -9 3 231.22 7.62 -8 9 -3 198.66 7.21 8 -9 4 179.15 9.89 -8 9 -4 166.03 5.93 8 -9 5 28.75 2.03 -8 9 -5 21.61 1.81 8 -9 6 1.13 2.32 -8 9 -6 1.35 1.47 8 -9 7 15.89 1.93 -8 9 -7 15.72 1.81 8 -9 8 140.44 5.11 -8 9 -8 132.24 5.04 8 -9 9 69.94 3.55 -8 9 -9 78.60 4.03 8 -9 10 49.37 4.10 -8 9 -10 46.45 3.16 8 -9 11 23.44 2.70 -8 9 -11 21.27 1.95 8 -9 12 0.92 1.74 -8 9 -12 3.11 1.62 8 -9 13 1.81 2.34 -8 9 -13 0.51 1.83 8 -9 14 2.53 3.57 -8 9 -14 -0.19 2.24 8 -9 15 10.80 1.93 -8 9 -15 11.34 2.07 8 -8 -13 16.57 2.65 -8 8 13 16.45 2.68 8 -8 -12 29.25 3.69 -8 8 12 29.13 3.62 8 -8 -11 133.54 6.08 -8 8 11 128.06 6.61 8 -8 -10 70.91 4.08 -8 8 10 74.86 3.86 8 -8 -9 -0.12 1.69 -8 8 9 -0.43 1.64 8 -8 -8 110.07 8.68 -8 8 8 112.89 5.11 8 -8 -7 393.77 12.78 -8 8 7 410.65 17.56 8 -8 -6 557.99 17.44 -8 8 6 577.72 22.33 8 -8 -5 44.16 3.47 -8 8 5 45.78 3.40 8 -8 -4 15.85 2.36 -8 8 4 12.88 2.27 8 -8 -3 3.50 2.00 -8 8 3 5.16 2.12 8 -8 -2 48.79 2.97 -8 8 2 51.56 2.73 8 -8 -1 54.31 2.89 -8 8 1 44.81 2.65 8 -8 0 141.96 5.23 -8 8 0 141.40 5.60 8 -8 1 227.33 7.65 -8 8 -1 238.93 11.14 8 -8 2 142.85 5.16 -8 8 -2 133.49 5.02 8 -8 3 5.33 1.42 -8 8 -3 4.80 1.18 8 -8 4 3.79 2.34 -8 8 -4 2.46 1.45 8 -8 5 95.24 4.90 -8 8 -5 92.42 4.00 8 -8 6 325.15 10.35 -8 8 -6 291.73 10.49 8 -8 7 143.50 5.57 -8 8 -7 143.86 5.23 8 -8 8 16.69 2.19 -8 8 -8 18.45 2.00 8 -8 9 3.30 2.24 -8 8 -9 3.64 1.69 8 -8 10 8.18 1.95 -8 8 -10 7.31 1.93 8 -8 11 25.81 2.41 -8 8 -11 27.49 2.17 8 -8 12 36.37 3.79 -8 8 -12 47.90 3.45 8 -8 13 28.94 2.82 -8 8 -13 36.06 2.58 8 -8 14 28.84 2.77 -8 8 -14 31.91 2.53 8 -7 -14 2.97 2.15 -8 7 14 2.36 2.29 8 -7 -13 5.47 2.89 -8 7 13 3.88 2.80 8 -7 -12 2.68 2.19 -8 7 12 2.07 2.19 8 -7 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120.90 6.13 10 0 0 52.17 3.62 -10 0 0 56.24 3.18 10 0 1 3.79 2.27 -10 0 -1 2.41 2.07 10 0 2 0.31 4.10 -10 0 -2 -0.84 2.17 10 0 3 29.66 3.88 -10 0 -3 38.90 3.88 10 1 -18 1.42 1.74 -10 -1 18 3.23 1.64 10 1 -17 7.50 3.62 -10 -1 17 7.28 2.10 10 1 -16 30.36 2.82 -10 -1 16 27.30 2.56 10 1 -15 35.62 4.46 -10 -1 15 35.65 4.29 10 1 -14 10.35 2.17 -10 -1 14 14.59 2.05 10 1 -13 -1.54 2.46 -10 -1 13 0.87 2.00 10 1 -12 34.51 2.80 -10 -1 12 36.30 2.77 10 1 -11 11.58 2.19 -10 -1 11 10.64 1.86 10 1 -10 28.34 3.81 -10 -1 10 30.70 2.70 10 1 -9 42.33 3.30 -10 -1 9 46.84 3.04 10 1 -8 57.64 3.35 -10 -1 8 52.99 3.52 10 1 -7 83.81 4.10 -10 -1 7 85.79 3.93 10 1 -6 14.42 2.24 -10 -1 6 10.32 2.00 10 1 -5 35.31 3.67 -10 -1 5 28.63 2.60 10 1 -4 261.39 9.21 -10 -1 4 252.01 8.56 10 1 -3 223.91 8.06 -10 -1 3 218.29 8.01 10 1 -2 61.98 4.00 -10 -1 2 53.76 3.57 10 1 -1 0.82 1.91 -10 -1 1 0.63 1.74 10 1 0 1.64 2.22 -10 -1 0 1.21 1.86 10 1 1 24.72 3.33 -10 -1 -1 23.03 3.14 10 1 2 126.57 6.46 -10 -1 -2 130.89 6.78 10 2 -18 10.64 2.56 -10 -2 18 21.20 2.41 10 2 -17 15.10 2.44 -10 -2 17 12.44 2.27 10 2 -16 1.11 2.12 -10 -2 16 0.89 1.95 10 2 -15 15.75 2.56 -10 -2 15 18.91 2.07 10 2 -14 39.96 2.89 -10 -2 14 33.45 3.88 10 2 -13 55.35 3.14 -10 -2 13 65.50 3.59 10 2 -12 62.20 3.59 -10 -2 12 58.41 3.06 10 2 -11 39.63 2.82 -10 -2 11 41.22 2.80 10 2 -10 6.87 2.48 -10 -2 10 11.60 2.51 10 2 -9 5.79 1.81 -10 -2 9 5.02 1.64 10 2 -8 2.05 1.69 -10 -2 8 2.36 1.66 10 2 -7 50.70 2.97 -10 -2 7 51.13 3.16 10 2 -6 153.22 6.15 -10 -2 6 157.22 6.37 10 2 -5 182.02 7.55 -10 -2 5 178.13 8.78 10 2 -4 10.30 2.12 -10 -2 4 12.71 2.03 10 2 -3 47.17 3.01 -10 -2 3 47.87 2.89 10 2 -2 6.08 2.24 -10 -2 2 7.52 1.91 10 2 -1 36.78 2.92 -10 -2 1 36.54 2.68 10 2 0 76.45 5.47 -10 -2 0 75.39 4.34 10 2 1 122.47 5.57 -10 -2 -1 116.30 6.15 10 3 -18 1.76 1.98 -10 -3 18 1.81 1.59 10 3 -17 7.16 2.41 -10 -3 17 8.54 1.78 10 3 -16 22.36 2.48 -10 -3 16 25.47 2.56 10 3 -15 17.58 2.32 -10 -3 15 15.80 2.03 10 3 -14 6.58 2.05 -10 -3 14 4.92 2.32 10 3 -13 0.31 1.62 -10 -3 13 0.43 1.47 10 3 -12 0.92 2.32 -10 -3 12 -0.92 2.10 10 3 -11 9.98 1.69 -10 -3 11 11.60 1.95 10 3 -10 64.73 3.35 -10 -3 10 63.53 3.33 10 3 -9 124.62 5.14 -10 -3 9 139.59 6.15 10 3 -8 96.28 4.24 -10 -3 8 104.38 5.06 10 3 -7 12.47 1.93 -10 -3 7 10.47 1.88 10 3 -6 9.89 1.83 -10 -3 6 9.94 1.93 10 3 -5 20.26 2.41 -10 -3 5 26.36 2.24 10 3 -4 69.19 3.88 -10 -3 4 75.44 3.74 10 3 -3 38.06 3.50 -10 -3 3 33.35 2.68 10 3 -2 3.55 3.98 -10 -3 2 7.77 2.60 10 3 -1 2.41 4.10 -10 -3 1 -0.58 2.15 10 3 0 1.50 2.22 -10 -3 0 0.87 1.71 10 4 -17 0.07 2.00 -10 -4 17 1.40 1.86 10 4 -16 -0.10 1.42 -10 -4 16 -0.94 1.33 10 4 -15 3.91 2.17 -10 -4 15 4.32 2.12 10 4 -14 13.39 1.98 -10 -4 14 11.87 1.91 10 4 -13 26.84 2.92 -10 -4 13 37.17 4.20 10 4 -12 55.95 3.30 -10 -4 12 59.40 3.16 10 4 -11 81.61 5.26 -10 -4 11 82.55 4.51 10 4 -10 20.19 2.53 -10 -4 10 17.41 2.41 10 4 -9 2.29 3.71 -10 -4 9 0.10 1.62 10 4 -8 10.47 2.29 -10 -4 8 11.31 2.10 10 4 -7 96.47 5.81 -10 -4 7 85.40 4.17 10 4 -6 80.24 4.44 -10 -4 6 66.85 3.28 10 4 -5 15.39 2.46 -10 -4 5 12.73 2.07 10 4 -4 4.29 2.73 -10 -4 4 8.44 2.19 10 4 -3 1.30 2.24 -10 -4 3 -1.16 1.93 10 4 -2 1.13 2.19 -10 -4 2 0.80 2.03 10 4 -1 14.23 2.77 -10 -4 1 16.04 2.39 10 5 -16 5.69 1.76 -10 -5 16 5.04 1.33 10 5 -15 19.78 2.36 -10 -5 15 14.95 2.10 10 5 -14 26.77 2.56 -10 -5 14 21.08 2.32 10 5 -13 8.15 2.00 -10 -5 13 8.27 1.88 10 5 -12 -0.41 1.30 -10 -5 12 1.01 1.69 10 5 -11 4.68 2.03 -10 -5 11 4.99 1.47 10 5 -10 97.36 7.40 -10 -5 10 78.84 4.63 10 5 -9 93.12 4.51 -10 -5 9 93.62 4.08 10 5 -8 41.60 3.06 -10 -5 8 39.53 2.65 10 5 -7 14.62 2.60 -10 -5 7 14.90 2.39 10 5 -6 2.99 2.22 -10 -5 6 1.42 1.66 10 5 -5 34.97 3.33 -10 -5 5 31.98 2.41 10 5 -4 19.39 2.56 -10 -5 4 19.46 2.27 10 5 -3 31.64 3.11 -10 -5 3 30.03 3.47 10 5 -2 34.30 3.96 -10 -5 2 30.12 4.08 10 6 -16 5.16 2.92 10 6 -15 -0.63 2.17 -10 -6 15 1.45 1.91 10 6 -14 0.31 1.47 -10 -6 14 1.13 1.25 -10 -6 13 2.12 2.00 10 6 -12 19.92 2.82 -10 -6 12 18.21 1.91 10 6 -11 50.21 3.42 -10 -6 11 46.86 3.23 10 6 -10 16.88 2.19 -10 -6 10 20.79 1.86 10 6 -9 2.80 2.03 -10 -6 9 0.92 1.74 10 6 -8 39.70 4.94 -10 -6 8 35.69 3.06 10 6 -7 81.04 5.23 -10 -6 7 70.79 3.50 10 6 -6 54.70 3.76 -10 -6 6 52.75 3.74 10 6 -5 27.74 5.21 -10 -6 5 26.99 3.42 10 6 -4 6.17 2.41 -10 -6 4 8.44 2.22 10 7 -14 28.99 2.27 -10 -7 14 24.79 2.00 10 7 -13 10.88 3.30 -10 -7 13 13.17 1.74 10 7 -12 -0.55 2.34 -10 -7 12 0.51 1.59 10 7 -11 9.53 3.23 -10 -7 11 10.15 1.86 10 7 -10 30.68 3.59 -10 -7 10 36.39 2.75 10 7 -9 27.04 2.65 -10 -7 9 22.43 2.73 10 7 -8 51.54 3.09 -10 -7 8 42.25 3.26 10 7 -7 13.41 2.48 -10 -7 7 15.31 2.05 10 7 -6 -1.66 3.45 -10 -7 6 1.37 2.00 10 7 -5 -0.36 2.07 -10 -7 5 0.55 1.86 10 8 -12 16.30 2.05 -10 -8 12 18.26 1.76 10 8 -11 9.89 2.12 -10 -8 11 9.53 2.19 10 8 -10 1.30 2.03 -10 -8 10 2.56 1.54 10 8 -9 0.43 2.03 -10 -8 9 1.28 1.57 10 8 -8 12.18 2.68 -10 -8 8 9.36 2.03 10 8 -7 36.35 5.79 -10 -8 7 40.98 3.16 10 9 -10 9.33 2.24 -10 -9 10 9.45 2.12 10 9 -9 -0.41 2.34 -10 -9 9 0.29 1.71 11 -10 -3 12.81 3.09 -11 10 3 12.76 3.96 11 -10 -2 21.46 3.45 -11 10 2 25.71 3.33 11 -10 -1 27.95 2.73 -11 10 1 27.23 2.85 11 -10 0 43.85 3.42 -11 10 0 41.00 3.26 11 -10 1 15.24 2.53 -11 10 -1 16.23 2.39 11 -10 2 -0.10 2.41 -11 10 -2 -0.39 2.32 11 -9 -5 87.06 4.58 -11 9 5 71.65 4.44 11 -9 -4 52.72 3.71 -11 9 4 44.55 3.57 11 -9 -3 41.02 3.55 -11 9 3 36.61 4.34 11 -9 -2 41.02 3.67 -11 9 2 36.78 3.35 11 -9 -1 3.76 3.18 -11 9 1 -0.51 3.04 11 -9 0 46.02 6.85 -11 9 0 47.08 3.79 11 -9 1 63.65 3.33 -11 9 -1 64.01 4.08 11 -9 2 3.01 2.77 -11 9 -2 4.61 2.58 11 -9 3 15.48 2.75 -11 9 -3 14.11 2.65 -11 8 6 19.66 4.51 11 -8 -5 10.97 2.46 -11 8 5 9.48 2.53 11 -8 -4 -1.01 2.46 -11 8 4 0.92 2.29 11 -8 -3 21.44 3.04 -11 8 3 18.18 2.70 11 -8 -2 135.35 5.81 -11 8 2 125.44 5.11 11 -8 -1 93.07 3.59 -11 8 1 94.52 4.70 11 -8 0 21.30 3.69 -11 8 0 21.54 2.85 11 -8 1 2.15 2.34 -11 8 -1 0.31 2.03 11 -8 2 27.93 3.26 -11 8 -2 22.67 2.75 11 -8 3 10.90 3.23 -11 8 -3 11.65 3.11 11 -7 -8 -0.58 2.41 -11 7 8 -1.83 2.51 11 -7 -7 0.48 2.65 -11 7 7 3.14 2.48 11 -7 -6 21.49 5.09 -11 7 6 17.44 4.90 11 -7 -5 108.72 9.12 -11 7 5 85.45 6.63 11 -7 -4 3.28 2.53 -11 7 4 111.35 7.55 11 -7 -3 22.89 2.85 -11 7 3 22.00 2.46 11 -7 -2 1.59 1.86 -11 7 2 -1.42 2.07 11 -7 -1 25.54 2.94 -11 7 1 26.29 2.73 11 -7 0 69.10 4.22 -11 7 0 59.76 3.52 11 -7 1 116.61 6.15 -11 7 -1 113.69 5.04 11 -7 2 31.62 2.99 -11 7 -2 37.58 2.70 11 -7 3 2.17 2.22 -11 7 -3 2.29 2.00 11 -6 -9 3.01 3.09 -11 6 9 1.86 3.14 11 -6 -8 35.55 3.33 -11 6 8 32.46 3.14 11 -6 -7 68.86 4.61 -11 6 7 65.36 4.00 11 -6 -6 86.58 5.45 -11 6 6 78.86 4.70 11 -6 -5 31.47 6.29 -11 6 5 13.43 3.33 11 -6 -4 6.49 4.85 -11 6 4 1.98 3.86 11 -6 -3 5.72 2.53 -11 6 3 46.35 5.26 11 -6 -2 76.79 4.08 -11 6 2 73.37 4.12 11 -6 -1 24.96 2.73 -11 6 1 23.13 2.46 11 -6 0 1.93 2.15 -11 6 0 2.53 2.10 11 -6 1 -0.02 2.22 -11 6 -1 0.70 2.17 11 -6 2 -2.39 2.27 -11 6 -2 -0.89 2.03 11 -6 3 7.33 2.32 -11 6 -3 6.85 2.24 -11 5 11 34.37 4.37 11 -5 -10 16.59 3.47 -11 5 10 9.70 4.58 11 -5 -9 43.12 3.76 -11 5 9 43.97 4.08 11 -5 -8 33.81 3.23 -11 5 8 29.83 3.28 11 -5 -7 -0.14 2.34 -11 5 7 1.47 2.53 11 -5 -6 18.06 3.47 -11 5 6 25.88 3.40 11 -5 -5 57.95 3.96 -11 5 5 54.63 3.45 11 -5 -4 42.93 4.29 -11 5 4 22.67 2.85 11 -5 -3 10.27 4.92 -11 5 3 5.21 3.86 11 -5 -2 1.62 3.26 -11 5 2 0.75 2.70 11 -5 -1 2.39 2.19 -11 5 1 0.94 2.03 11 -5 0 34.61 3.04 -11 5 0 30.46 2.77 11 -5 1 71.05 4.78 -11 5 -1 70.40 4.27 11 -5 2 59.31 3.71 -11 5 -2 59.09 3.57 -11 4 12 4.24 5.19 11 -4 -11 8.63 2.36 -11 4 11 7.21 2.22 11 -4 -10 1.59 3.18 -11 4 10 3.50 2.99 11 -4 -9 20.86 3.01 -11 4 9 21.22 3.06 11 -4 -8 161.20 6.85 -11 4 8 153.41 6.46 11 -4 -7 110.43 5.98 -11 4 7 107.85 8.39 11 -4 -6 34.30 4.94 -11 4 6 21.90 3.52 11 -4 -5 3.01 2.51 -11 4 5 2.80 2.41 11 -4 -4 6.83 2.46 -11 4 4 6.56 2.34 11 -4 -3 40.01 3.64 -11 4 3 45.03 3.30 -11 4 2 46.67 4.51 11 -4 -1 17.22 3.98 -11 4 1 15.56 3.38 -11 4 0 55.04 3.71 11 -4 1 30.51 3.38 -11 4 -1 28.68 3.04 11 -4 2 -1.13 2.53 -11 4 -2 -1.28 2.19 -11 3 13 1.66 3.59 11 -3 -12 1.83 2.29 -11 3 12 0.14 2.34 11 -3 -11 31.71 2.89 -11 3 11 34.90 3.26 11 -3 -10 125.22 10.85 -11 3 10 105.13 5.45 11 -3 -9 150.54 6.85 -11 3 9 139.38 6.46 11 -3 -8 0.55 2.32 -11 3 8 2.75 2.44 11 -3 -7 22.55 2.94 -11 3 7 24.55 2.97 11 -3 -6 -0.07 3.71 -11 3 6 4.63 2.75 11 -3 -5 72.93 5.96 -11 3 5 64.37 4.17 11 -3 -4 97.51 5.06 -11 3 4 86.44 4.24 11 -3 -3 42.21 3.55 -11 3 3 36.49 3.47 11 -3 -2 3.33 2.22 -11 3 2 4.15 2.03 11 -3 -1 1.74 3.62 -11 3 1 2.75 1.71 11 -3 0 3.21 3.47 -11 3 0 2.32 2.82 -11 3 -1 43.27 3.50 11 -2 -13 33.02 4.17 -11 2 13 36.03 3.55 11 -2 -12 49.56 3.98 -11 2 12 51.66 3.59 11 -2 -11 7.21 2.34 -11 2 11 8.75 2.24 11 -2 -10 18.52 2.94 -11 2 10 19.58 3.23 11 -2 -9 45.94 3.33 -11 2 9 49.95 3.55 11 -2 -8 191.57 8.44 -11 2 8 175.29 8.08 11 -2 -7 62.08 4.80 -11 2 7 67.12 4.22 11 -2 -6 1.04 2.22 -11 2 6 0.24 2.15 11 -2 -5 4.80 2.92 -11 2 5 4.37 2.60 11 -2 -4 8.78 3.01 -11 2 4 11.62 3.09 11 -2 -3 36.54 3.26 -11 2 3 38.59 3.06 11 -2 -2 66.47 4.73 -11 2 2 65.29 3.45 11 -2 -1 86.10 4.24 -11 2 1 87.11 4.41 11 -2 0 100.69 9.62 11 -1 -14 11.02 2.77 -11 1 14 8.95 2.46 11 -1 -13 -0.02 2.32 -11 1 13 0.14 2.41 11 -1 -12 10.66 4.53 -11 1 12 13.82 3.16 11 -1 -11 21.85 2.46 -11 1 11 15.48 2.41 11 -1 -10 11.60 2.27 -11 1 10 12.69 2.19 11 -1 -9 7.19 2.70 -11 1 9 6.49 2.19 11 -1 -8 1.88 2.65 -11 1 8 1.52 1.98 11 -1 -7 7.93 2.34 -11 1 7 9.31 2.48 11 -1 -6 24.24 2.92 -11 1 6 25.59 2.92 11 -1 -5 68.16 4.46 -11 1 5 60.70 3.86 11 -1 -4 96.45 5.40 -11 1 4 91.74 4.87 11 -1 -3 107.18 6.05 -11 1 3 113.30 5.35 11 -1 -2 64.30 4.10 -11 1 2 62.30 3.86 11 -1 -1 0.46 2.10 -11 1 1 -1.23 2.15 11 -1 0 7.38 2.94 -11 1 0 6.51 2.58 11 0 -15 0.17 2.73 -11 0 15 -0.12 2.41 11 0 -14 12.03 2.80 -11 0 14 15.05 2.99 11 0 -13 52.48 3.69 -11 0 13 56.29 3.71 11 0 -12 53.54 3.71 -11 0 12 50.72 3.59 11 0 -11 9.19 2.56 -11 0 11 10.03 2.80 11 0 -10 0.58 1.91 -11 0 10 1.62 1.86 11 0 -9 31.14 2.32 -11 0 9 29.79 2.75 11 0 -8 27.01 2.99 -11 0 8 30.24 2.85 11 0 -7 26.60 4.00 -11 0 7 29.06 2.89 11 0 -6 39.34 3.14 -11 0 6 35.48 2.73 11 0 -5 65.07 3.91 -11 0 5 64.73 4.03 11 0 -4 0.02 2.05 -11 0 4 0.39 1.93 11 0 -3 5.09 2.19 -11 0 3 5.28 1.95 11 0 -2 28.41 3.47 -11 0 2 26.24 3.14 11 0 -1 91.55 6.66 -11 0 1 88.51 5.33 11 1 -15 20.62 2.63 -11 -1 15 15.87 2.36 11 1 -14 3.98 2.36 -11 -1 14 0.17 2.32 11 1 -13 1.78 2.51 -11 -1 13 1.54 2.29 11 1 -12 35.67 3.04 -11 -1 12 40.86 3.38 11 1 -11 34.22 3.52 -11 -1 11 33.40 3.26 11 1 -10 27.01 4.15 -11 -1 10 24.91 3.26 11 1 -9 3.57 2.07 -11 -1 9 3.30 1.86 11 1 -8 0.77 1.91 -11 -1 8 1.91 1.74 11 1 -7 -1.06 2.56 -11 -1 7 0.34 1.83 11 1 -6 9.21 2.53 -11 -1 6 8.44 2.32 11 1 -5 78.00 4.56 -11 -1 5 75.87 3.79 11 1 -4 136.12 6.78 -11 -1 4 120.40 5.69 11 1 -3 93.70 8.18 -11 -1 3 86.10 4.68 11 1 -2 37.09 3.88 -11 -1 2 37.24 3.38 11 2 -16 1.06 2.48 -11 -2 16 -0.34 2.24 11 2 -15 7.43 2.00 -11 -2 15 6.78 1.95 11 2 -14 21.15 2.75 -11 -2 14 25.59 2.80 11 2 -13 41.92 3.28 -11 -2 13 42.78 3.21 11 2 -12 17.70 2.82 -11 -2 12 16.18 2.29 11 2 -11 0.96 1.91 -11 -2 11 -0.92 1.74 11 2 -10 2.82 2.34 -11 -2 10 0.99 2.10 11 2 -9 3.35 2.75 -11 -2 9 2.39 2.56 11 2 -8 22.21 2.73 -11 -2 8 24.89 3.09 11 2 -7 56.63 4.00 -11 -2 7 67.84 3.74 11 2 -6 56.51 3.38 -11 -2 6 57.38 3.52 11 2 -5 60.08 5.60 -11 -2 5 52.43 3.18 11 2 -4 8.80 3.35 -11 -2 4 8.06 2.99 11 2 -3 1.64 3.11 -11 -2 3 -0.89 2.82 11 3 -16 11.48 1.95 -11 -3 16 11.24 1.83 11 3 -15 7.62 2.53 -11 -3 15 10.30 2.51 11 3 -14 3.18 2.00 -11 -3 14 0.55 1.76 11 3 -13 6.15 2.27 -11 -3 13 5.09 1.88 11 3 -12 25.20 2.87 -11 -3 12 23.80 2.58 11 3 -11 39.48 2.63 -11 -3 11 41.87 2.87 11 3 -10 43.92 4.78 -11 -3 10 33.81 3.16 11 3 -9 16.47 2.48 -11 -3 9 19.00 2.46 11 3 -8 44.57 3.30 -11 -3 8 30.80 2.85 11 3 -7 18.76 3.33 -11 -3 7 23.71 3.09 11 3 -6 0.19 2.48 -11 -3 6 -0.72 2.87 11 3 -5 23.37 2.48 -11 -3 5 21.95 2.48 11 4 -15 10.54 1.98 -11 -4 15 14.93 1.86 11 4 -14 8.59 2.75 -11 -4 14 6.85 3.79 11 4 -13 3.91 2.10 -11 -4 13 2.68 1.88 11 4 -12 3.26 2.29 -11 -4 12 1.91 1.66 11 4 -11 9.72 2.87 -11 -4 11 11.41 2.65 11 4 -10 2.75 2.65 -11 -4 10 3.62 2.15 11 4 -9 -1.11 2.34 -11 -4 9 0.55 2.07 11 4 -8 47.54 3.33 -11 -4 8 51.30 2.97 11 4 -7 125.17 5.45 -11 -4 7 138.82 5.67 11 4 -6 73.90 7.28 -11 -4 6 66.93 3.93 11 5 -14 -0.63 2.58 -11 -5 14 0.24 2.12 11 5 -13 1.33 1.62 -11 -5 13 0.53 1.09 -11 -5 12 2.05 2.05 11 5 -11 17.73 2.32 -11 -5 11 13.77 1.98 11 5 -10 55.95 3.57 -11 -5 10 54.14 3.35 11 5 -9 62.75 4.03 -11 -5 9 79.66 5.52 11 5 -8 60.10 3.98 -11 -5 8 53.01 3.47 11 6 -13 8.83 3.04 -11 -6 13 5.81 2.58 11 6 -12 14.86 1.81 -11 -6 12 10.37 1.71 11 6 -11 21.01 3.01 -11 -6 11 21.22 2.39 11 6 -10 16.35 3.33 -11 -6 10 11.36 2.10 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 62768 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ru1 Ru 0.55109(2) 0.24090(2) 0.57931(2) 0.01040(6) Uani 1 1 d . . . . . Cl1 Cl 0.37615(7) 0.36170(5) 0.66793(4) 0.01583(10) Uani 1 1 d . . . . . O1 O 0.3166(2) 0.13030(14) 0.44522(12) 0.0139(3) Uani 1 1 d . . . . . O2 O 0.4775(2) 0.10646(14) 0.64027(12) 0.0139(3) Uani 1 1 d . . . . . N1 N 0.6409(2) 0.37328(16) 0.52377(15) 0.0120(3) Uani 1 1 d . . . . . N2 N 0.7881(2) 0.35195(16) 0.70877(14) 0.0125(3) Uani 1 1 d . . . . . C1 C 0.2795(3) 0.1536(2) 0.35643(17) 0.0136(4) Uani 1 1 d . . . . . C2 C 0.1157(3) 0.0618(2) 0.26521(18) 0.0162(4) Uani 1 1 d . . . . . H2 H 0.040558 -0.011483 0.271805 0.019 Uiso 1 1 calc R U . . . C3 C 0.0638(3) 0.0764(2) 0.16811(18) 0.0183(4) Uani 1 1 d . . . . . H3 H -0.045438 0.012918 0.108496 0.022 Uiso 1 1 calc R U . . . C4 C 0.1707(3) 0.1849(2) 0.15555(18) 0.0188(4) Uani 1 1 d . . . . . H4 H 0.133969 0.194361 0.087985 0.023 Uiso 1 1 calc R U . . . C5 C 0.3278(3) 0.2761(2) 0.24200(18) 0.0170(4) Uani 1 1 d . . . . . H5 H 0.397966 0.349774 0.233918 0.020 Uiso 1 1 calc R U . . . C6 C 0.3889(3) 0.2636(2) 0.34393(16) 0.0131(4) Uani 1 1 d . . . . . C7 C 0.5561(3) 0.3663(2) 0.42545(17) 0.0133(4) Uani 1 1 d . . . . . H7 H 0.610533 0.435432 0.407033 0.016 Uiso 1 1 calc R U . . . C8 C 0.8144(3) 0.47486(19) 0.59898(17) 0.0127(4) Uani 1 1 d . . . . . C9 C 0.9049(3) 0.58158(19) 0.58099(18) 0.0153(4) Uani 1 1 d . . . . . H9 H 0.847450 0.593213 0.516806 0.018 Uiso 1 1 calc R U . . . C10 C 1.0796(3) 0.67065(19) 0.65767(19) 0.0178(4) Uani 1 1 d . . . . . H10 H 1.140590 0.744168 0.646234 0.021 Uiso 1 1 calc R U . . . C11 C 1.1661(3) 0.6535(2) 0.75081(19) 0.0189(4) Uani 1 1 d . . . . . H11 H 1.287725 0.713916 0.801324 0.023 Uiso 1 1 calc R U . . . C12 C 1.0765(3) 0.5488(2) 0.77097(18) 0.0168(4) Uani 1 1 d . . . . . H12 H 1.136147 0.537380 0.834882 0.020 Uiso 1 1 calc R U . . . C13 C 0.8975(3) 0.46044(18) 0.69609(17) 0.0129(4) Uani 1 1 d . . . . . C14 C 0.8308(3) 0.3354(2) 0.80029(17) 0.0152(4) Uani 1 1 d . . . . . H14 H 0.942622 0.397861 0.858770 0.018 Uiso 1 1 calc R U . . . C15 C 0.7234(3) 0.2307(2) 0.82044(17) 0.0146(4) Uani 1 1 d . . . . . C16 C 0.7948(3) 0.2358(2) 0.92787(17) 0.0177(4) Uani 1 1 d . . . . . H16 H 0.904967 0.306710 0.980034 0.021 Uiso 1 1 calc R U . . . C17 C 0.7104(3) 0.1420(2) 0.95917(18) 0.0194(4) Uani 1 1 d . . . . . H17 H 0.762302 0.147430 1.031518 0.023 Uiso 1 1 calc R U . . . C18 C 0.5462(3) 0.0378(2) 0.88263(19) 0.0197(4) Uani 1 1 d . . . . . H18 H 0.486455 -0.027835 0.903271 0.024 Uiso 1 1 calc R U . . . C19 C 0.4714(3) 0.0303(2) 0.77802(18) 0.0183(4) Uani 1 1 d . . . . . H19 H 0.358825 -0.040104 0.727824 0.022 Uiso 1 1 calc R U . . . C20 C 0.5572(3) 0.1241(2) 0.74336(16) 0.0135(4) Uani 1 1 d . . . . . O3 O 0.6992(2) 0.13159(14) 0.49576(13) 0.0149(3) Uani 1 1 d D . . . . H1O3 H 0.6520(18) 0.0548(12) 0.456(2) 0.022 Uiso 1 1 d D U . . . C21 C 0.9051(3) 0.1519(2) 0.5340(2) 0.0198(4) Uani 1 1 d D . . . . H21A H 0.942715 0.097201 0.474707 0.030 Uiso 1 1 calc R U . . . H21B H 0.935690 0.128810 0.597352 0.030 Uiso 1 1 calc R U . . . H21C H 0.977031 0.243420 0.556031 0.030 Uiso 1 1 calc R U . . . O1SA O 0.3561(6) 0.4136(4) 0.9074(3) 0.0215(10) Uani 0.439(6) 1 d D . P A 1 H1SA H 0.361000 0.387812 0.842821 0.032 Uiso 0.439(6) 1 calc R U P A 1 C1SA C 0.3093(6) 0.3088(4) 0.9346(4) 0.0745(12) Uani 0.439(6) 1 d D . P A 1 H1S1 H 0.408437 0.265151 0.929529 0.112 Uiso 0.439(6) 1 calc R U P A 1 H1S2 H 0.182142 0.247819 0.883613 0.112 Uiso 0.439(6) 1 calc R U P A 1 H1S3 H 0.303981 0.338878 1.010037 0.112 Uiso 0.439(6) 1 calc R U P A 1 O1SB O 0.3093(6) 0.3088(4) 0.9346(4) 0.0745(12) Uani 0.561(6) 1 d D . P A 2 H1SB H 0.212721 0.241500 0.909862 0.112 Uiso 0.561(6) 1 calc R U P A 2 C1SB C 0.2565(6) 0.4175(4) 0.9851(4) 0.0241(10) Uani 0.561(6) 1 d D . P A 2 H1S4 H 0.197149 0.404464 1.039648 0.036 Uiso 0.561(6) 1 calc R U P A 2 H1S5 H 0.162814 0.429594 0.929358 0.036 Uiso 0.561(6) 1 calc R U P A 2 H1S6 H 0.372528 0.494609 1.021854 0.036 Uiso 0.561(6) 1 calc R U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ru1 0.00389(9) 0.00776(9) 0.01084(9) -0.00265(6) -0.00131(6) -0.00058(6) Cl1 0.0094(2) 0.0143(2) 0.0184(2) 0.00068(18) 0.00370(17) 0.00401(16) O1 0.0060(6) 0.0124(6) 0.0109(6) -0.0024(5) -0.0044(5) -0.0017(5) O2 0.0102(6) 0.0068(6) 0.0148(7) -0.0011(5) -0.0004(5) -0.0029(5) N1 0.0050(7) 0.0047(6) 0.0181(8) -0.0020(6) 0.0027(6) -0.0025(5) N2 0.0043(6) 0.0095(7) 0.0115(7) -0.0042(6) -0.0036(6) -0.0009(5) C1 0.0063(8) 0.0127(8) 0.0126(8) -0.0028(7) -0.0010(6) 0.0027(6) C2 0.0079(8) 0.0128(8) 0.0167(9) -0.0022(8) -0.0013(7) 0.0003(7) C3 0.0106(8) 0.0175(9) 0.0146(9) -0.0020(8) -0.0025(7) 0.0017(7) C4 0.0143(9) 0.0214(10) 0.0146(9) 0.0029(8) 0.0008(7) 0.0053(8) C5 0.0118(9) 0.0186(9) 0.0158(9) 0.0028(8) 0.0015(7) 0.0058(7) C6 0.0071(8) 0.0134(8) 0.0122(8) -0.0007(7) 0.0001(6) 0.0032(6) C7 0.0093(8) 0.0128(8) 0.0146(9) 0.0022(7) 0.0030(7) 0.0034(7) C8 0.0069(8) 0.0092(8) 0.0142(8) -0.0024(7) 0.0014(6) 0.0014(6) C9 0.0112(8) 0.0104(8) 0.0193(9) -0.0002(7) 0.0060(7) 0.0023(7) C10 0.0113(8) 0.0086(8) 0.0241(10) -0.0031(8) 0.0069(8) -0.0003(7) C11 0.0085(8) 0.0128(9) 0.0200(10) -0.0063(8) 0.0026(7) -0.0026(7) C12 0.0076(8) 0.0131(8) 0.0170(9) -0.0039(8) -0.0001(7) -0.0007(7) C13 0.0066(7) 0.0079(7) 0.0149(8) -0.0034(7) 0.0007(6) 0.0004(6) C14 0.0077(8) 0.0123(8) 0.0141(8) -0.0022(7) -0.0028(7) -0.0002(6) C15 0.0087(8) 0.0134(8) 0.0130(8) -0.0017(7) -0.0007(7) 0.0028(7) C16 0.0112(9) 0.0191(10) 0.0130(9) -0.0006(8) -0.0017(7) 0.0031(7) C17 0.0147(9) 0.0233(10) 0.0141(9) 0.0030(8) 0.0011(7) 0.0056(8) C18 0.0170(10) 0.0174(9) 0.0180(10) 0.0024(8) 0.0041(8) 0.0018(8) C19 0.0136(9) 0.0140(9) 0.0158(9) -0.0020(8) 0.0007(7) -0.0004(7) C20 0.0093(8) 0.0132(8) 0.0115(8) -0.0011(7) 0.0008(7) 0.0039(7) O3 0.0059(6) 0.0094(6) 0.0182(7) -0.0052(5) 0.0010(5) 0.0013(5) C21 0.0082(8) 0.0172(9) 0.0248(10) 0.0001(8) 0.0022(7) 0.0031(7) O1SA 0.0231(19) 0.0221(19) 0.0165(17) 0.0053(15) 0.0058(14) 0.0065(15) C1SA 0.069(2) 0.065(2) 0.118(4) 0.040(2) 0.064(3) 0.0348(19) O1SB 0.069(2) 0.065(2) 0.118(4) 0.040(2) 0.064(3) 0.0348(19) C1SB 0.0080(16) 0.0227(19) 0.026(2) -0.0026(16) -0.0011(14) 0.0020(14) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0021 0.0012 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0044 0.0025 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0080 0.0047 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1230 0.1255 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru -1.7757 0.6751 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Ru1 N2 82.98(8) . . ? N1 Ru1 O1 95.39(7) . . ? N2 Ru1 O1 178.04(6) . . ? N1 Ru1 O2 176.28(6) . . ? N2 Ru1 O2 94.09(7) . . ? O1 Ru1 O2 87.49(7) . . ? N1 Ru1 O3 88.50(7) . . ? N2 Ru1 O3 93.47(7) . . ? O1 Ru1 O3 85.39(7) . . ? O2 Ru1 O3 89.39(7) . . ? N1 Ru1 Cl1 91.10(5) . . ? N2 Ru1 Cl1 88.32(6) . . ? O1 Ru1 Cl1 92.81(5) . . ? O2 Ru1 Cl1 91.10(5) . . ? O3 Ru1 Cl1 178.11(4) . . ? C1 O1 Ru1 123.05(13) . . ? C20 O2 Ru1 123.80(13) . . ? C7 N1 C8 122.68(18) . . ? C7 N1 Ru1 123.97(14) . . ? C8 N1 Ru1 113.28(14) . . ? C14 N2 C13 122.58(17) . . ? C14 N2 Ru1 124.16(15) . . ? C13 N2 Ru1 112.96(14) . . ? O1 C1 C2 116.73(19) . . ? O1 C1 C6 125.55(18) . . ? C2 C1 C6 117.7(2) . . ? C3 C2 C1 121.6(2) . . ? C3 C2 H2 119.2 . . ? C1 C2 H2 119.2 . . ? C2 C3 C4 120.86(19) . . ? C2 C3 H3 119.6 . . ? C4 C3 H3 119.6 . . ? C5 C4 C3 119.2(2) . . ? C5 C4 H4 120.4 . . ? C3 C4 H4 120.4 . . ? C4 C5 C6 121.8(2) . . ? C4 C5 H5 119.1 . . ? C6 C5 H5 119.1 . . ? C5 C6 C7 114.9(2) . . ? C5 C6 C1 118.79(18) . . ? C7 C6 C1 126.3(2) . . ? N1 C7 C6 125.5(2) . . ? N1 C7 H7 117.2 . . ? C6 C7 H7 117.2 . . ? C9 C8 C13 119.94(18) . . ? C9 C8 N1 124.7(2) . . ? C13 C8 N1 115.36(18) . . ? C10 C9 C8 119.4(2) . . ? C10 C9 H9 120.3 . . ? C8 C9 H9 120.3 . . ? C11 C10 C9 120.7(2) . . ? C11 C10 H10 119.6 . . ? C9 C10 H10 119.6 . . ? C10 C11 C12 120.63(19) . . ? C10 C11 H11 119.7 . . ? C12 C11 H11 119.7 . . ? C11 C12 C13 119.2(2) . . ? C11 C12 H12 120.4 . . ? C13 C12 H12 120.4 . . ? C12 C13 C8 119.94(19) . . ? C12 C13 N2 124.8(2) . . ? C8 C13 N2 115.27(17) . . ? N2 C14 C15 125.72(18) . . ? N2 C14 H14 117.1 . . ? C15 C14 H14 117.1 . . ? C16 C15 C20 118.1(2) . . ? C16 C15 C14 115.36(18) . . ? C20 C15 C14 126.5(2) . . ? C17 C16 C15 122.3(2) . . ? C17 C16 H16 118.8 . . ? C15 C16 H16 118.8 . . ? C16 C17 C18 119.0(2) . . ? C16 C17 H17 120.5 . . ? C18 C17 H17 120.5 . . ? C19 C18 C17 120.4(2) . . ? C19 C18 H18 119.8 . . ? C17 C18 H18 119.8 . . ? C18 C19 C20 121.7(2) . . ? C18 C19 H19 119.1 . . ? C20 C19 H19 119.1 . . ? O2 C20 C19 117.16(18) . . ? O2 C20 C15 124.4(2) . . ? C19 C20 C15 118.46(19) . . ? C21 O3 Ru1 125.44(13) . . ? C21 O3 H1O3 104.4(10) . . ? Ru1 O3 H1O3 123.8(14) . . ? O3 C21 H21A 109.5 . . ? O3 C21 H21B 109.5 . . ? H21A C21 H21B 109.5 . . ? O3 C21 H21C 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C1SA O1SA H1SA 109.5 . . ? O1SA C1SA H1S1 109.5 . . ? O1SA C1SA H1S2 109.5 . . ? H1S1 C1SA H1S2 109.5 . . ? O1SA C1SA H1S3 109.5 . . ? H1S1 C1SA H1S3 109.5 . . ? H1S2 C1SA H1S3 109.5 . . ? C1SB O1SB H1SB 109.5 . . ? O1SB C1SB H1S4 109.5 . . ? O1SB C1SB H1S5 109.5 . . ? H1S4 C1SB H1S5 109.5 . . ? O1SB C1SB H1S6 109.5 . . ? H1S4 C1SB H1S6 109.5 . . ? H1S5 C1SB H1S6 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ru1 N1 1.9776(19) . ? Ru1 N2 1.992(2) . ? Ru1 O1 2.0119(18) . ? Ru1 O2 2.0237(16) . ? Ru1 O3 2.0692(15) . ? Ru1 Cl1 2.3305(8) . ? O1 C1 1.309(3) . ? O2 C20 1.322(3) . ? N1 C7 1.314(3) . ? N1 C8 1.426(3) . ? N2 C14 1.305(3) . ? N2 C13 1.422(3) . ? C1 C2 1.424(3) . ? C1 C6 1.435(3) . ? C2 C3 1.371(3) . ? C2 H2 0.9500 . ? C3 C4 1.414(3) . ? C3 H3 0.9500 . ? C4 C5 1.370(3) . ? C4 H4 0.9500 . ? C5 C6 1.428(3) . ? C5 H5 0.9500 . ? C6 C7 1.428(3) . ? C7 H7 0.9500 . ? C8 C9 1.395(3) . ? C8 C13 1.410(3) . ? C9 C10 1.388(3) . ? C9 H9 0.9500 . ? C10 C11 1.387(3) . ? C10 H10 0.9500 . ? C11 C12 1.391(3) . ? C11 H11 0.9500 . ? C12 C13 1.398(3) . ? C12 H12 0.9500 . ? C14 C15 1.440(3) . ? C14 H14 0.9500 . ? C15 C16 1.418(3) . ? C15 C20 1.426(3) . ? C16 C17 1.372(3) . ? C16 H16 0.9500 . ? C17 C18 1.405(3) . ? C17 H17 0.9500 . ? C18 C19 1.375(3) . ? C18 H18 0.9500 . ? C19 C20 1.407(3) . ? C19 H19 0.9500 . ? O3 C21 1.441(2) . ? O3 H1O3 0.811(10) . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C21 H21C 0.9800 . ? O1SA C1SA 1.376(5) . ? O1SA H1SA 0.8400 . ? C1SA H1S1 0.9800 . ? C1SA H1S2 0.9800 . ? C1SA H1S3 0.9800 . ? O1SB C1SB 1.395(5) . ? O1SB H1SB 0.8400 . ? C1SB H1S4 0.9800 . ? C1SB H1S5 0.9800 . ? C1SB H1S6 0.9800 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag O3 H1O3 O2 0.811(10) 1.767(9) 2.572(2) 172(2) 2_656 yes C21 H21C Cl1 0.98 2.80 3.456(3) 125.4 1_655 yes O1SA^a H1SA^a Cl1 0.84 2.33 3.155(4) 167.6 . yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Ru1 O1 C1 C2 175.71(13) . . . . ? Ru1 O1 C1 C6 -4.7(3) . . . . ? O1 C1 C2 C3 -179.91(19) . . . . ? C6 C1 C2 C3 0.5(3) . . . . ? C1 C2 C3 C4 -0.7(3) . . . . ? C2 C3 C4 C5 -0.1(3) . . . . ? C3 C4 C5 C6 1.2(3) . . . . ? C4 C5 C6 C7 179.5(2) . . . . ? C4 C5 C6 C1 -1.4(3) . . . . ? O1 C1 C6 C5 -179.02(19) . . . . ? C2 C1 C6 C5 0.5(3) . . . . ? O1 C1 C6 C7 0.0(3) . . . . ? C2 C1 C6 C7 179.53(19) . . . . ? C8 N1 C7 C6 176.20(18) . . . . ? Ru1 N1 C7 C6 -0.3(3) . . . . ? C5 C6 C7 N1 -178.03(19) . . . . ? C1 C6 C7 N1 2.9(3) . . . . ? C7 N1 C8 C9 4.9(3) . . . . ? Ru1 N1 C8 C9 -178.25(15) . . . . ? C7 N1 C8 C13 -173.58(18) . . . . ? Ru1 N1 C8 C13 3.3(2) . . . . ? C13 C8 C9 C10 2.0(3) . . . . ? N1 C8 C9 C10 -176.42(18) . . . . ? C8 C9 C10 C11 1.0(3) . . . . ? C9 C10 C11 C12 -2.0(3) . . . . ? C10 C11 C12 C13 0.0(3) . . . . ? C11 C12 C13 C8 2.9(3) . . . . ? C11 C12 C13 N2 -177.92(18) . . . . ? C9 C8 C13 C12 -3.9(3) . . . . ? N1 C8 C13 C12 174.63(17) . . . . ? C9 C8 C13 N2 176.84(17) . . . . ? N1 C8 C13 N2 -4.6(2) . . . . ? C14 N2 C13 C12 10.6(3) . . . . ? Ru1 N2 C13 C12 -175.48(16) . . . . ? C14 N2 C13 C8 -170.21(18) . . . . ? Ru1 N2 C13 C8 3.7(2) . . . . ? C13 N2 C14 C15 177.79(18) . . . . ? Ru1 N2 C14 C15 4.5(3) . . . . ? N2 C14 C15 C16 -178.0(2) . . . . ? N2 C14 C15 C20 2.8(3) . . . . ? C20 C15 C16 C17 0.4(3) . . . . ? C14 C15 C16 C17 -178.8(2) . . . . ? C15 C16 C17 C18 -0.7(3) . . . . ? C16 C17 C18 C19 0.0(3) . . . . ? C17 C18 C19 C20 1.1(3) . . . . ? Ru1 O2 C20 C19 170.76(14) . . . . ? Ru1 O2 C20 C15 -9.6(3) . . . . ? C18 C19 C20 O2 178.2(2) . . . . ? C18 C19 C20 C15 -1.4(3) . . . . ? C16 C15 C20 O2 -178.98(19) . . . . ? C14 C15 C20 O2 0.1(3) . . . . ? C16 C15 C20 C19 0.6(3) . . . . ? C14 C15 C20 C19 179.7(2) . . . . ?