Crystallography Open Database

Information card for entry 7710924

Preview

Coordinates	7710924.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C98 H182 Al4 Si16
Calculated formula	C98 H182 Al4 Si16
Title of publication	Synthesis of bi- and tetradentate poly-Lewis acids by hydroalumination of poly-alkynyl-anthracene derivatives
Authors of publication	Mitzel, Norbert Werner; Aders, Niklas; Lamm, Jan-Hendrik; Beckmann, Jean Louis; Neumann, Beate; Stammler, Georg
Journal of publication	Dalton Transactions
Year of publication	2022
a	15.1482 ± 0.0003 Å
b	18.535 ± 0.0003 Å
c	23.3981 ± 0.0004 Å
α	102.967 ± 0.002°
β	103.576 ± 0.002°
γ	97.456 ± 0.002°
Cell volume	6106.6 ± 0.2 Å³
Cell temperature	100 ± 0.1 K
Ambient diffraction temperature	100 ± 0.1 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0687
Residual factor for significantly intense reflections	0.0538
Weighted residual factors for significantly intense reflections	0.1331
Weighted residual factors for all reflections included in the refinement	0.1455
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
277157 (current)	2022-08-09	cif/ Adding structures of 7710915, 7710916, 7710917, 7710918, 7710919, 7710920, 7710921, 7710922, 7710923, 7710924, 7710925, 7710926 via cif-deposit CGI script.	7710924.cif