Crystallography Open Database

Information card for entry 7711818

Preview

Coordinates	7711818.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C276 H272 Ag11.55 Cu7.45 F18 P6 Sb3
Calculated formula	C275.999 H271.998 Ag11.531 Cu7.469 F17.9992 P6 Sb3
Title of publication	An alkynyl-protected Ag<sub>13-<i>x</i></sub>Cu<sub>6+<i>x</i></sub> nanocluster for catalytic hydrogenation.
Authors of publication	Gao, Yan-Li; Sun, Xueli; Tang, Xiongkai; Xie, Zhenlang; Tian, Guolong; Nan, Zi-Ang; Yang, Huayan; Shen, Hui
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2022
Journal volume	52
Journal issue	1
Pages of publication	52 - 57
a	20.222 ± 0.0005 Å
b	20.222 ± 0.0005 Å
c	59.983 ± 0.002 Å
α	90°
β	90°
γ	120°
Cell volume	21242.6 ± 1 Å³
Cell temperature	100.01 ± 0.1 K
Ambient diffraction temperature	100.01 ± 0.1 K
Number of distinct elements	7
Space group number	146
Hermann-Mauguin space group symbol	R 3 :H
Hall space group symbol	R 3
Residual factor for all reflections	0.1271
Residual factor for significantly intense reflections	0.0686
Weighted residual factors for significantly intense reflections	0.1703
Weighted residual factors for all reflections included in the refinement	0.2075
Goodness-of-fit parameter for all reflections included in the refinement	1
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
283226 (current)	2023-05-05	cif/ Updating files of 7711818 Original log message: Adding full bibliography for 7711818.cif.	7711818.cif
279446	2022-11-22	cif/ Adding structures of 7711818 via cif-deposit CGI script.	7711818.cif