Crystallography Open Database

Information card for entry 7711853

Preview

Coordinates	7711853.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	bis(thiophen-2-yl)digermene
Formula	C66 H100 Ge2 O0.5 S2
Calculated formula	C66 H100 Ge2 O0.5 S2
Title of publication	A series of (<i>E</i>)-1,2-diaryldigermenes incorporating bulky Eind groups: structural characteristics and absorption properties.
Authors of publication	Yagura, Shogo; Hayakawa, Naoki; Kuroda, Airi; Ota, Kei; Tanishita, Rhota; Urasaki, Genya; Nakahodo, Tsukasa; Nakai, Hidetaka; Hoshino, Manabu; Hashizume, Daisuke; Matsuo, Tsukasa
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2022
a	11.3963 ± 0.0005 Å
b	16.324 ± 0.0006 Å
c	18.0362 ± 0.0007 Å
α	103.576 ± 0.003°
β	105.459 ± 0.003°
γ	95.039 ± 0.003°
Cell volume	3102.8 ± 0.2 Å³
Cell temperature	100 K
Ambient diffraction temperature	100 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1092
Residual factor for significantly intense reflections	0.0867
Weighted residual factors for significantly intense reflections	0.2365
Weighted residual factors for all reflections included in the refinement	0.2553
Goodness-of-fit parameter for all reflections included in the refinement	1.046
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
279657 (current)	2022-12-01	cif/ Adding structures of 7711850, 7711851, 7711852, 7711853 via cif-deposit CGI script.	7711853.cif