Crystallography Open Database

Information card for entry 7711863

Preview

Coordinates	7711863.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H65 N2 Sb Si
Calculated formula	C42 H65 N2 Sb Si
Title of publication	The reactivity of antimony and bismuth <i>N</i>,<i>C</i>,<i>N</i>-pincer compounds toward K[BEt<sub>3</sub>H] - the formation of heterocyclic compounds <i>vs</i>. element-element bonds <i>vs.</i> stable terminal Sb-H bonds.
Authors of publication	Novák, Pavel; Erben, Milan; Jambor, Roman; Hejda, Martin; Růžička, Aleš; Rychagova, Elena; Ketkov, Sergey; Dostál, Libor
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2022
Journal volume	52
Journal issue	1
Pages of publication	218 - 227
a	13.5556 ± 0.0005 Å
b	18.201 ± 0.0006 Å
c	16.9952 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	4193.1 ± 0.3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	33
Hermann-Mauguin space group symbol	P n a 21
Hall space group symbol	P 2c -2n
Residual factor for all reflections	0.0551
Residual factor for significantly intense reflections	0.0386
Weighted residual factors for significantly intense reflections	0.0851
Weighted residual factors for all reflections included in the refinement	0.0911
Goodness-of-fit parameter for all reflections included in the refinement	1.027
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
283232 (current)	2023-05-05	cif/ Updating files of 7711860, 7711861, 7711862, 7711863, 7711864, 7711865 Original log message: Adding full bibliography for 7711860--7711865.cif.	7711863.cif
279661	2022-12-01	cif/ Adding structures of 7711860, 7711861, 7711862, 7711863, 7711864, 7711865 via cif-deposit CGI script.	7711863.cif