Crystallography Open Database

Information card for entry 7711865

Preview

Coordinates	7711865.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H50 Bi F3 N2 O3 S Si
Calculated formula	C37 H50 Bi F3 N2 O3 S Si
Title of publication	The reactivity of antimony and bismuth <i>N</i>,<i>C</i>,<i>N</i>-pincer compounds toward K[BEt<sub>3</sub>H] - the formation of heterocyclic compounds <i>vs</i>. element-element bonds <i>vs.</i> stable terminal Sb-H bonds.
Authors of publication	Novák, Pavel; Erben, Milan; Jambor, Roman; Hejda, Martin; Růžička, Aleš; Rychagova, Elena; Ketkov, Sergey; Dostál, Libor
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2022
Journal volume	52
Journal issue	1
Pages of publication	218 - 227
a	13.8907 ± 0.0007 Å
b	13.5122 ± 0.0005 Å
c	21.3741 ± 0.0009 Å
α	90°
β	92.234 ± 0.002°
γ	90°
Cell volume	4008.7 ± 0.3 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0701
Residual factor for significantly intense reflections	0.0443
Weighted residual factors for significantly intense reflections	0.063
Weighted residual factors for all reflections included in the refinement	0.0674
Goodness-of-fit parameter for all reflections included in the refinement	1.053
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
283232 (current)	2023-05-05	cif/ Updating files of 7711860, 7711861, 7711862, 7711863, 7711864, 7711865 Original log message: Adding full bibliography for 7711860--7711865.cif.	7711865.cif
279661	2022-12-01	cif/ Adding structures of 7711860, 7711861, 7711862, 7711863, 7711864, 7711865 via cif-deposit CGI script.	7711865.cif