Crystallography Open Database

Information card for entry 7711929

7711928 << 7711929 >> 7711930

Preview

Coordinates	7711929.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	[{κP, κC-(i-Pr)2PO-(5-OMe-C6H4}{κN-Et2NH}NiBr]
Formula	C17 H31 Br N Ni O2 P
Calculated formula	C17 H31 Br N Ni O2 P
Title of publication	Reactivities of cyclonickellated complexes with hydroxylamines: formation of κ<sup>O</sup>-hydroxylamine and κ<sup>N</sup>-imine adducts and a κ<sup>O</sup>, κ<sup>N</sup>-aminoxide derivative.
Authors of publication	Sarker, Rajib K.; Mangin, Loïc P; Zargarian, Davit
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2023
Journal volume	52
Journal issue	2
Pages of publication	366 - 375
a	11.3886 ± 0.0004 Å
b	11.7955 ± 0.0004 Å
c	15.524 ± 0.0005 Å
α	90°
β	92.048 ± 0.002°
γ	90°
Cell volume	2084.07 ± 0.12 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0526
Residual factor for significantly intense reflections	0.0516
Weighted residual factors for significantly intense reflections	0.1664
Weighted residual factors for all reflections included in the refinement	0.1684
Goodness-of-fit parameter for all reflections included in the refinement	1.115
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	1.34139 Å
Diffraction radiation type	GaKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
283290 (current)	2023-05-05	cif/ Updating files of 7711929, 7711930, 7711931, 7711932, 7711933, 7711934, 7711935, 7711936, 7711937, 7711938, 7711939 Original log message: Adding full bibliography for 7711929--7711939.cif.	7711929.cif
279895	2022-12-15	cif/ Adding structures of 7711929, 7711930, 7711931, 7711932, 7711933, 7711934, 7711935, 7711936, 7711937, 7711938, 7711939 via cif-deposit CGI script.	7711929.cif