Crystallography Open Database

Information card for entry 7711935

7711934 << 7711935 >> 7711936

Preview

Coordinates	7711935.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H33 Br N Ni O2 P
Calculated formula	C27 H33 Br N Ni O2 P
SMILES	Br[Ni]1([P](Oc2c1ccc(OC)c2)(C(C)C)C(C)C)[N](=Cc1ccccc1)Cc1ccccc1
Title of publication	Reactivities of cyclonickellated complexes with hydroxylamines: formation of κ<sup>O</sup>-hydroxylamine and κ<sup>N</sup>-imine adducts and a κ<sup>O</sup>, κ<sup>N</sup>-aminoxide derivative.
Authors of publication	Sarker, Rajib K.; Mangin, Loïc P; Zargarian, Davit
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2023
Journal volume	52
Journal issue	2
Pages of publication	366 - 375
a	13.143 ± 0.0003 Å
b	15.5918 ± 0.0004 Å
c	13.1678 ± 0.0003 Å
α	90°
β	103.571 ± 0.001°
γ	90°
Cell volume	2623.05 ± 0.11 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0276
Residual factor for significantly intense reflections	0.0272
Weighted residual factors for significantly intense reflections	0.0706
Weighted residual factors for all reflections included in the refinement	0.0709
Goodness-of-fit parameter for all reflections included in the refinement	1.102
Diffraction radiation wavelength	1.34139 Å
Diffraction radiation type	GaKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
283290 (current)	2023-05-05	cif/ Updating files of 7711929, 7711930, 7711931, 7711932, 7711933, 7711934, 7711935, 7711936, 7711937, 7711938, 7711939 Original log message: Adding full bibliography for 7711929--7711939.cif.	7711935.cif
279895	2022-12-15	cif/ Adding structures of 7711929, 7711930, 7711931, 7711932, 7711933, 7711934, 7711935, 7711936, 7711937, 7711938, 7711939 via cif-deposit CGI script.	7711935.cif