Crystallography Open Database

Information card for entry 7712017

7712016 << 7712017 >> 7712018

Preview

Coordinates	7712017.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C88 H114 B6 K2 O4 P6 Sn2
Calculated formula	C88 H114 B6 K2 O4 P6 Sn2
Title of publication	Phosphido-borane-supported stannates.
Authors of publication	Izod, Keith; Madlool, Atheer M.; Craig, Alex; Waddell, Paul G.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2023
Journal volume	52
Journal issue	4
Pages of publication	947 - 954
a	12.5263 ± 0.0004 Å
b	12.841 ± 0.0006 Å
c	16.3428 ± 0.0005 Å
α	83.991 ± 0.003°
β	75.367 ± 0.003°
γ	62.619 ± 0.004°
Cell volume	2258.32 ± 0.17 Å³
Cell temperature	150 ± 0.2 K
Ambient diffraction temperature	150 ± 0.2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0651
Residual factor for significantly intense reflections	0.0399
Weighted residual factors for significantly intense reflections	0.0727
Weighted residual factors for all reflections included in the refinement	0.0811
Goodness-of-fit parameter for all reflections included in the refinement	1.025
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
283277 (current)	2023-05-05	cif/ Updating files of 7712014, 7712015, 7712016, 7712017, 7712018, 7712019, 7712020 Original log message: Adding full bibliography for 7712014--7712020.cif.	7712017.cif
280039	2022-12-25	cif/ Adding structures of 7712014, 7712015, 7712016, 7712017, 7712018, 7712019, 7712020 via cif-deposit CGI script.	7712017.cif